Example #1
0
pulsesequence()
{



/* DECLARE AND LOAD VARIABLES */

char        f1180[MAXSTR],   		      /* Flag to start t1 @ halfdwell */
            mag_flg[MAXSTR],                            /*magic angle gradient*/
            f2180[MAXSTR],    		      /* Flag to start t2 @ halfdwell */
            codecseq[MAXSTR];       /* sequence for 13C' decoupling */
 
int         icosel1,          			  /* used to get n and p type */
            icosel2,
	    t1_counter,  		        /* used for states tppi in t1 */
	    ni2 = getval("ni2");

double      tau1,         				         /*  t1 delay */
            tau2,        				         /*  t2 delay */
	    del = getval("del"),     /* time delays for CH coupling evolution */
	    del1 = getval("del1"),
	    del2 = getval("del2"),
            del3 = getval("del3"),
            del4 = getval("del4"),
            TC = getval("TC"),
            satpwr = getval("satpwr"),
            waltzB1 = getval("waltzB1"),
            spinlock = getval("spinlock"),
            pwco,copwr, cores,codmf,
            kappa,

	pwClvl = getval("pwClvl"), 	        /* coarse power for C13 pulse */
        pwC = getval("pwC"),          /* C13 90 degree pulse length at pwClvl */
	rf0,            	  /* maximum fine power when using pwC pulses */

/* p_d is used to calculate the isotropic mixing on the Cab region            */
        p_d,                  	       /* 50 degree pulse for DIPSI-2 at rfd  */
        rfd,                    /* fine power for 7 kHz rf for 500MHz magnet  */
	ncyc = getval("ncyc"), 			  /* no. of cycles of DIPSI-3 */


   compC = getval("compC"),         /* adjustment for C13 amplifier compression */


	pwNlvl = getval("pwNlvl"),	              /* power for N15 pulses */
        pwN = getval("pwN"),          /* N15 90 degree pulse length at pwNlvl */

        pwHd,                           /* H1 90 degree pulse length at tpwrd */
        tpwrd,                             /*rf for WALTZ decoupling */

	sw1 = getval("sw1"),
	sw2 = getval("sw2"),

	gt1 = getval("gt1"),  		       /* coherence pathway gradients */
	gzcal = getval("gzcal"),               /* G/cm to DAC coversion factor*/
        gstab = getval("gstab"),
        gzlvl1 = getval("gzlvl1"),
	gzlvl2 = getval("gzlvl2"),

	gt3 = getval("gt3"),				   /* other gradients */
	gt5 = getval("gt5"),
	gzlvl3 = getval("gzlvl3"),
	gzlvl4 = getval("gzlvl4"),
	gzlvl5 = getval("gzlvl5"),
	gzlvl6 = getval("gzlvl6");

    getstr("mag_flg",mag_flg);
    getstr("f1180",f1180);
    getstr("f2180",f2180);
    getstr("codecseq",codecseq);

/*   LOAD PHASE TABLE    */

	settable(t1,2,phi1);
	settable(t2,1,phi2);
	settable(t3,1,phi3);
	settable(t4,1,phi4);
	settable(t11,2,rec);

        

/*   INITIALIZE VARIABLES   */

    if( dpwrf < 4095 )
	{ printf("reset dpwrf=4095 and recalibrate C13 90 degree pulse");
	  psg_abort(1); }

    /* maximum fine power for pwC pulses */
	rf0 = 4095.0;

   /* dipsi-3 decoupling on CbCa */	
 	p_d = (5.0)/(9.0*4.0*spinlock); /* DIPSI-3*/
 	rfd = (compC*4095.0*pwC*5.0)/(p_d*9.0);
	rfd = (int) (rfd + 0.5);
  	ncyc = (int) (ncyc + 0.5);


   /* power level and pulse time for WALTZ 1H decoupling */
        pwHd = 1/(4.0 * waltzB1) ;    
        tpwrd = tpwr - 20.0*log10(pwHd/(pw));
        tpwrd = (int) (tpwrd + 0.5);

/* activate auto-calibration flags */
setautocal();
  if (autocal[0] == 'n')
  {
    codmf= getval("codmf");
    pwco = 1.0/codmf; /* pw for 13C' decoupling field */
    copwr = getval("copwr"); /* power level for 13C' decoupling */
    cores = getval("cores"); /* power level for 13C' decoupling */
  }
  else        /* if autocal = 'y'(yes), 'q'(quiet), r(read), or 's'(semi) */
  {
    strcpy(codecseq,"Pdec_154p");
    if(FIRST_FID)                                            /* call Pbox */
    {
      ppm = getval("dfrq");
      bw=20.0*ppm; ofs=154*ppm;
      Pdec_154p = pbox_Dsh("Pdec_154p", "WURST2", bw, ofs, compC*pwC, pwClvl);
      bw=30*ppm; ofs=0.0*ppm; nst = 1000; pws = 0.001;
      me180 = pbox_makeA("me180", "sech", bw, pws, ofs, compC*pwC, pwClvl, nst);
    }

    copwr = Pdec_154p.pwr; pwco = 1.0/Pdec_154p.dmf;
    cores = Pdec_154p.dres;
    pwme180 = me180.pw; me180pwr= me180.pwr; me180pwrf = me180.pwrf;

  }
/* CHECK VALIDITY OF PARAMETER RANGES */

    if( gt1 > 0.5*del - 1.0e-4)
    {
        printf(" gt1 is too big. Make gt1 less than %f.\n", (0.5*del - 1.0e-4));
        psg_abort(1);
    }

    if( dm[A] == 'y' )
    {
        printf("incorrect dec1 decoupler flag! Should be 'nny' or 'nnn' ");
        psg_abort(1);
    }

    if((dm2[A] == 'y' || dm2[C] == 'y'))
    {
        printf("incorrect dec2 decoupler flags! Should be 'nnn' ");
        psg_abort(1);
    }
    if((dm3[A] == 'y' || dm3[C] == 'y'))
    {
        printf("incorrect dec3 decoupler flags! Should be 'nnn' or 'nyn' ");
        psg_abort(1);
    }

    if( dpwr > 52 )
    {
        printf("don't fry the probe, DPWR too large!  ");
        psg_abort(1);
    }

    if( pw > 50.0e-6 )
    {
        printf("dont fry the probe, pw too high ! ");
        psg_abort(1);
    } 
  
    if( pwN > 100.0e-6 )
    {
        printf("dont fry the probe, pwN too high ! ");
        psg_abort(1);
    } 
 

/* PHASES AND INCREMENTED TIMES */

/*  Phase incrementation for hypercomplex 2D data, States-Haberkorn element */

    icosel1 = 1; icosel2 = 1;
    if (phase1 == 2) 
	{ tsadd(t2,2,4); icosel1 = -1;}
    if (phase2 == 2) 
	{ tsadd(t4,2,4); icosel2 = -1; tsadd(t2,2,4);}

/*  Set up f1180  */
   
    tau1 = d2;
    if((f1180[A] == 'y') && (ni > 1.0)) 
	{ tau1 += ( 1.0 / (2.0*sw1) ); if(tau1 < 0.2e-6) tau1 = 0.0; }
    tau1 = tau1/2.0;


/*  Set up f2180  */

    tau2 = d3;
    if((f2180[A] == 'y') && (ni2 > 1.0)) 
	{ tau2 += ( 1.0 / (2.0*sw2) ); if(tau2 < 0.2e-6) tau2 = 0.0; }
    tau2 = tau2/2.0;


/* Calculate modifications to phases for States-TPPI acquisition  */

   if( ix == 1) d2_init = d2;
   t1_counter = (int) ( (d2-d2_init)*sw1 + 0.5 );
   if(t1_counter % 2) 
	{ tsadd(t1,2,4); tsadd(t11,2,4); }

   
   if(ni > 1)
           kappa = (double)(t1_counter*(del2)) / ( (double) (ni-1) );
      else kappa = 0.0;   

/*   BEGIN PULSE SEQUENCE   */

status(A);

        decoffset(dof-140*dfrq);
	obspower(tpwr);
	decpower(pwClvl);
 	dec2power(pwNlvl);
	decpwrf(rf0);
	obsoffset(tof);
	txphase(zero);
	delay(1.0e-5);

  if (satmode[A] == 'y')
    {
      obspower(satpwr);
      txphase(zero);
      rgpulse(d1,zero,20.0e-6,20.0e-6);
      obspower(tpwr);            /* Set power for hard pulses  */
    }
  else  
    {
      obspower(tpwr); /* Set power for hard pulses  */ 
      delay(d1);
    }

	decrgpulse(pwC, zero, 0.0, 0.0);	   /*destroy C13 magnetization*/
	zgradpulse(gzlvl1, 0.5e-3);
	delay(gstab);
	decrgpulse(pwC, one, 0.0, 0.0);
	zgradpulse(0.7*gzlvl1, 0.5e-3);
	delay(1.1*gstab);

   if(dm3[B] == 'y')				  /*optional 2H decoupling on */
        { 
          dec3unblank();
          dec3rgpulse(1/dmf3, one, 0.0, 0.0); 
          dec3unblank();
          setstatus(DEC3ch, TRUE, 'w', FALSE, dmf3);
         } 
	rgpulse(pw, zero, 0.0, 0.0);                    /* 1H pulse excitation */

	zgradpulse(gzlvl3, gt3);
        decphase(zero);
	delay(0.5*del - gt3);

	simpulse(2.0*pw, 2.0*pwC, zero, zero, 0.0, 0.0);

	zgradpulse(gzlvl3, gt3);
        txphase(one);
        decphase(t1);
	delay(0.5*del - gt3);

        rgpulse(pw,one,0.0,0.0);
        zgradpulse(1.8*gzlvl3, gt3);
        txphase(zero);
        delay(150e-6);
	decrgpulse(pwC, t1, 0.0, 0.0);
        
      /* decoupling on for carbonyl carbon */
         decpwrf(4095.0);
         decpower(copwr);
         decprgon(codecseq,pwco,cores);
         decon();
      /* decoupling on for carbonyl carbon */

        delay(tau1);

        dec2rgpulse(2.0*pwN, zero, 0.0, 0.0);
 
        zgradpulse(icosel1*gzlvl4, gt1);

	delay(0.5*del2 - 2.0*pwN - gt1 - 2.0*pw);

        rgpulse(2.0*pw,zero,0.0,0.0);

        delay(tau1 - (kappa*tau1));

      /* co-decoupling off */
         decoff();
         decprgoff();
      /* co-decoupling off */
         decpower(pwClvl);

	decrgpulse(2.0*pwC, zero, 0.0, 0.0);

      /* decoupling on for carbonyl carbon */
         decpwrf(4095.0);
         decpower(copwr);
         decprgon(codecseq,pwco,cores);
         decon();
      /* decoupling on for carbonyl carbon */

	delay(0.5*del2 - kappa*tau1);

      /* co-decoupling off */
         decoff();
         decprgoff();
      /* co-decoupling off */
         decpower(pwClvl);

        decphase(t2);

	decrgpulse(pwC, t2, 0.0, 0.0);

	decpwrf(rfd);
	delay(2.0e-6);
	initval(ncyc, v2);
	starthardloop(v2);
     decrgpulse(4.9*p_d,one,0.0,0.0);
     decrgpulse(7.9*p_d,three,0.0,0.0);
     decrgpulse(5.0*p_d,one,0.0,0.0);
     decrgpulse(5.5*p_d,three,0.0,0.0);
     decrgpulse(0.6*p_d,one,0.0,0.0);
     decrgpulse(4.6*p_d,three,0.0,0.0);
     decrgpulse(7.2*p_d,one,0.0,0.0);
     decrgpulse(4.9*p_d,three,0.0,0.0);
     decrgpulse(7.4*p_d,one,0.0,0.0);
     decrgpulse(6.8*p_d,three,0.0,0.0);
     decrgpulse(7.0*p_d,one,0.0,0.0);
     decrgpulse(5.2*p_d,three,0.0,0.0);
     decrgpulse(5.4*p_d,one,0.0,0.0);
     decrgpulse(0.6*p_d,three,0.0,0.0);
     decrgpulse(4.5*p_d,one,0.0,0.0);
     decrgpulse(7.3*p_d,three,0.0,0.0);
     decrgpulse(5.1*p_d,one,0.0,0.0);
     decrgpulse(7.9*p_d,three,0.0,0.0);

     decrgpulse(4.9*p_d,three,0.0,0.0);
     decrgpulse(7.9*p_d,one,0.0,0.0);
     decrgpulse(5.0*p_d,three,0.0,0.0);
     decrgpulse(5.5*p_d,one,0.0,0.0);
     decrgpulse(0.6*p_d,three,0.0,0.0);
     decrgpulse(4.6*p_d,one,0.0,0.0);
     decrgpulse(7.2*p_d,three,0.0,0.0);
     decrgpulse(4.9*p_d,one,0.0,0.0);
     decrgpulse(7.4*p_d,three,0.0,0.0);
     decrgpulse(6.8*p_d,one,0.0,0.0);
     decrgpulse(7.0*p_d,three,0.0,0.0);
     decrgpulse(5.2*p_d,one,0.0,0.0);
     decrgpulse(5.4*p_d,three,0.0,0.0);
     decrgpulse(0.6*p_d,one,0.0,0.0);
     decrgpulse(4.5*p_d,three,0.0,0.0);
     decrgpulse(7.3*p_d,one,0.0,0.0);
     decrgpulse(5.1*p_d,three,0.0,0.0);
     decrgpulse(7.9*p_d,one,0.0,0.0);

     decrgpulse(4.9*p_d,three,0.0,0.0);
     decrgpulse(7.9*p_d,one,0.0,0.0);
     decrgpulse(5.0*p_d,three,0.0,0.0);
     decrgpulse(5.5*p_d,one,0.0,0.0);
     decrgpulse(0.6*p_d,three,0.0,0.0);
     decrgpulse(4.6*p_d,one,0.0,0.0);
     decrgpulse(7.2*p_d,three,0.0,0.0);
     decrgpulse(4.9*p_d,one,0.0,0.0);
     decrgpulse(7.4*p_d,three,0.0,0.0);
     decrgpulse(6.8*p_d,one,0.0,0.0);
     decrgpulse(7.0*p_d,three,0.0,0.0);
     decrgpulse(5.2*p_d,one,0.0,0.0);
     decrgpulse(5.4*p_d,three,0.0,0.0);
     decrgpulse(0.6*p_d,one,0.0,0.0);
     decrgpulse(4.5*p_d,three,0.0,0.0);
     decrgpulse(7.3*p_d,one,0.0,0.0);
     decrgpulse(5.1*p_d,three,0.0,0.0);
     decrgpulse(7.9*p_d,one,0.0,0.0);

     decrgpulse(4.9*p_d,one,0.0,0.0);
     decrgpulse(7.9*p_d,three,0.0,0.0);
     decrgpulse(5.0*p_d,one,0.0,0.0);
     decrgpulse(5.5*p_d,three,0.0,0.0);
     decrgpulse(0.6*p_d,one,0.0,0.0);
     decrgpulse(4.6*p_d,three,0.0,0.0);
     decrgpulse(7.2*p_d,one,0.0,0.0);
     decrgpulse(4.9*p_d,three,0.0,0.0);
     decrgpulse(7.4*p_d,one,0.0,0.0);
     decrgpulse(6.8*p_d,three,0.0,0.0);
     decrgpulse(7.0*p_d,one,0.0,0.0);
     decrgpulse(5.2*p_d,three,0.0,0.0);
     decrgpulse(5.4*p_d,one,0.0,0.0);
     decrgpulse(0.6*p_d,three,0.0,0.0);
     decrgpulse(4.5*p_d,one,0.0,0.0);
     decrgpulse(7.3*p_d,three,0.0,0.0);
     decrgpulse(5.1*p_d,one,0.0,0.0);
     decrgpulse(7.9*p_d,three,0.0,0.0);
	endhardloop();

        txphase(one);
	decpwrf(rf0);
        decphase(t3);
        obspower(tpwrd);
        decrgpulse(pwC,t3,0.0,0.0);
        decoffset(dof - 155*dfrq);
        rgpulse(pwHd,one,0.0,2.0e-6);
        txphase(zero);
        obsunblank();
        obsprgon("waltz16", pwHd, 90.0);              /* PRG_START_DELAY */
        xmtron();

	delay(TC - OFFSET_DELAY - POWER_DELAY - PRG_START_DELAY - tau2);

	decrgpulse(2.0*pwC, zero, 0.0, 0.0);

        delay(TC + tau2 - POWER_DELAY - PRG_STOP_DELAY - 2*gt1 - gstab - 2.0*pw);

        xmtroff();
        obsprgoff();
        obsblank();
        rgpulse(pwHd,three,2.0e-6,0.0);
        obspower(tpwr);

    if (mag_flg[A] =='y')
        magradpulse(gzcal*icosel2*gzlvl2, gt1);
    else
        zgradpulse(icosel2*gzlvl2, gt1);
        delay(gstab/2.0);
        rgpulse(2.0*pw,zero,0.0,0.0);
    if (mag_flg[A] =='y')
        magradpulse(gzcal*icosel2*gzlvl2, gt1);
    else
        zgradpulse(icosel2*gzlvl2, gt1);
        delay(gstab/2.0);

        decphase(zero);
        simpulse(0.0,pwC, two, zero, 0.0, 0.0);

        zgradpulse(gzlvl5, gt5);
        delay(0.5*del1 - gt5);

        simpulse(2.0*pw, 2.0*pwC, zero, zero, 0.0, 0.0);

        zgradpulse(gzlvl5, gt5);
        txphase(one);
        decphase(t4);
        delay(0.5*del1 - gt5);

	simpulse(pw, pwC, one, t4, 0.0, 0.0);

	zgradpulse(gzlvl6, gt5);
	txphase(zero);
	decphase(zero);
	delay(0.5*del4 - gt5);

	simpulse(2.0*pw, 2.0*pwC, zero, zero, 0.0, 0.0);

	zgradpulse(gzlvl6, gt5);
	delay(0.5*del4 - gt5);

	simpulse(pw,pwC,zero,zero,0.0,0.0);
        zgradpulse(2.3*gzlvl6, gt1);

   if (autocal[A] == 'y')
       {
        decpower(me180pwr); decpwrf(me180pwrf);
	delay(0.5*del3 - gt1 - 0.0005 -2.0*POWER_DELAY- WFG2_START_DELAY);
	simshaped_pulse("","me180",2.0*pw,0.001, zero, zero, 0.0, 0.0);
        decpwrf(rf0);
        decphase(zero);

       }
   else
       {
	delay(0.5*del3 - 0.5*pwC - gt1);
	simpulse(2.0*pw,2.0*pwC, zero, zero, 0.0, 0.0);
       }


   decpower(dpwr);
        if (mag_flg[A] == 'y')
            magradpulse(gzcal*((2.3*gzlvl6)+gzlvl1), gt1);
        else
            zgradpulse(((2.3*gzlvl6)+gzlvl1), gt1);

   if (autocal[A] == 'y')
   {
     if(dm3[B] == 'y')
       delay(0.5*del3 - 0.0005 -gt1 -1/dmf3 - 2.0*GRADIENT_DELAY - 2.0*POWER_DELAY);
        else
       delay(0.5*del3 -  0.0005 -gt1 - 2.0*GRADIENT_DELAY - 2.0*POWER_DELAY);
   }
   else
   {
     if(dm3[B] == 'y') 
      delay(0.5*del3  - gt1 -1/dmf3 - 2.0*GRADIENT_DELAY - POWER_DELAY);
         else
      delay(0.5*del3  - gt1 - 2.0*GRADIENT_DELAY - POWER_DELAY);
   }

   if(dm3[B] == 'y')			         /*optional 2H decoupling off */
        {
          dec3rgpulse(1/dmf3, three, 0.0, 0.0); 
          setstatus(DEC3ch, FALSE, 'w', FALSE, dmf3);
          dec3blank();
        }
 if (dm3[B]=='y') lk_sample();
status(C); 
 setreceiver(t11);
}
Example #2
0
pulsesequence() {

// Define Variables and Objects and Get Parameter Values

   double aXxyxy8 = getval("aXxyxy8");
   double aYxyxy8 = getval("aYxyxy8");
   double pwXxyxy8 = getval("pwXxyxy8");
   double pwYxyxy8 = getval("pwYxyxy8");
   double nXYxy8 = getval("nXYxy8");
   int counter = nXYxy8;
   initval(nXYxy8,v8);
   double fXYxy8 = getval("fXYxy8");
   double onYxyxy8 = getval("onYxyxy8");
   double srate = getval("srate");

   DSEQ dec = getdseq("H");
   strncpy(dec.t.ch,"dec",3);
   putCmd("chHtppm='dec'\n"); 
   strncpy(dec.s.ch,"dec",3);
   putCmd("chHspinal='dec'\n");

   DSEQ mix = getdseq("Hmix");
   strncpy(mix.t.ch,"dec",3);
   putCmd("chHmixtppm='dec'\n");
   strncpy(dec.s.ch,"dec",3);
   putCmd("chHmixspinal='dec'\n");

//--------------------------------------
// Copy Current Parameters to Processed
//-------------------------------------

   putCmd("groupcopy('current','processed','acquisition')");

// Dutycycle Protection

   DUTY d = init_dutycycle();
   d.dutyon = getval("pwX90") + nXYxy8*(pwXxyxy8 + pwYxyxy8);
   d.dutyoff = d1 + 4.0e-6;
   d.c1 = d.c1 + (!strcmp(dec.seq,"tppm"));
   d.c1 = d.c1 + ((!strcmp(dec.seq,"tppm")) && (dec.t.a > 0.0));
   d.t1 = getval("rd") + getval("ad") + at;
   d.c2 = d.c2 + (!strcmp(dec.seq,"spinal"));
   d.c2 = d.c2 + ((!strcmp(dec.seq,"spinal")) && (dec.s.a > 0.0));
   d.t2 = getval("rd") + getval("ad") + at;
   d.c3 = d.c3 + (!strcmp(mix.seq,"tppm"));
   d.c3 = d.c3 + ((!strcmp(mix.seq,"tppm")) && (mix.t.a > 0.0));
   d.t3 = nXYxy8*(1.0/srate - pwXxyxy8 - pwYxyxy8);
   d.c4 = d.c4 + (!strcmp(mix.seq,"spinal"));
   d.c4 = d.c4 + ((!strcmp(mix.seq,"spinal")) && (mix.s.a > 0.0));
   d.t4 = nXYxy8*(1.0/srate - pwXxyxy8 - pwYxyxy8);
   d = update_dutycycle(d);
   abort_dutycycle(d,10.0);

// Set Phase Tables

   settable(phX90,4,table1);
   settable(phXYxy8,8,table2);
   settable(phXxyxy8,4,table3);
   settable(phYxyxy8,4,table4);
   settable(phRec,4,table5);
   settable(ph1Rec,4,table6);
   settable(ph2Rec,4,table7);
   settable(ph3Rec,4,table8);
   int tix = counter%8;

   if ((tix == 1) || (tix == 7)) ttadd(phRec,ph1Rec,4);
   if ((tix == 2) || (tix == 6)) ttadd(phRec,ph2Rec,4);
   if ((tix == 3) || (tix == 5)) ttadd(phRec,ph3Rec,4);
   setreceiver(phRec);

// Begin Sequence

   txphase(phX90); decphase(zero);
   obspwrf(getval("aX90"));
   obsunblank(); decunblank(); _unblank34();
   delay(d1);
   sp1on(); delay(2.0e-6); sp1off(); delay(2.0e-6);

// X Direct Polarization

   rgpulse(getval("pwX90"),phX90,0.0,0.0);

// xy8XY Period

   if (counter > 0) {
      _dseqon(mix);
      delay(pwXxyxy8/2.0);
      obspwrf(aXxyxy8); dec2pwrf(aYxyxy8);
      sub(v1,v1,v1);
      if (counter >= 1) {
         loop(v8,v9);
	    getelem(phXYxy8,v1,v4);
	    incr(v1);
	    getelem(phXxyxy8,ct,v2);
	    getelem(phYxyxy8,ct,v3);
	    add(v4,v2,v2);
	    add(v4,v3,v3);
	    txphase(v2); dec2phase(v3);
	    delay((1.0 - fXYxy8)/srate - pwYxyxy8/2.0 - pwXxyxy8/2.0);
	    if (onYxyxy8 == 2)
               dec2rgpulse(pwYxyxy8,v3,0.0,0.0);
            else
               delay(pwYxyxy8);
	    delay(fXYxy8/srate - pwYxyxy8/2.0 - pwXxyxy8/2.0);
	    rgpulse(pwXxyxy8,v2,0.0,0.0);
	 endloop(v9);
	 delay(1.0/srate - pwXxyxy8/2.0);
      }
      _dseqoff(mix);
   }

// Begin Acquisition

   _dseqon(dec);
   obsblank(); _blank34();
   delay(getval("rd"));
   startacq(getval("ad"));
   acquire(np, 1/sw);
   endacq();
   _dseqoff(dec);
   obsunblank(); decunblank(); _unblank34();
}
Example #3
0
pulsesequence()
{
   double          slpwrR = getval("slpwrR"),
                   slpwR = getval("slpwR"),
                   mixR = getval("mixR"),
                   gzlvlz = getval("gzlvlz"),
                   gtz = getval("gtz"),
		   zfphinc = getval("zfphinc");
   char		   slpatR[MAXSTR];
   int		   phase1 = (int)(getval("phase")+0.5);

/* LOAD AND INITIALIZE PARAMETERS */
   getstr("slpatR",slpatR);

   if (strcmp(slpatR,"cw") &&
        strcmp(slpatR,"troesy") &&
        strcmp(slpatR,"dante"))
        abort_message("SpinLock pattern %s not supported!.\n", slpatR);


   sub(ct,ssctr,v7);

   settable(t1,4,ph1);	getelem(t1,v7,v1);
   settable(t2,8,ph2);	getelem(t2,v7,v2);
   settable(t3,8,ph3);	
   settable(t8,4,ph8);	getelem(t8,v7,v8);
   settable(t6,8,ph6);	getelem(t6,v7,v6);
  
   assign(v1,oph); 
   if (getflag("zfilt"))
	getelem(t3,v7,oph);

   add(v2,one,v3);
   add(v2,two,v4);
   add(v2,three,v5);

   if (phase1 == 2)
      {incr(v1); incr(v6);}			/* hypercomplex method */
/*
   mod2(id2,v13);
   dbl(v13,v13);
*/
  initval(2.0*(double)(((int)(d2*getval("sw1")+0.5)%2)),v13);

       add(v1,v13,v1);
       add(v6,v13,v6);
       add(oph,v13,oph);

/* The following is for flipback pulse */
   zfphinc=zfphinc+180;
   if (zfphinc < 0) zfphinc=zfphinc+360;
   initval(zfphinc,v10);

/* BEGIN ACTUAL PULSE SEQUENCE */
   status(A);
      obspower(tpwr);

   delay(5.0e-5);
   if (getflag("sspul"))
        steadystate();

   if (satmode[0] == 'y')
     {
        if ((d1-satdly) > 0.02)
                delay(d1-satdly);
        else
                delay(0.02);
        satpulse(satdly,v6,rof1,rof1);
     }
   else
        delay(d1);

   if (getflag("wet"))
     wet4(zero,one);
   decpower(dpwr);

   status(B);
      rgpulse(pw, v1, rof1, rof1);
      if (d2 > 0.0)
       delay(d2 - POWER_DELAY - (2*pw/PI) - rof1);
      else
       delay(d2);
      
      obspower(slpwrR);

      if (mixR > 0.0)
      {
        if (dps_flag)
	  {
	     if (!strcmp(slpatR,"troesy"))
          	rgpulse(mixR,v2,0.0,0.0);
	     else
		rgpulse(mixR,v3,0.0,0.0);
	  }
        else
          SpinLock(slpatR,mixR,slpwR,v2,v3,v4,v5, v9);
      }

       if ((getflag("zfilt")) && (getflag("PFGflg")))
        {
           obspower(tpwr);
           rgpulse(pw,v2,1.0e-6,rof1);
           zgradpulse(gzlvlz,gtz);
           delay(gtz/3);
           if (getflag("flipback"))
                FBpulse(v8,v10);
           rgpulse(pw,v8,rof1,rof2);
        }
       else
           delay(rof2);

   status(C);
}
Example #4
0
pulsesequence()
{
        double gzlvl1,qlvl,grise,gstab,gt1,ss,phase;
	int icosel,iphase;
  	ss = getval("ss");
        grise=getval("grise");
        gstab=getval("gstab"); 
        gt1=getval("gt1");
        gzlvl1=getval("gzlvl1");
        qlvl=getval("qlvl");
        phase=getval("phase");
        iphase = (int) (phase + 0.5);



/* DETERMINE STEADY-STATE MODE */
   if (ss < 0) ss = (-1) * ss;
   else
      if ((ss > 0) && (ix == 1)) ss = ss;
      else
         ss = 0;
   initval(ss, ssctr);
   initval(ss, ssval);

   assign(oph,v2);
   assign(oph,v1);
   if (iphase == 2)
      incr(v1);

/* HYPERCOMPLEX MODE */
   initval(2.0*(double)(((int)(d2*getval("sw1")+0.5)%2)),v6);
   if ((iphase==1) || (iphase==2))
      {add(v1,v6,v1); add(oph,v6,oph);} 
	

     status(A);
        rcvroff();
	delay(d1);
     if (getflag("wet")) wet4(zero,one);
	rlpower(tpwr,TODEV);

	rgpulse(pw,v1,rof1,rof2);
     status(B);
        if (d2 > rof1 + 4.0*pw/3.1416)
           delay(d2 - rof1 - 4.0*pw/3.1416);
     status(C);
        rgpulse(pw,v2,rof1,rof2);
      
        delay(gt1+2.0*grise+24.4e-6);
        rgpulse(2.0*pw,v2,rof1,rof2);
        icosel=-1;
        rgradient('z',gzlvl1*(double)icosel);
	delay(gt1+grise);
	rgradient('z',0.0);
        txphase(oph);
	delay(grise);

	rgpulse(pw,v2,rof1,rof2);

        rgradient('z',gzlvl1*qlvl);

	delay(gt1+grise);
	rgradient('z',0.0);
	delay(grise);
       rcvron();
	delay(gstab);  
     status(D);
}
Example #5
0
pulsesequence()
{
  char rcvrsflag[MAXSTR],
       mrmode[MAXSTR];

  double compH, Hdpwr, pw90,
         pwx = getval("pwx"),
         pwxlvl = getval("pwxlvl");
	  
  getstr("rcvrs",rcvrsflag);
  getstr("mrmode",mrmode);
  Hdpwr = 0.0; compH = 1.0;   /* initialize the parameters */

  if (strcmp(rcvrsflag,"yy"))
    printf("rcvrs parameter should be set to 'yy'\n");

  /* check decoupling modes */

  if ((dm[A] == 'y') || (dm[B] == 'y') || (dm[C] == 'y') || (dm[D] == 'y') || (h**o[0] == 'y'))
  {
    printf("dm should be set to 'nnnn' and h**o should set to 'n'");
    psg_abort(1);
  }
  
  if(mrmode[A] == 'd')  /* make the decoupling waveform */
  {
    Hdpwr = getval("Hdpwr");
    compH = getval("compH");
    pw90  = getval("pw90");
    if(FIRST_FID) 
      H1dec = pbox_mix("pansyW16", "WALTZ16", Hdpwr, pw90*compH, tpwr);
  }
  else if(mrmode[A] != 's') 
    mrmode[A] = 'p';           /* default is 'p' */

  
  status(A);
  
  delay(1.0e-4);
  decpower(pwxlvl);
  obspower(tpwr);    
  delay(d1);
  
  status(B);

  if(mrmode[A] != 'p')   /* sequential acquisition */
  {    
    rgpulse(pw, oph, rof1, rof2);
     
    setactivercvrs("yn");
    startacq(alfa);
    acquire(np,1.0/sw);
    endacq();             
    delay(1.0e-6);

    if(mrmode[A] == 'd')
    {
      obsunblank();
      pbox_xmtron(&H1dec);
    }   
      delay(d2);    
      decrgpulse(pwx, oph, rof1, rof2);

      status(C);
      
      setactivercvrs("ny");
      startacq(alfa);
      acquire(np,1.0/sw);
      endacq();
      
    if(mrmode[A] == 'd')
    {
      pbox_xmtroff();    
      obsblank();
    }
  }
  else 
  {    
    delay(d2);
    simpulse(pw, pwx, oph, oph, rof1, rof2);
 
    status(C);
  }
}
Example #6
0
pulsesequence()
{
   char            sspul[MAXSTR];

   double         pwClvl=getval("pwClvl");
/* LOAD VARIABLES AND CHECK CONDITIONS */
   getstr("sspul", sspul);

/* STEADY-STATE PHASECYCLING */
/* This section determines if the phase calculations trigger off of (SS - SSCTR)
   or off of CT */

   ifzero(ssctr);
      hlv(ct, v4);
      mod4(ct, v3);
   elsenz(ssctr);
      sub(ssval, ssctr, v12);	/* v12 = 0,...,ss-1 */
      hlv(v12, v4);
      mod4(v12, v3);
   endif(ssctr);


/* CALCULATE PHASECYCLE */
/* The phasecycle first performs a 4-step cycle on the third pulse in order
   to select for DQC.  Second, the 2-step QIS cycle is added in.  Third, a
   2-step cycle for axial peak suppression is performed on the second pulse.
   Fourth, a 2-step cycle for axial peak suppression is performed on the
   first pulse.  If P-type peaks only are being selected, the 2-step cycle
   for P-type peak selection is performed on the first pulse immediately
   after the 4-step cycle on the third pulse. */

   hlv(v4, v4);
   if (phase1 == 0)
   {
      assign(v4, v6);
      hlv(v4, v4);
      mod2(v6, v6);		/* v6 = P-type peak selection in w1 */
   }
   hlv(v4, v2);
   mod4(v4, v4);		/* v4 = quadrature image suppression */
   hlv(v2, v1);
   mod2(v1, v1);
   dbl(v1, v1);
   mod2(v2, v2);
   dbl(v2, v2);
   dbl(v3, v5);
   add(v3, v5, v5);
   add(v1, v5, v5);
   add(v2, v5, v5);
   add(v4, v5, v5);
   add(v4, v1, v1);
   add(v4, v2, v2);
   add(v4, v3, v3);
   if (phase1 == 0)
   {
      add(v6, v1, v1);
      add(v6, v5, v5);
   }
   if (phase1 == 2)
      incr(v1);
   if (phase1 == 3)
      add(id2, v1, v1);		/* adds TPPI increment to the phase of the
				 * first pulse */
   assign(v5, oph);

  /* FOR HYPERCOMPLEX, USE STATES-TPPI TO MOVE AXIALS TO EDGE */  
   if ((phase1==2)||(phase1==1))
   {
      initval(2.0*(double)(d2_index%2),v9);  /* moves axials */
      add(v1,v9,v1); add(oph,v9,oph);
   }

/* BEGIN ACTUAL PULSE SEQUENCE CODE */
   status(A);
   if (sspul[0] == 'y')
   {
      obspower(pwClvl-12);
      rgpulse(200*pw, one, 10.0e-6, 0.0e-6);
      rgpulse(200*pw, zero, 0.0e-6, 1.0e-6);
      obspower(pwClvl);
   }
   delay(d1);
   status(B);
   rgpulse(pw, v1, rof1, 1.0e-6);
   if (d2>0.0)
      delay(d2 - rof1 - 1.0e-6 -(4*pw)/3.1416);
   rgpulse(pw, v2, rof1, 0.0);
   rgpulse(pw, v3, 1.0e-6, rof2);
   add(v3,one,v8);
   delay(d3);
   rgpulse(2.0*pw,v8,rof1,rof1);
   delay(d3);
   status(C);
}
Example #7
0
pulsesequence()
{
/* DECLARE VARIABLES */

 char       autocal[MAXSTR],  /* auto-calibration flag */
            fsat[MAXSTR],
	    fscuba[MAXSTR],
            f1180[MAXSTR],    /* Flag to start t1 @ halfdwell             */
            f2180[MAXSTR],    /* Flag to start t2 @ halfdwell             */
            spco180a[MAXSTR],
            spco90b[MAXSTR],
            spco180b[MAXSTR],
            cadecseq[MAXSTR];


 int         phase, phase2, ni, ni2, icosel,  /* used to get n and p type */
             t1_counter,   /* used for states tppi in t1           */ 
             t2_counter;   /* used for states tppi in t2           */ 

 double      tau1,         /*  t1 delay */
             tau2,         /*  t2 delay */
             taua,         /*  ~ 1/4JCH =  1.7 ms */
             tauc,         /* ~ 1/4JCAC' = 3.6 ms  */
             taud,         /* ~ 1/4JC'CA = 4.3, 4.4 ms */
             taue,         /* 1/4JC'N = 12.4 ms    */
             tauf,         /* 1/4JNH = 2.25 ms */
             BigTC,        /* carbon constant time period */
             BigTN,        /* nitrogen constant time period */
             pwn,          /* PW90 for 15N pulse              */
             pwca90a,      /* PW90 for 13C at dvhpwr    */
             pwca180a,     /* PW180 for 13C at dvhpwra  */
             pwco180a,
             pwca180b,      /* PW180 for ca nucleus @ dvhpwrb         */
             pwco180b,
             pwco90b,      /* PW90 for co nucleus @ dhpwrb         */
             tsatpwr,      /* low level 1H trans.power for presat  */
             tpwrml,       /* power level for h decoupling  */
             pwmlev,       /* h 90 pulse at tpwrml            */
             dhpwr,        /* power level for 13C pulses on dec1  
                              90 for part a of the sequence at 43 ppm */
             dvhpwra,        /* power level for 180 13C pulses at 43 ppm */
             dhpwrb,        /* power level for 13C pulses on dec1 - 54 ppm
                               90  for part b of the sequence*/
             dvhpwrb,        /* power level for 13C pulses on dec1 - 54 ppm
                               180 for part b of the sequence     */
             dhpwr2,       /* high dec2 pwr for 15N hard pulses    */
             sw1,          /* sweep width in f1                    */             
             sw2,          /* sweep width in f2                    */             
             dofcacb,      /* dof for dipsi part, 43  ppm            */      
             pwcadec,     /* seduce ca decoupling at dpwrsed        */
             dpwrsed,     /* power level for seduce ca decoupling   */
             dressed,     /* resoln for seduce decoupling  = 2      */
             dhpwrcoa,    /* power level for pwco180a, 180 shaped C'  */
             sphase1,     /* phase shift for off resonance C' 180  */
             pwN, pwNlvl,      /* N-15 RF calibration parameters */
             pwC, compC, pwClvl,      /* C-13 RF calibration parameters */
             compH,waltzB1,
             BigT1,     
             gt1,
             gt2,
             gt4,
             gt5,
             gt6,
             gt7,
             gt9,
             gt10,
             gstab,
             gzlvl1,
             gzlvl2,
             gzlvl4,
             gzlvl5,
             gzlvl6,
             gzlvl7,
             gzlvl9,
             gzlvl10;
           


/*  variables commented out are already defined by the system      */


/* LOAD VARIABLES */


  getstr("autocal",autocal);
  getstr("fsat",fsat);
  getstr("f1180",f1180);
  getstr("f2180",f2180);
  getstr("fscuba",fscuba);

  taua   = getval("taua"); 
  tauc   = getval("tauc"); 
  taud   = getval("taud");
  taue   = getval("taue");
  tauf   = getval("tauf");
  BigTC  = getval("BigTC");
  BigTN  = getval("BigTN");
  pwN = getval("pwN");
  pwNlvl = getval("pwNlvl");
  pwn = getval("pwn");
  tpwr = getval("tpwr");
  tsatpwr = getval("tsatpwr");
  tpwrml  = getval("tpwrml");
  dpwr = getval("dpwr");
  dhpwr2 = getval("dhpwr2");
  phase = (int) ( getval("phase") + 0.5);
  phase2 = (int) ( getval("phase2") + 0.5);
  sw1 = getval("sw1");
  sw2 = getval("sw2");
  dofcacb = getval("dofcacb");
  ni = getval("ni");
  ni2 = getval("ni2");
  BigT1 = getval("BigT1");
  sphase1 = getval("sphase1");
  gt1 = getval("gt1");
  gt2 = getval("gt2");
  gt4 = getval("gt4");
  gt5 = getval("gt5");
  gt6 = getval("gt6");
  gt7 = getval("gt7");
  gt9 = getval("gt9");
  gt10 = getval("gt10");
  gstab = getval("gstab");
  gzlvl1 = getval("gzlvl1");
  gzlvl2 = getval("gzlvl2");
  gzlvl4 = getval("gzlvl4");
  gzlvl5 = getval("gzlvl5");
  gzlvl6 = getval("gzlvl6");
  gzlvl7 = getval("gzlvl7");
  gzlvl9 = getval("gzlvl9");
  gzlvl10 = getval("gzlvl10");


  if(autocal[0]=='n')
  {
    getstr("spco180a",spco180a);
    getstr("spco90b",spco90b);
    getstr("spco180b",spco180b);
    getstr("cadecseq",cadecseq);    
    pwca90a = getval("pwca90a");
    pwca180a = getval("pwca180a");
    pwco180a = getval("pwco180a");
    pwca180b = getval("pwca180b");
    pwco90b = getval("pwco90b");
    pwco180b = getval("pwco180b"); 
    dhpwr = getval("dhpwr");
    dvhpwra = getval("dvhpwra");
    dhpwrb = getval("dhpwrb");
    dvhpwrb = getval("dvhpwrb");    
    dhpwrcoa = getval("dhpwrcoa");
    dpwrsed = getval("dpwrsed"); 
    dressed = getval("dressed");
    pwcadec = getval("pwcadec");    
    pwmlev = getval("pwmlev");
  }
  else
  {
    waltzB1=getval("waltzB1");
    pwmlev=1/(4.0*waltzB1);
    compH = getval("compH");
    tpwrml= tpwr - 20.0*log10(pwmlev/(compH*pw));
    tpwrml= (int) (tpwrml + 0.5);
    strcpy(spco180a,"Psed180_133p");
    strcpy(spco90b,"Phard90co_118p");
    strcpy(spco180b,"Phard180co_118p");
    strcpy(cadecseq,"Pseduce1_lek");
    if (FIRST_FID)
    {
      pwN = getval("pwN");
      pwNlvl = getval("pwNlvl");
      pwC = getval("pwC");
      pwClvl = getval("pwClvl");
      compC = getval("compC");
      ca90 = pbox("cal", CA90, "", dfrq, compC*pwC, pwClvl);
      ca180 = pbox("cal", CA180, "", dfrq, compC*pwC, pwClvl);      
      co180 = pbox(spco180a, CO180, CO180ps, dfrq, compC*pwC, pwClvl);
      co90b = pbox(spco90b, CO90b, CA180ps, dfrq, compC*pwC, pwClvl);
      co180b = pbox(spco180b, CO180b, CA180ps, dfrq, compC*pwC, pwClvl);
      ca180b = pbox("cal", CA180b, "", dfrq, compC*pwC, pwClvl);          
      cadec = pbox(cadecseq, CADEC, CADECps, dfrq, compC*pwC, pwClvl);
      w16 = pbox_dec("cal", "WALTZ16", tpwrml, sfrq, compH*pw, tpwr);
    }
    pwca90a = ca90.pw;       dhpwr = ca90.pwr;    
    pwca180a = ca180.pw;     dvhpwra = ca180.pwr;
    pwco180a = co180.pw;     dhpwrcoa = co180.pwr;
    pwco90b = co90b.pw;      dhpwrb = co90b.pwr;
    pwco180b = co180b.pw;    
    pwca180b = ca180b.pw;    dvhpwrb = ca180b.pwr;    
    pwcadec = 1.0/cadec.dmf; dpwrsed = cadec.pwr; dressed = cadec.dres;
    pwmlev = 1.0/w16.dmf;
    pwn=pwN; dhpwr2=pwNlvl;
  }   



/* LOAD PHASE TABLE */

  settable(t1,1,phi1);
  settable(t2,1,phi2);
  settable(t3,4,phi3);
  settable(t4,1,phi4);
  settable(t5,2,phi5);
  settable(t6,2,phi6);
  settable(t7,1,phi7);
  settable(t8,1,phi8);
  settable(t9,8,phi9);
  settable(t10,8,rec);
  settable(t11,1,phi11);
  settable(t12,1,phi12);
  settable(t13,1,phi13);

/* CHECK VALIDITY OF PARAMETER RANGES */

    if( 0.5*ni*1/(sw1) > BigTC - gt10 )
    {
        printf(" ni is too big\n");
        psg_abort(1);
    }

    if( ni2*1/(sw2) > 2.0*BigTN )
    {
        printf(" ni2 is too big\n");
        psg_abort(1);
    }

    if((dm[A] == 'y' || dm[B] == 'y' || dm[C] == 'y'))
    {
        printf("incorrect dec1 decoupler flags!  ");
        psg_abort(1);
    }

    if((dm2[A] == 'y' || dm2[B] == 'y' ))
    {
        printf("incorrect dec2 decoupler flags! Should be 'nny' ");
        psg_abort(1);
    }

    if( pwmlev < 30.0e-6 ) 
    {
        printf("too much power during proton mlev sequence\n");
        psg_abort(1);
     }

    if( tpwrml > 53 )
     {
        printf("tpwrml is too high\n");
        psg_abort(1);
     }

    if( tsatpwr > 6 )
    {
        printf("TSATPWR too large !!!  ");
        psg_abort(1);
    }

    if( dpwr > 50 )
    {
        printf("don't fry the probe, DPWR too large!  ");
        psg_abort(1);
    }

    if( dpwr2 > 50 )
    {
        printf("don't fry the probe, DPWR2 too large!  ");
        psg_abort(1);
    }

    if( dhpwr > 62 )
    {
        printf("don't fry the probe, DHPWR too large!  ");
        psg_abort(1);
    }

    if( dhpwrb > 62 )
    {
        printf("don't fry the probe, DHPWRB too large!  ");
        psg_abort(1);
    }

    if( dvhpwrb > 62 )   /* pwr level for dipsi  */
    {
        printf("don't fry the probe, DVHPWRB too large!  ");
        psg_abort(1);
    }

    if( dhpwr2 > 62 )
    {
        printf("don't fry the probe, DHPWR2 too large!  ");
        psg_abort(1);
    }

    if( pw > 200.0e-6 )
    {
        printf("dont fry the probe, pw too high ! ");
        psg_abort(1);
    } 
    if( pwmlev > 200.0e-6 )
    {
        printf("dont fry the probe, pwmlev too high ! ");
        psg_abort(1);
    } 
    if( pwn > 200.0e-6 )
    {
        printf("dont fry the probe, pwn too high ! ");
        psg_abort(1);
    } 


    if( pwcadec > 500.0e-6 || pwcadec < 200.0e-6 )
    {
        printf("pwcadec outside reasonable limits: < 500e-6 > 200e-6 \n");
        psg_abort(1);
    }

    if( dpwrsed > 45 )
    {
        printf("dpwrsed is too high\n");
        psg_abort(1);
    }

    if( gt1 > 15e-3 || gt2 > 15e-3 || gt4 >=15e-3 || gt5 > 15e-3 || gt6 >= 15e-3 || gt7 >= 15e-3 || gt9 >= 15e-3 || gt10 >= 15e-3) 
    {
        printf("all gti values must be < 15e-3\n");
        psg_abort(1);
    }

    if(gt10 > 250.0e-6) {
        printf("gt10 must be 250e-6\n");
        psg_abort(1);
    }


/*  Phase incrementation for hypercomplex 2D data */

    if (phase == 2)
      tsadd(t3,1,4);  
    if (phase2 == 2) {
      tsadd(t11,2,4);   
      icosel = 1;
    }
    else icosel = -1; 

/*  Set up f1180  tau1 = t1               */
   
    tau1 = d2;
    if(f1180[A] == 'y') {
        tau1 += ( 1.0 / (2.0*sw1) );
        if(tau1 < 0.2e-6) tau1 = 0.0;
    }
        tau1 = tau1/2.0;

/*  Set up f2180  tau2 = t2               */

    tau2 = d3;
    if(f2180[A] == 'y') {
        tau2 += ( 1.0 / (2.0*sw2) ); 
        if(tau2 < 0.2e-6) tau2 = 0.0;
    }
        tau2 = tau2/2.0;

/* Calculate modifications to phases for States-TPPI acquisition          */

   if( ix == 1) d2_init = d2 ;
   t1_counter = (int) ( (d2-d2_init)*sw1 + 0.5 );
   if(t1_counter % 2) {
      tsadd(t3,2,4);     
      tsadd(t10,2,4);    
    }

   if( ix == 1) d3_init = d3 ;
   t2_counter = (int) ( (d3-d3_init)*sw2 + 0.5 );
   if(t2_counter % 2) {
      tsadd(t8,2,4);  
      tsadd(t10,2,4);    
    }

/* BEGIN ACTUAL PULSE SEQUENCE */


status(A);
   decoffset(dofcacb);       /* initially pulse at 43 ppm */
   decpower(dhpwr);        /* Set Dec1 power for hard 13C pulses         */
   dec2power(dhpwr2);      /* Set Dec2 power for 15N hard pulses         */

/* Presaturation Period */
   if (fsat[A] == 'y')
   {
        obspower(tsatpwr);      /* Set transmitter power for 1H presaturation */
	delay(2.0e-5);
        rgpulse(d1,zero,rof1,rof1);
   	obspower(tpwr);      /* Set transmitter power for hard 1H pulses */
	delay(2.0e-5);
	if(fscuba[A] == 'y')
	{
		delay(2.2e-2);
		rgpulse(pw,zero,2.0e-6,0.0);
		rgpulse(2*pw,one,2.0e-6,0.0);
		rgpulse(pw,zero,2.0e-6,0.0);
		delay(2.2e-2);
	}
   }
   else
   obspower(tpwr);           /* Set transmitter power for hard 1H pulses */
   delay(d1);
   txphase(zero);
   delay(1.0e-5);

/* Begin Pulses */

status(B);

   rcvroff();
   delay(20.0e-6);


/* ensure that magnetization originates on H and not 13C  */
   decrgpulse(pwca90a,zero,0.0,0.0);

   delay(0.2e-6);
   zgradpulse(gzlvl6,gt6);
   delay(gstab);

   rgpulse(pw,zero,0.0,0.0);                    /* 90 deg 1H pulse */
   decphase(t1);

   delay(0.2e-6);
   zgradpulse(gzlvl9,gt9);
   delay(2.0e-6);

   decpower(dvhpwra);
   delay(taua - POWER_DELAY - gt2 - 2.2e-6);   /* taua <= 1/4JCH */                          
   simpulse(2*pw,pwca180a,zero,t1,0.0,0.0);
   decpower(dhpwr);

   delay(0.2e-6);
   zgradpulse(gzlvl9,gt9);
   delay(2.0e-6);

   txphase(t2); decphase(t3);
   delay(taua - POWER_DELAY - gt2 - 2.2e-6); 

   rgpulse(pw,t2,0.0,0.0);

   decrgpulse(pwca90a,t3,2.0e-6,0.0);

   delay(2.0e-6);

     delay(tau1);

     decpower(dhpwrcoa);
     decshaped_pulse(spco180a,pwco180a,zero,4.0e-6,0.0);

     dec2rgpulse(2*pwn,zero,0.0,0.0);

     delay(2.0e-6);
     zgradpulse(gzlvl10,gt10);
     delay(2.0e-6);

     decpower(dvhpwra);

     delay(0.80e-3 - gt10 - 4.0e-6 - 2*POWER_DELAY);
     delay(0.2e-6);
     
     rgpulse(2*pw,zero,0.0,0.0);

     decphase(t4);

     initval(1.0,v3);
     decstepsize(0.0);
     dcplrphase(v3);

     delay(BigTC - 0.80e-3);

     decrgpulse(pwca180a,t4,0.0,0.0);

     dcplrphase(zero);

     delay(2.0e-6);
     zgradpulse(gzlvl10,gt10);
     delay(2.0e-6);

     delay(BigTC - tau1 + 2*pwn + 2*pw - 2*POWER_DELAY - gt10 - 4.0e-6);
     delay(0.2e-6);

     decpower(dhpwrcoa);
     decshaped_pulse(spco180a,pwco180a,zero,4.0e-6,0.0); /* bloch seigert */
     decpower(dhpwr);

   decrgpulse(pwca90a,zero,2.0e-6,0.0);

     txphase(one); delay(2.0e-6);

     /* H decoupling on */
     obspower(tpwrml);
     obsprgon("waltz16",pwmlev,90.0);
     xmtron();    /* TURN ME OFF  DONT FORGET  */
     /* H decoupling on */

   decpower(dhpwrcoa);
   decshaped_pulse(spco180a,pwco180a,zero,4.0e-6,0.0); /* bloch seigert */
   decphase(t5);

   initval(1.0,v3);
   decstepsize(0.0);
   dcplrphase(v3);
 
   delay(tauc - 3*POWER_DELAY - PRG_START_DELAY);
   
   decpower(dvhpwra);
   decrgpulse(pwca180a,t5,0.0,0.0);

   dcplrphase(zero);

   decpower(dhpwrcoa);
   decshaped_pulse(spco180a,pwco180a,zero,4.0e-6,0.0); 
   decphase(zero);
   decpower(dhpwr);
   delay(tauc - 2*POWER_DELAY);

   decrgpulse(pwca90a,zero,0.0,0.0);

   /* H decoupling off */
   xmtroff();
   obsprgoff();
   /* H decoupling off */

   rgpulse(pwmlev,two,2.0e-6,0.0);

   delay(0.2e-6);
   decoffset(dof);
   decpower(dhpwrb);

   delay(0.2e-6);
   zgradpulse(gzlvl4,gt4);
   delay(gstab);

   rgpulse(pwmlev,zero,2.0e-6,0.0);
   txphase(one); delay(2.0e-6);

   /* H decoupling on */
   obspower(tpwrml);
   obsprgon("waltz16",pwmlev,90.0);
   xmtron();
   /* H decoupling on */

   decphase(t6);
   delay(2.0e-6);
   decshaped_pulse(spco90b,pwco90b,t6,0.0,0.0);

   decphase(zero);
   delay(taud - POWER_DELAY - 4.0e-6);

   decpower(dvhpwrb);
   decrgpulse(pwca180b,zero,4.0e-6,0.0);
   decpower(dhpwrb);
   delay(taue - taud - POWER_DELAY + 2*pwn);

   /* adjust phase */
   initval(1.0,v2);
   decstepsize(sphase1);
   dcplrphase(v2);
   /* adjust phase */
    
   decshaped_pulse(spco180b,pwco180b,zero,0.0,0.0);
   dcplrphase(zero);
   
   dec2rgpulse(2*pwn,zero,0.0,0.0);
   delay(taue - 2*POWER_DELAY - 4.0e-6 - 4.0e-6);    

   decpower(dvhpwrb);
   decrgpulse(pwca180b,zero,4.0e-6,0.0); /* bloch seigert */
   decpower(dhpwrb);

   decshaped_pulse(spco90b,pwco90b,t7,4.0e-6,0.0);

   /* H decoupling off */
   xmtroff();
   obsprgoff();
   /* H decoupling off */

   rgpulse(pwmlev,two,2.0e-6,0.0);

   delay(0.2e-6);
   zgradpulse(gzlvl5,gt5);
   delay(gstab);

   rgpulse(pwmlev,zero,2.0e-6,0.0);

   txphase(one); delay(2.0e-6);

   /* H decoupling on */
   obspower(tpwrml);
   obsprgon("waltz16",pwmlev,90.0);
   xmtron();
   /* H decoupling on */

   dec2rgpulse(pwn,t8,2.0e-6,0.0);
   dec2phase(t9); decphase(zero);

   /* seduce on */

   decpower(dpwrsed);
   decprgon(cadecseq,pwcadec,dressed);
   decon();
   /* seduce on */

   delay(BigTN - tau2 + WFG_START_DELAY + WFG_STOP_DELAY + pwco180b);


  /* seduce off */
  decoff();
  decprgoff();
  
  decpower(dhpwrb);
  /* seduce off */

  dec2rgpulse(2*pwn,t9,0.0,0.0);
  decshaped_pulse(spco180b,pwco180b,zero,0.0,0.0);

  dec2phase(t11);

   /* seduce on */

   decpower(dpwrsed);
   decprgon(cadecseq,pwcadec,dressed);
   decon();
   /* seduce on */

  delay(BigTN + tau2 - 5.5e-3 - POWER_DELAY - PRG_STOP_DELAY - pwmlev - 2.0e-6);

   /* H decoupling off */ 
   xmtroff();
   obsprgoff();
   /* H decoupling off */

   rgpulse(pwmlev,two,2.0e-6,0.0);    
   obspower(tpwr);

   delay(2.5e-3);

  /* seduce off */
  decoff();
  decprgoff();
  decpower(dhpwrb);
  /* seduce off */

   delay(0.2e-6);
   zgradpulse(gzlvl1,gt1);
   delay(2.0e-6);
   
   txphase(zero);
   dec2phase(t11);
   delay(3.0e-3 - gt1 - 2.2e-6 - 2.0*GRADIENT_DELAY);
  
   sim3pulse(pw,0.0,pwn,zero,zero,t11,0.0,0.0);

   delay(0.2e-6);
   zgradpulse(gzlvl7,gt7);
   delay(2.0e-6);

   dec2phase(zero);
   delay(tauf - gt7 - 2.2e-6);

   sim3pulse(2*pw,0.0,2*pwn,zero,zero,zero,0.0,0.0);

   delay(0.2e-6);
   zgradpulse(gzlvl7,gt7);
   delay(2.0e-6);
   
   txphase(t12);
   dec2phase(t13);
   delay(tauf - gt7 - 2.2e-6);

   sim3pulse(pw,0.0,pwn,t12,zero,t13,0.0,0.0);
   
   delay(0.2e-6);
   zgradpulse(gzlvl7,gt7);
   delay(2.0e-6);
 
   txphase(zero);
   dec2phase(zero);
   delay(tauf - gt7 - 2.2e-6);
   sim3pulse(2*pw,0.0,2*pwn,zero,zero,zero,0.0,0.0);

  
   delay(0.2e-6);
   zgradpulse(gzlvl7,gt7);
   delay(2.0e-6);

   txphase(zero);
   delay(tauf - gt7 - 2.2e-6);
   
   rgpulse(pw,zero,0.0,0.0);

   txphase(zero);

   delay(BigT1);

   rgpulse(2*pw,zero,0.0,0.0);

   delay(2.0e-6);
   zgradpulse(icosel*gzlvl2,gt1/10);
   delay(2.0e-6);

   delay(BigT1 - gt1/10 - POWER_DELAY - 4.0e-6 - 2*GRADIENT_DELAY);

   dec2power(dpwr2);  /* set power for 15N decoupling */
    

/* BEGIN ACQUISITION */

status(C);
         setreceiver(t10);

}
Example #8
0
pulsesequence()
{
  /* DECLARE AND LOAD VARIABLES */

  char f1180[MAXSTR],		/* Flag to start t1 @ halfdwell */
       f2180[MAXSTR],		/* Flag to start t2 @ halfdwell */
       H2Opurge[MAXSTR], stCdec[MAXSTR],	/* calls STUD+ waveforms from shapelib */
       STUD[MAXSTR];		/* apply automatically calculated STUD decoupling */

  int t1_counter,		/* used for states tppi in t1 */
      t2_counter;		/* used for states tppi in t2 */

  double tau1,			/*  t1 delay */
         BPdpwrspinlock,        /*  user-defined upper limit for spinlock(Hz) */
         BPpwrlimits,           /*  =0 for no limit, =1 for limit             */
         tau2,			/*  t2 delay */
         ni = getval("ni"), ni2 = getval("ni2"),
	 stdmf = getval("dmf80"),	/* dmf for 80 ppm of STUD decoupling */
         rf80 = getval("rf80"),	/* rf in Hz for 80ppm STUD+ */
         taua = getval("taua"),	/* time delays for CH coupling evolution */
         taub = getval("taub"), tauc = getval("tauc"),
	 /* string parameter stCdec calls stud decoupling waveform from your shapelib. */
         studlvl,		/* coarse power for STUD+ decoupling */
         pwClvl = getval("pwClvl"),	/* coarse power for C13 pulse */
         pwC = getval("pwC"),	/* C13 90 degree pulse length at pwClvl */
         rf0,			/* maximum fine power when using pwC pulses */
	 /* p_d is used to calculate the isotropic mixing on the Cab region            */
         p_d,			/* 50 degree pulse for DIPSI-3 at rfd  */
         rfd,			/* fine power for 9.0 kHz rf at 600MHz         */
         ncyc = getval("ncyc"),	/* no. of cycles of DIPSI-3 */
         spinlock = getval("spinlock"),		/* DIPSI-3 Field Strength in Hz */
	 /* the following pulse length for the SLP pulse is automatically calculated   */
	 /* by the macro "hcch_tocsy".  The SLP pulse shape,"offC10" is called         */
	 /* directly from your shapelib.                                               */
         pwC10 = getval("pwC10"),	/* 180 degree selective sinc pulse on CO(174ppm) */
         rf7,			/* fine power for the pwC10 ("offC10") pulse */
         compC = getval("compC"),	/* adjustment for C13 amplifier compression */
         pwNlvl = getval("pwNlvl"),	/* power for N15 pulses */
         pwN = getval("pwN"),	/* N15 90 degree pulse length at pwNlvl */
         sw1 = getval("sw1"), sw2 = getval("sw2"),
	 gt0 = getval("gt0"),	/* other gradients */
         gt3 = getval("gt3"), gt4 = getval("gt4"), gt5 = getval("gt5"),
         gt7 = getval("gt7"), gzlvl0 = getval("gzlvl0"), gzlvl3 = getval("gzlvl3"),
         gzlvl4 = getval("gzlvl4"), gzlvl5 = getval("gzlvl5"), gzlvl6 = getval("gzlvl6"),
         gzlvl7 = getval("gzlvl7");

  getstr("f1180", f1180);
  getstr("f2180", f2180);
  getstr("H2Opurge", H2Opurge);
  getstr("STUD", STUD);
  /* 80 ppm STUD+ decoupling */
  strcpy(stCdec, "stCdec80");
  studlvl = pwClvl + 20.0 * log10(compC * pwC * 4.0 * rf80);
  studlvl = (int) (studlvl + 0.5);

  P_getreal(GLOBAL,"BPpwrlimits",&BPpwrlimits,1);
  P_getreal(GLOBAL,"BPdpwrspinlock",&BPdpwrspinlock,1);

  /*   LOAD PHASE TABLE    */
  settable(t3, 2, phi3);
  settable(t5, 4, phi5);
  settable(t9, 8, phi9);
  settable(t11, 8, rec);


  /*   INITIALIZE VARIABLES   */
  if (BPpwrlimits > 0.5)
  {
   if (spinlock > BPdpwrspinlock)
    {
     spinlock = BPdpwrspinlock;  
     printf("spinlock too large, reset to user-defined limit (BPdpwrspinlock)");
     psg_abort(1);
    }
  }

  if (dpwrf < 4095)
  {
    printf("reset dpwrf=4095 and recalibrate C13 90 degree pulse");
    psg_abort(1);
  }

  if ((pwC > (25.0e-6 * 600.0 / sfrq)) && (ncyc > 0.0))
  {
    printf("Increase pwClvl so that pwC < 25*600/sfrq");
    psg_abort(1);
  }

  /* maximum fine power for pwC pulses */
  rf0 = 4095.0;

  /* 180 degree one-lobe sinc pulse on CO, null at Ca 139ppm away */
  rf7 = (compC * 4095.0 * pwC * 2.0 * 1.65) / pwC10;	/* needs 1.65 times more     */
  rf7 = (int) (rf7 + 0.5);	/* power than a square pulse */

  if (spinlock < 1000.0)
  {
    printf("Spinlock seems too low. Please check spinlock value ! ");
    psg_abort(1);
  }

  /* dipsi-3 spinlock on CbCa */
  p_d = (5.0) / (9.0 * 4.0 * spinlock);		/* DIPSI-3 */
  rfd = (compC * 4095.0 * pwC * 5.0) / (p_d * 9.0);
  rfd = (int) (rfd + 0.5);
  ncyc = (int) (ncyc + 0.5);
/*************************For Ultra-High Field Probes***************************/
if (sfrq>590.0)
{
 if (ncyc>2)
  {
    if (pwC>15)
     {
      if (rfd > 2000)
       {
        printf("spinlock too large. Lower value for probe protection");
        psg_abort(1);
       }
     }
    else
     {
      if (pwC>14)
       {
        if (rfd > 1800)
         {
          printf("spinlock too large. Lower value for probe protection");
          psg_abort(1);
         }
       }
      else
       {
        if (pwC>13)
         {
          if (rfd > 1600)
           {
            printf("spinlock too large. Lower value for probe protection");
            psg_abort(1);
           }
         }
        else
         {
          if (pwC>12)
           {
            if (rfd > 1400)
             {
               printf("spinlock too large. Lower value for probe protection");
               psg_abort(1);
             }
           }
          else
           {
            if (pwC>11)
             {
              if (rfd > 1200)
               {
                printf("spinlock too large. Lower value for probe protection");
                psg_abort(1);
               }
             }
            else
             {
                if (rfd > 1000)
                 {
                  printf("spinlock too large. Lower value for probe protection");
                  psg_abort(1);
                 }
             }
           }
         }    
       }
     }
  }
 else 
  {
   if (ncyc == 2)
    {
     if (pwC>15)
      {
       if (rfd > 2200)
        {
         printf("spinlock too large. Lower value for probe protection");
         psg_abort(1);
        }
      }
     else
      {
       if (pwC>14)
        {
         if (rfd > 2000)
          {
           printf("spinlock too large. Lower value for probe protection");
           psg_abort(1);
          }
        }
       else
        {
         if (pwC>13)
          {
           if (rfd > 1800)
            {
             printf("spinlock too large. Lower value for probe protection");
             psg_abort(1);
            }
          }
         else
          {
           if (pwC>12)
            {
             if (rfd > 1600)
              {
                printf("spinlock too large. Lower value for probe protection");
                psg_abort(1);
              }
            }
           else
            {
             if (pwC>11)
              {
               if (rfd > 1400)
                {
                 printf("spinlock too large. Lower value for probe protection");
                 psg_abort(1);
                }
              }
             else
              {
                 if (rfd > 1200)
                  {
                   printf("spinlock too large. Lower value for probe protection");
                   psg_abort(1);
                  }
              }
            }
          }    
        }
      }
     }
   else
    {
     if (ncyc == 1)
      {
       if (pwC>15)
        {
         if (rfd > 2400)
          {
           printf("spinlock too large. Lower value for probe protection");
           psg_abort(1);
          }
        }
       else
        {
         if (pwC>14)
          {
           if (rfd > 2200)
            {
             printf("spinlock too large. Lower value for probe protection");
             psg_abort(1);
            }
          }
         else
          {
           if (pwC>13)
            {
             if (rfd > 2000)
              {
               printf("spinlock too large. Lower value for probe protection");
               psg_abort(1);
              }
            }
           else
            {
             if (pwC>12)
              {
               if (rfd > 1800)
                {
                  printf("spinlock too large. Lower value for probe protection");
                  psg_abort(1);
                }
              }
             else
              {
               if (pwC>11)
                {
                 if (rfd > 1600)
                  {
                   printf("spinlock too large. Lower value for probe protection");
                   psg_abort(1);
                  }
                }
               else
                {
                   if (rfd > 1400)
                    {
                     printf("spinlock too large. Lower value for probe protection");
                     psg_abort(1);
                    }
                }
              }
            }       
          }
        }
      }
    }

  }


}
/*********************End: For Ultra-High Field Probes***************************/

  /* CHECK VALIDITY OF PARAMETER RANGES */

  if ((dm[A] == 'y' || dm[B] == 'y'))
  {
    printf("incorrect dec1 decoupler flags! Should be 'nny' or 'nnn' ");
    psg_abort(1);
  }

  if ((dm2[A] == 'y' || dm2[B] == 'y' || dm2[C] == 'y'))
  {
    printf("incorrect dec2 decoupler flags! Should be 'nnn' ");
    psg_abort(1);
  }

  if ((dm3[A] == 'y' || dm3[C] == 'y'))
  {
    printf("incorrect dec1 decoupler flags! Should be 'nyn' or 'nnn' ");
    psg_abort(1);
  }

  if (dpwr > 52)
  {
    printf("don't fry the probe, DPWR too large!  ");
    psg_abort(1);
  }

  if (pw > 80.0e-6)
  {
    printf("dont fry the probe, pw too high ! ");
    psg_abort(1);
  }

  if (pwN > 100.0e-6)
  {
    printf("dont fry the probe, pwN too high ! ");
    psg_abort(1);
  }


  /* PHASES AND INCREMENTED TIMES */
  /*  Phase incrementation for hypercomplex 2D data, States-Haberkorn element */
  if (phase1 == 2)
    tsadd(t3, 1, 4);
  if (phase2 == 2)
    tsadd(t5, 1, 4);

  /*  C13 TIME INCREMENTATION and set up f1180  */

  /*  Set up f1180  */
  tau1 = d2;

  if (f1180[A] == 'y')
  {
    tau1 += (1.0 / (2.0 * sw1));
    if (tau1 < 0.2e-6)
      tau1 = 0.0;
  }

  tau1 = tau1 / 2.0;


  /*  Set up f2180  */

  tau2 = d3;

  if (f2180[A] == 'y')
  {
    tau2 += (1.0 / (2.0 * sw2));
    if (tau2 < 0.2e-6)
      tau2 = 0.0;
  }

  tau2 = tau2 / 2.0;



  /* Calculate modifications to phases for States-TPPI acquisition          */

  if (ix == 1)
    d2_init = d2;
  t1_counter = (int) ((d2 - d2_init) * sw1 + 0.5);
  if (t1_counter % 2)
  {
    tsadd(t3, 2, 4);
    tsadd(t11, 2, 4);
  }

  if (ix == 1)
    d3_init = d3;
  t2_counter = (int) ((d3 - d3_init) * sw2 + 0.5);
  if (t2_counter % 2)
  {
    tsadd(t5, 2, 4);
    tsadd(t11, 2, 4);
  }



  /*   BEGIN PULSE SEQUENCE   */

  status(A);
  if (dm3[B] == 'y')
    lk_sample();
  if ((ni / sw1 - d2) > 0)
    delay(ni / sw1 - d2);	/*decreases as t1 increases for const.heating */
  if ((ni2 / sw2 - d3) > 0)
    delay(ni2 / sw2 - d3);	/*decreases as t2 increases for const.heating */
  delay(d1);
  if (dm3[B] == 'y')
  {
    lk_hold();
    lk_sampling_off();
  }				/*freezes z0 correction, stops lock pulsing */
  rcvroff();

  obspower(tpwr);
  decpower(pwClvl);
  dec2power(pwNlvl);
  decpwrf(rf0);
  obsoffset(tof);
  txphase(t3);
  delay(1.0e-5);

  decrgpulse(pwC, zero, 0.0, 0.0);	/*destroy C13 magnetization */
  zgradpulse(gzlvl0, 0.5e-3);
  delay(1.0e-4);
  decrgpulse(pwC, one, 0.0, 0.0);
  zgradpulse(0.7 * gzlvl0, 0.5e-3);
  delay(5.0e-4);

  if (dm3[B] == 'y')		/* begins optional 2H decoupling */
  {
    dec3rgpulse(1 / dmf3, one, 10.0e-6, 2.0e-6);
    dec3unblank();
    dec3phase(zero);
    delay(2.0e-6);
    setstatus(DEC3ch, TRUE, 'w', FALSE, dmf3);
  }

  rgpulse(pw, t3, 0.0, 0.0);	/* 1H pulse excitation */
  zgradpulse(gzlvl0, gt0);	/* 2.0*GRADIENT_DELAY */
  decphase(zero);
  delay(taua + tau1 - gt0 - 2.0 * GRADIENT_DELAY - 2.0 * pwC);
  decrgpulse(2.0 * pwC, zero, 0.0, 0.0);
  txphase(zero);
  delay(tau1);
  rgpulse(2.0 * pw, zero, 0.0, 0.0);
  zgradpulse(gzlvl0, gt0);
  txphase(one);
  decphase(t5);
  delay(taua - gt0);
  rgpulse(pw, one, 0.0, 0.0);
  zgradpulse(gzlvl3, gt3);
  delay(2.0e-4);
  decrgpulse(pwC, t5, 0.0, 0.0);
  delay(tau2);
  dec2rgpulse(2.0 * pwN, zero, 0.0, 0.0);
  zgradpulse(gzlvl4, gt4);	/* 2.0*GRADIENT_DELAY */
  decphase(zero);
  decpwrf(rf7);
  delay(taub - 2.0 * pwN - gt4 - 2.0 * GRADIENT_DELAY);
  decshaped_pulse("offC10", pwC10, zero, 0.0, 0.0);
  txphase(zero);
  decpwrf(rf0);
  delay(taub - 2.0 * pw);
  rgpulse(2.0 * pw, zero, 0.0, 0.0);
  delay(tau2);
  decrgpulse(2.0 * pwC, zero, 0.0, 0.0);
  decpwrf(rf7);
  delay(taub);
  decshaped_pulse("offC10", pwC10, zero, 0.0, 0.0);
  zgradpulse(gzlvl4, gt4);	/* 2.0*GRADIENT_DELAY */
  delay(taub - gt4 - 2.0 * GRADIENT_DELAY);
  decpwrf(rfd);
  decrgpulse(1.0e-3, zero, 0.0, 0.0);
  if (ncyc>0)
  {
  initval(ncyc, v2);
  starthardloop(v2);
  decrgpulse(4.9 * p_d, one, 0.0, 0.0);
  decrgpulse(7.9 * p_d, three, 0.0, 0.0);
  decrgpulse(5.0 * p_d, one, 0.0, 0.0);
  decrgpulse(5.5 * p_d, three, 0.0, 0.0);
  decrgpulse(0.6 * p_d, one, 0.0, 0.0);
  decrgpulse(4.6 * p_d, three, 0.0, 0.0);
  decrgpulse(7.2 * p_d, one, 0.0, 0.0);
  decrgpulse(4.9 * p_d, three, 0.0, 0.0);
  decrgpulse(7.4 * p_d, one, 0.0, 0.0);
  decrgpulse(6.8 * p_d, three, 0.0, 0.0);
  decrgpulse(7.0 * p_d, one, 0.0, 0.0);
  decrgpulse(5.2 * p_d, three, 0.0, 0.0);
  decrgpulse(5.4 * p_d, one, 0.0, 0.0);
  decrgpulse(0.6 * p_d, three, 0.0, 0.0);
  decrgpulse(4.5 * p_d, one, 0.0, 0.0);
  decrgpulse(7.3 * p_d, three, 0.0, 0.0);
  decrgpulse(5.1 * p_d, one, 0.0, 0.0);
  decrgpulse(7.9 * p_d, three, 0.0, 0.0);

  decrgpulse(4.9 * p_d, three, 0.0, 0.0);
  decrgpulse(7.9 * p_d, one, 0.0, 0.0);
  decrgpulse(5.0 * p_d, three, 0.0, 0.0);
  decrgpulse(5.5 * p_d, one, 0.0, 0.0);
  decrgpulse(0.6 * p_d, three, 0.0, 0.0);
  decrgpulse(4.6 * p_d, one, 0.0, 0.0);
  decrgpulse(7.2 * p_d, three, 0.0, 0.0);
  decrgpulse(4.9 * p_d, one, 0.0, 0.0);
  decrgpulse(7.4 * p_d, three, 0.0, 0.0);
  decrgpulse(6.8 * p_d, one, 0.0, 0.0);
  decrgpulse(7.0 * p_d, three, 0.0, 0.0);
  decrgpulse(5.2 * p_d, one, 0.0, 0.0);
  decrgpulse(5.4 * p_d, three, 0.0, 0.0);
  decrgpulse(0.6 * p_d, one, 0.0, 0.0);
  decrgpulse(4.5 * p_d, three, 0.0, 0.0);
  decrgpulse(7.3 * p_d, one, 0.0, 0.0);
  decrgpulse(5.1 * p_d, three, 0.0, 0.0);
  decrgpulse(7.9 * p_d, one, 0.0, 0.0);

  decrgpulse(4.9 * p_d, three, 0.0, 0.0);
  decrgpulse(7.9 * p_d, one, 0.0, 0.0);
  decrgpulse(5.0 * p_d, three, 0.0, 0.0);
  decrgpulse(5.5 * p_d, one, 0.0, 0.0);
  decrgpulse(0.6 * p_d, three, 0.0, 0.0);
  decrgpulse(4.6 * p_d, one, 0.0, 0.0);
  decrgpulse(7.2 * p_d, three, 0.0, 0.0);
  decrgpulse(4.9 * p_d, one, 0.0, 0.0);
  decrgpulse(7.4 * p_d, three, 0.0, 0.0);
  decrgpulse(6.8 * p_d, one, 0.0, 0.0);
  decrgpulse(7.0 * p_d, three, 0.0, 0.0);
  decrgpulse(5.2 * p_d, one, 0.0, 0.0);
  decrgpulse(5.4 * p_d, three, 0.0, 0.0);
  decrgpulse(0.6 * p_d, one, 0.0, 0.0);
  decrgpulse(4.5 * p_d, three, 0.0, 0.0);
  decrgpulse(7.3 * p_d, one, 0.0, 0.0);
  decrgpulse(5.1 * p_d, three, 0.0, 0.0);
  decrgpulse(7.9 * p_d, one, 0.0, 0.0);

  decrgpulse(4.9 * p_d, one, 0.0, 0.0);
  decrgpulse(7.9 * p_d, three, 0.0, 0.0);
  decrgpulse(5.0 * p_d, one, 0.0, 0.0);
  decrgpulse(5.5 * p_d, three, 0.0, 0.0);
  decrgpulse(0.6 * p_d, one, 0.0, 0.0);
  decrgpulse(4.6 * p_d, three, 0.0, 0.0);
  decrgpulse(7.2 * p_d, one, 0.0, 0.0);
  decrgpulse(4.9 * p_d, three, 0.0, 0.0);
  decrgpulse(7.4 * p_d, one, 0.0, 0.0);
  decrgpulse(6.8 * p_d, three, 0.0, 0.0);
  decrgpulse(7.0 * p_d, one, 0.0, 0.0);
  decrgpulse(5.2 * p_d, three, 0.0, 0.0);
  decrgpulse(5.4 * p_d, one, 0.0, 0.0);
  decrgpulse(0.6 * p_d, three, 0.0, 0.0);
  decrgpulse(4.5 * p_d, one, 0.0, 0.0);
  decrgpulse(7.3 * p_d, three, 0.0, 0.0);
  decrgpulse(5.1 * p_d, one, 0.0, 0.0);
  decrgpulse(7.9 * p_d, three, 0.0, 0.0);

  endhardloop();
  }
  decrgpulse(9.0 * p_d / 5.0, t9, 2.0e-6, 0.0);
  if (H2Opurge[A] == 'y')
  {
    obspwrf(1000);
    rgpulse(900 * pw, zero, 0.0, 0.0);
    rgpulse(500 * pw, one, 0.0, 0.0);
    obspwrf(4095.0);
  }
  zgradpulse(gzlvl7, gt7);
  decpwrf(rf0);
  delay(50.0e-6);
  rgpulse(pw, zero, 0.0, 0.0);
  zgradpulse(gzlvl7, gt7 / 1.6);
  decrgpulse(pwC, three, 100.0e-6, 0.0);
  zgradpulse(gzlvl5, gt5);
  decphase(zero);
  delay(tauc - gt5);
  simpulse(2.0 * pw, 2.0 * pwC, zero, zero, 0.0, 0.0);
  zgradpulse(gzlvl5, gt5);
  delay(tauc - gt5);
  decrgpulse(pwC, zero, 0.0, 0.0);
  zgradpulse(gzlvl3, gt3);
  if (dm3[B] == 'y')		/* turns off 2H decoupling  */
  {
    setstatus(DEC3ch, FALSE, 'c', FALSE, dmf3);
    dec3rgpulse(1 / dmf3, three, 2.0e-6, 2.0e-6);
    dec3blank();
    lk_autotrig();		/* resumes lock pulsing */
  }
  delay(2.0e-4);
  rgpulse(pw, zero, 0.0, 0.0);
  zgradpulse(gzlvl6, gt5);
  delay(taua - gt5 + rof1);
  simpulse(2.0 * pw, 2.0 * pwC, zero, zero, 0.0, rof1);
  zgradpulse(gzlvl6, gt5);
  if (STUD[A] == 'y')
    decpower(studlvl);
  else
    decpower(dpwr);
  dec2power(dpwr2);
  delay(taua - gt5 - 2.0 * POWER_DELAY);
  rgpulse(pw, zero, 0.0, rof2);
  rcvron();
  if (dm3[B] == 'y')
    lk_sample();
  setreceiver(t11);
  if ((STUD[A] == 'y') && (dm[C] == 'y'))
  {
    decprgon(stCdec, 1.0 / stdmf, 1.0);
    decon();
    if (dm2[C] == 'y')
    {
      setstatus(DEC2ch, TRUE, dmm2[C], FALSE, dmf2);
    }
  }
  else
    status(C);
}
Example #9
0
void pulsesequence()
{
/* DECLARE VARIABLES */

 char       autocal[MAXSTR],  /* auto-calibration flag */
            fsat[MAXSTR],
            fscuba[MAXSTR],
            f1180[MAXSTR],    /* Flag to start t1 @ halfdwell         */
            f2180[MAXSTR],    /* Flag to start t2 @ halfdwell         */
            shib[MAXSTR],     /* iburp for inversion during first inept     */
            Hshp[MAXSTR],     /* proton inversion during chirp        */
            ddseq[MAXSTR],
            shreb[MAXSTR],    /* reburb hard during t2                */
            co_shp[MAXSTR],   /* shape of co 180 at 176 ppm */
            CT_flg[MAXSTR],
            codecseq[MAXSTR],
            c180_flg[MAXSTR],

            n_shift[MAXSTR],
            shibca[MAXSTR],
            shibcai[MAXSTR];

 int         phase, phase2, t2_counter, ni2, ni,
             t1_counter;   /* used for states tppi in t2,t1        */ 

 double      tau1,         /*  t1 delay */
             tau2,         /*  t2 delay */
             taua,         /*  ~ 1/4JCH =  1.7 ms; first inept */
             mix,	   /* noesy mixing time */
             TC,           /* Variable CT period during t1 1/2JCC */
             TC2,          /* Variable CT period during t3  1/2JCC */
             pwc,          /* 90 c pulse at dhpwr            */
             tsatpwr,      /* low level 1H trans.power for presat  */
             dhpwr,        /* power level for high power 13C pulses on dec1 */
             sw1,          /* sweep width in f1                    */ 
             sw2,          /* sweep width in f2                    */ 
             pwC,pwClvl,compC,pwN,pwNlvl,ppm,ofs,bw,  /*used by Pbox */
             d_ib,
             pwib,

             pwhshp,

             pwd1,        /* 2H flip back pulses   */

             d_reb,
             pwreb,

             ph_reb,
             ph_reb1,    /* only used if CT_flg=='y' and n_shift=='y'  */

             pwco180,

             dhpwr2,
             pwn,

             d_co180,

             pwcodec,    /* carbon pw90 for seduce decoupling */
             dpwrsed,
             dressed,

             d_ibca,     /* power level for selective 13Ca pulse during CT-t2 */
             pwibca,     /* selective 13Ca pulse width  */

             gt1,
             gt2,
             gt3,
             gt4,
             gt5,
             gt6,
             gt7,
             gt8,
             gt9,
             gt10,
             gt11,
             gt12,
             gstab,
             gzlvl1,
             gzlvl2,
             gzlvl3,
             gzlvl4,
             gzlvl5,
             gzlvl6,
             gzlvl7,
             gzlvl8,
             gzlvl9,
             gzlvl10,
             gzlvl11,
             gzlvl12;

/*  variables commented out are already defined by the system      */


/* LOAD VARIABLES */

  getstr("autocal",autocal);
  getstr("fsat",fsat);
  getstr("f1180",f1180);
  getstr("f2180",f2180);
  getstr("fscuba",fscuba);
  getstr("ddseq",ddseq);
  getstr("n_shift",n_shift); 
  getstr("Hshp",Hshp);
  getstr("CT_flg",CT_flg);
  getstr("c180_flg",c180_flg);

  compC = getval("compC"); pwN=getval("pwN"); pwNlvl=getval("pwNlvl");
  pwC = getval("pwC"); pwClvl=getval("pwClvl");
  
  pwhshp = getval("pwhshp");
  taua   = getval("taua"); 
  mix   = getval("mix"); 
  TC = getval("TC");
  pwc = getval("pwc");
  tpwr = getval("tpwr");
  tsatpwr = getval("tsatpwr");
  dhpwr = getval("dhpwr");
  dpwr = getval("dpwr");
  phase = (int) ( getval("phase") + 0.5);
  phase2 = (int) ( getval("phase2") + 0.5);
  sw1 = getval("sw1");
  sw2 = getval("sw2");
  ni2 = getval("ni2");
  ni  = getval("ni");

  pwd1 = getval("pwd1");

  ph_reb = getval("ph_reb");
  ph_reb1 = getval("ph_reb1");

  TC2 = getval("TC2");

  dhpwr2 = getval("dhpwr2");
  pwn = getval("pwn");

  setautocal();

  if(autocal[0]=='n')
  {     
    getstr("shreb",shreb);
    getstr("shib",shib);
    getstr("shibca",shibca);
    getstr("shibcai",shibcai);
    getstr("co_shp",co_shp);
    getstr("codecseq",codecseq);

    d_reb = getval("d_reb");
    pwreb = getval("pwreb");
    d_ib = getval("d_ib");
    pwib = getval("pwib");
    d_ibca = getval("d_ibca");
    pwibca = getval("pwibca"); 
    d_co180 = getval("d_co180");
    pwco180 = getval("pwco180");
    pwcodec = getval("pwcodec");
    dpwrsed = getval("dpwrsed");
    dressed = getval("dressed");
  }
  else
  {    
  /*strcpy(Hshp,"hard");  former declarations using TNMR.h syntax
    strcpy(shreb,"Preb_5p");
    strcpy(shib,"Pib_1p5");
    strcpy(shibca,"Pib_35p");
    strcpy(shibcai,"Pib_35pi");    
    strcpy(co_shp,"Psed_156p");
    strcpy(codecseq,"Pdec_156p");*/

    strcpy(Hshp,"hard");
    strcpy(shreb,"Preb_5p");
    strcpy(shib,"Pib_1p5");
    strcpy(shibca,"Pib_35p");
    strcpy(shibcai,"Pib_35pi");    
    strcpy(co_shp,"Psed_156p");
    strcpy(codecseq,"Pdec_156p");
    if (FIRST_FID)
    {
      ppm = getval("dfrq");

/*       These are former declarations (at top) using TNMR.h syntax                     */
/*REB180   "reburp 110p 5p"*/             /* RE-BURP 180 on Cab at 24.6 ppm, 5 ppm away */
/*IB180    "iburp2 24.4p 1.5p"*/          /* I-BURP 180 on  Me at 21.1 ppm, 1.5 ppm away */
/*IBCA     "iburp2 24.4p 35p"*/           /* I-BURP 180 on Cab at 54.6 ppm, 35 ppm away */
/*IBCAI    "iburp2 24.4p 35p"*/           /* I-BURP 180 on Cab at 54.6 ppm, 35 ppm away */
/*CO180    "seduce 30p 156p"*/            /* SEDUCE 180 on C' at 175.6 ppm 156 ppm away */
/*CODEC    "WURST2 20p/4m 156p"*/  /* WURST2 decoupling on C' at 175.6 ppm 156 ppm away */
/*REB180ps "-stepsize 0.5 -attn i"*/                     /* seduce 180 shape parameters */
/*CODECps  "-dres 1.0 -maxincr 20.0 -attn i"*/
    /*co180 = pbox(co_shp, CO180, REB180ps, dfrq, compC*pwc, dhpwr);*/
    /*ibcai = pbox(shibcai, IBCAI, REB180ps, dfrq, compC*pwc, dhpwr);*/      
    /*ibca = pbox(shibca, IBCA, REB180ps, dfrq, compC*pwc, dhpwr);*/
    /*ib180 = pbox(shib, IB180, REB180ps, dfrq, compC*pwc, dhpwr);*/          
    /*reb = pbox(shreb, REB180, REB180ps, dfrq, compC*pwc, dhpwr);*/
    /*COdec = pbox(codecseq, CODEC, CODECps, dfrq, compC*pwc, dhpwr);*/

      bw = 110.0*ppm; ofs = 5.0*ppm;
      Preb_5p = pbox_Rsh("Preb_5p", "reburp", bw , ofs, compC*pwC, pwClvl);
      bw = 24.4*ppm; ofs = 1.5*ppm;
      Pib_1p5 = pbox_Rsh("Pib_1p5", "iburp2", bw , ofs, compC*pwC, pwClvl);
      bw = 24.4*ppm; ofs = 35*ppm;
      Pib_35p = pbox_Rsh("Pib_35p", "iburp2", bw , ofs, compC*pwC, pwClvl);
      bw = 24.4*ppm; ofs = 35*ppm;
      Pib_35pi = pbox_Rsh("Pib_35pi", "iburp2", bw , ofs, compC*pwC, pwClvl);
      bw = 30.0*ppm; ofs = 156*ppm;
      Psed_156p = pbox_Rsh("Psed_156p", "seduce", bw , ofs, compC*pwC, pwClvl);
      bw = 20.0*ppm; ofs = 156*ppm;
      Pdec_156p = pbox_Dsh("Pdec_156p", "WURST2", bw , ofs, compC*pwC, pwClvl);


      ofs_check(H1ofs, C13ofs, N15ofs, H2ofs);
    }
    d_reb = Preb_5p.pwr;        pwreb = Preb_5p.pw;
    d_ib = Pib_1p5.pwr;         pwib = Pib_1p5.pw;
    d_ibca = Pib_35p.pwr;       pwibca = Pib_35p.pw;       
    d_co180 = Psed_156p.pwr;    pwco180 = Psed_156p.pw;  
    dpwrsed = Pdec_156p.pwr;    pwcodec = 1.0/Pdec_156p.dmf;  dressed = Pdec_156p.dres;

    pwc=pwC; dhpwr=pwClvl; pwn=pwN; dhpwr2=pwNlvl; pwhshp=2.0*pw;
    pwd1=1/dmf3; pwhshp=2.0*pw;
  }   
   
  gt1 = getval("gt1");
  gt2 = getval("gt2");
  gt3 = getval("gt3");
  gt4 = getval("gt4");
  gt5 = getval("gt5");
  gt6 = getval("gt6");
  gt7 = getval("gt7");
  gt8 = getval("gt8");
  gt9 = getval("gt9");
  gt10 = getval("gt10");
  gt11 = getval("gt11");
  gt12 = getval("gt12");

  gstab  = getval("gstab");
  gzlvl1 = getval("gzlvl1");
  gzlvl2 = getval("gzlvl2");
  gzlvl3 = getval("gzlvl3");
  gzlvl4 = getval("gzlvl4");
  gzlvl5 = getval("gzlvl5");
  gzlvl6 = getval("gzlvl6");
  gzlvl7 = getval("gzlvl7");
  gzlvl8 = getval("gzlvl8");
  gzlvl9 = getval("gzlvl9");
  gzlvl10 = getval("gzlvl10");
  gzlvl11 = getval("gzlvl11");
  gzlvl12 = getval("gzlvl12");

/* LOAD PHASE TABLE */

  settable(t1,4,phi1);
  settable(t2,8,phi2);
  settable(t7,2,phi7);
  settable(t8,2,phi8);
  settable(t9,8,rec);

/* CHECK VALIDITY OF PARAMETER RANGES */

   if(TC/2.0 - 0.5*(ni-1)*1/(sw1) - POWER_DELAY - 4.0e-6 
         - WFG3_START_DELAY - pwco180
         - WFG3_STOP_DELAY - pwd1 
         - gt4 - gstab -2.0e-6 - POWER_DELAY
         - 4.0e-6 - WFG_START_DELAY < 0.2e-6)
    {
        printf(" ni is too big\n");
        psg_abort(1);
    }

  if(CT_flg[A] == 'y' && n_shift[A] == 'n') {

   if(TC2/2.0 - 0.5*(ni2-1)*1/(sw2) - POWER_DELAY - 4.0e-6 
         - WFG3_START_DELAY - pwco180
         - WFG3_STOP_DELAY - pwd1 
         - gt10 - gstab -2.0e-6 - POWER_DELAY
         - 4.0e-6 - WFG_START_DELAY < 0.2e-6)
    {
        printf(" ni2 is too big\n");
        psg_abort(1);
    }

   }

  if(CT_flg[A] == 'y' && n_shift[A] == 'y') {

   if(TC2/2.0 - 0.5*(ni2-1)/sw2 - POWER_DELAY 
         - 4.0e-6 - WFG3_START_DELAY - pwco180
         - WFG3_STOP_DELAY - 2.0e-6 - POWER_DELAY - WFG_START_DELAY
         - 4.0e-6 - pwibca - WFG_STOP_DELAY - pwd1 
         - gt10 - gstab -2.0e-6 - POWER_DELAY
         - 4.0e-6 - WFG3_START_DELAY < 0.2e-6)
    {
        printf(" ni2 is too big\n");
        psg_abort(1);
    }

   }

    if((dm[A] == 'y' || dm[B] == 'y' ))
    {
        printf("incorrect dec1 decoupler flags!  ");
        psg_abort(1);
    }

    if((dm2[A] == 'y' || dm2[B] == 'y'))
    {
        printf("incorrect dec2 decoupler flags!  ");
        psg_abort(1);
    }

    if((dm3[A] == 'y' || dm3[B] == 'y' || dm3[C] == 'y'))
    {
        printf("incorrect dec3 decoupler flags!  ");
        psg_abort(1);
    }

    if( tsatpwr > 6 )
    {
        printf("TSATPWR too large !!!  ");
        psg_abort(1);
    }

    if( dpwr > 48 )
    {
        printf("don't fry the probe, DPWR too large!  ");
        psg_abort(1);
    }

    if( d_ib > 54 )
    {
        printf("don't fry the probe, d_ib too large!  ");
        psg_abort(1);
    }

    if( dpwr2 > 49 )
    {
        printf("don't fry the probe, DPWR2 too large!  ");
        psg_abort(1);
    }

    if( dpwr3 > 51 )
    {
        printf("don't fry the probe, DPWR3 too large!  ");
        psg_abort(1);
    }

    if( dhpwr > 63 )
    {
        printf("don't fry the probe, DHPWR too large!  ");
        psg_abort(1);
    }

    if( pw > 200.0e-6 )
    {
        printf("dont fry the probe, pw too high ! ");
        psg_abort(1);
    } 

    if( pwd1 < 100.0e-6 && pwd1 != 0.0)
    {
        printf("dont fry the probe, pwd1 too short and dpwr3 too high! ");
        psg_abort(1);
    } 

    if(d_co180 > 50)
    {
        printf("dont fry the probe, d_co180 is too high\n ");
        psg_abort(1);
    } 

    if(((pwco180 > 250e-6) || (pwco180 < 200e-6)) && (autocal[A] == 'n'))
     {
        printf("pwco180 is misset < 250 us > 200 us\n");
        psg_abort(1);
     }

    if(dpwrsed > 45) 
     {
        printf("dpwrsed is misset < 46\n");
        psg_abort(1);
     }

    if(gt1 > 15e-3 || gt2 > 15e-3 || gt3 > 15e-3 || 
        gt4 > 15e-3 || gt5 > 15e-3 || gt6 > 15e-3 ||
        gt7 > 15e-3 || gt8 > 15e-3 || gt9 > 15e-3 || 
        gt10 > 15e-3 || gt11 > 15e-3 || gt12 > 15e-3) 
    {
        printf("gradients on for too long. Must be < 15e-3 \n");
        psg_abort(1);
    }

/*  Phase incrementation for hypercomplex 2D data */

    if (phase2 == 2) {
      tsadd(t2,1,4);  
    }

    if (phase == 2) 
      tsadd(t1,1,4);

/*  Set up f2180  tau2 = t2               */
   
    tau2 = d3;

    if(CT_flg[A] == 'y') {

    if(f2180[A] == 'y') {
        tau2 += ( 1.0 / (2.0*sw2) );
    }

    }

    if(CT_flg[A] == 'n' && n_shift[A] == 'n') {

         if(f2180[A] == 'y') {
            tau2 += ( 1.0 / (2.0*sw2) - 4.0/PI*pwc - POWER_DELAY
                      - PRG_START_DELAY - 4.0*pw - 4.0e-6 - 2.0*pwn
                      - PRG_STOP_DELAY - POWER_DELAY - 4.0e-6);

            if(tau2 < 0.0 && ix == 1) 
               printf("tau2 start2 negative; decrease sw2\n");
          }

         if(f2180[A] == 'n') {
            tau2 = ( tau2 - 4.0/PI*pwc - POWER_DELAY
                      - PRG_START_DELAY - 4.0*pw - 4.0e-6 - 2.0*pwn
                      - PRG_STOP_DELAY - POWER_DELAY - 4.0e-6);
         }

     } 

    if(CT_flg[A] == 'n' && n_shift[A] == 'y') {

         if(f2180[A] == 'y') {
            tau2 += ( 1.0 / (2.0*sw2) - 4.0/PI*pwn - POWER_DELAY
                      - PRG_START_DELAY - 4.0*pw - 4.0e-6 
                      - PRG_STOP_DELAY - POWER_DELAY - 4.0e-6);

            if(tau2 < 0.0 && ix == 1) 
               printf("tau2 start2 negative; decrease sw2\n");
          }

         if(f2180[A] == 'n') {
            tau2 = ( tau2 - 4.0/PI*pwn - POWER_DELAY
                      - PRG_START_DELAY - 4.0*pw - 4.0e-6
                      - PRG_STOP_DELAY - POWER_DELAY - 4.0e-6);
         }

     } 

    if(tau2 < 0.4e-6) tau2 = 0.4e-6;
    tau2 = tau2/2.0;

/*  Set up f1180  tau1 = t1               */
   
    tau1 = d2;
    if(f1180[A] == 'y') {
        tau1 += ( 1.0 / (2.0*sw1) );
    }
    if(tau1 < 0.4e-6) tau1 = 0.4e-6;
    tau1 = tau1/2.0;

/* Calculate modifications to phases for States-TPPI acquisition          */

   if( ix == 1) d2_init = d2 ;
   t1_counter = (int) ( (d2-d2_init)*sw1 + 0.5 );
   if(t1_counter % 2) {
      tsadd(t1,2,4);     
      tsadd(t9,2,4);     
    }

   if( ix == 1) d3_init = d3 ;
   t2_counter = (int) ( (d3-d3_init)*sw2 + 0.5 );
   if(t2_counter % 2) {
      tsadd(t2,2,4);     
      tsadd(t9,2,4);    
    }

/* BEGIN ACTUAL PULSE SEQUENCE */

status(A);
   obspower(tsatpwr);     /* Set transmitter power for 1H presaturation */
   decpower(dhpwr);       /* Set Dec1 power for hard 13C pulses         */
   dec2power(dhpwr2);    /* Set Dec2 power for hard 15N pulses         */
   dec3power(dpwr3);     /* Set Dec3 power for 2H pulses        */

/* Presaturation Period */


   if (fsat[0] == 'y')
   {
        delay(2.0e-5);
        rgpulse(d1,zero,2.0e-6,2.0e-6); /* presat */
        obspower(tpwr);    /* Set transmitter power for hard 1H pulses */
        delay(2.0e-5);
        if(fscuba[0] == 'y')
        {
                delay(2.2e-2);
                rgpulse(pw,zero,2.0e-6,0.0);
                rgpulse(2*pw,one,2.0e-6,0.0);
                rgpulse(pw,zero,2.0e-6,0.0);
                delay(2.2e-2);
        }
   }
   else
   {
    delay(d1);
   }

   obspower(tpwr);          /* Set transmitter power for hard 1H pulses */
   txphase(zero);
   dec2phase(zero);
   decphase(zero);
   delay(1.0e-5);

/* Begin Pulses */

status(B);

   rcvroff();
   lk_hold();
   delay(20.0e-6);

/* first ensure that magnetization does infact start on H and not C */

   decrgpulse(pwc,zero,2.0e-6,2.0e-6);

   delay(2.0e-6);
   zgradpulse(gzlvl1,gt1);
   delay(gstab);

   decpower(d_ib);			/* set power for chirp during inept */
   delay(4e-6);

/* this is the real start */

   rgpulse(pw,zero,0.0,0.0);                    /* 90 deg 1H pulse */

   delay(2.0e-6);
   zgradpulse(gzlvl2,gt2);
   delay(2.0e-6);

   delay(taua - gt2 - 4.0e-6 - WFG2_START_DELAY);   /* taua <= 1/4JCH */                          

   simshaped_pulse(Hshp,shib,pwhshp,pwib,zero,zero,0.0,0.0);
   decphase(zero);

   txphase(one); decphase(t1);
   decpower(dhpwr);

   delay(2.0e-6);
   zgradpulse(gzlvl2,gt2);
   delay(2.0e-6);

   delay(taua - gt2 - 4.0e-6 - WFG2_STOP_DELAY - POWER_DELAY); 

   rgpulse(pw,one,0.0,0.0);
   txphase(zero);

   delay(2.0e-6);
   zgradpulse(gzlvl3,gt3);
   delay(gstab);

   decrgpulse(pwc,t1,0.0,0.0);
   decphase(zero);

   delay(tau1);

   decpower(d_co180);
   sim3shaped_pulse(Hshp,co_shp,"hard",pwhshp,pwco180,2.0*pwn,zero,zero,zero,4.0e-6,0.0);

   delay(TC/2.0 - tau1 - POWER_DELAY - 4.0e-6 - WFG3_START_DELAY - pwco180
         - WFG3_STOP_DELAY - pwd1 
         - gt4 - gstab -2.0e-6 - POWER_DELAY
         - 4.0e-6 - WFG_START_DELAY);

   dec3rgpulse(pwd1,zero,0.0,0.0);

   delay(tau1);

   delay(2.0e-6);
   zgradpulse(gzlvl4,gt4);
   delay(gstab);

   initval(1.0,v3);
   decstepsize(ph_reb);
   dcplrphase(v3);

   decpower(d_reb);

   decshaped_pulse(shreb,pwreb,zero,4.0e-6,0.0);
   dcplrphase(zero);

   decphase(zero); decpower(dhpwr);
  
   delay(2.0e-6);
   zgradpulse(gzlvl4,gt4);
   delay(gstab);

   delay(TC/2.0 - tau1 - WFG_STOP_DELAY - POWER_DELAY
         - gt4 - gstab -2.0e-6);

   decrgpulse(pwc,zero,0.0,0.0);

   dec3rgpulse(pwd1,two,4.0e-6,0.0);


   delay(2.0e-6);
   zgradpulse(gzlvl5,gt5);
   delay(gstab);

   rgpulse(pw,zero,0.0,0.0);

   delay(2.0e-6);
   zgradpulse(gzlvl6,gt6);
   delay(gstab);

   decpower(d_ib);
   delay(taua - gt6 - 4.0e-6 - WFG2_START_DELAY - POWER_DELAY);

   simshaped_pulse(Hshp,shib,pwhshp,pwib,zero,zero,0.0,0.0);
   decphase(zero);

   delay(2.0e-6);
   zgradpulse(gzlvl6,gt6);
   delay(gstab);


   decpower(dhpwr);
   txphase(one);
   delay(taua - gt6 - gstab -2.0e-6 - POWER_DELAY - WFG2_STOP_DELAY);

   rgpulse(pw,one,0.0,0.0);
   txphase(zero);

   delay(mix - gt7 - 352.0e-6);

   decrgpulse(pwc,zero,0.0,0.0);

   delay(2.0e-6);
   zgradpulse(gzlvl7,gt7);
   delay(gstab);

   decpower(d_ib); /* set power level for iburp */

   rgpulse(pw,zero,0.0,0.0);                    /* 90 deg 1H pulse */

   delay(2.0e-6);
   zgradpulse(gzlvl8,gt8);
   delay(2.0e-6);

   if(n_shift[A] == 'n') {

   delay(taua - gt8 - 4.0e-6 - WFG2_START_DELAY);   /* taua <= 1/4JCH */                          
   simshaped_pulse(Hshp,shib,pwhshp,pwib,zero,zero,0.0,0.0);
   decphase(zero);

   }

   else {
 delay(taua - gt8 - 4.0e-6 - WFG3_START_DELAY);                 
 sim3shaped_pulse(Hshp,shib,"hard",pwhshp,pwib,2.0*pwn,zero,zero,zero,0.0,0.0);
    }


   txphase(one); decphase(t2);
   decpower(dhpwr);

   delay(2.0e-6);
   zgradpulse(gzlvl8,gt8);
   delay(2.0e-6);

   if(n_shift[A] == 'n') 
      delay(taua - gt8 - 4.0e-6 - WFG2_STOP_DELAY - POWER_DELAY); 
   else
      delay(taua - gt8 - 4.0e-6 - WFG3_STOP_DELAY - POWER_DELAY); 

   rgpulse(pw,one,0.0,0.0);
   txphase(zero);

   delay(2.0e-6);
   zgradpulse(gzlvl9,gt9);
   delay(gstab);

  if(CT_flg[A] == 'y' && n_shift[A] == 'n') {

   decrgpulse(pwc,t2,0.0,0.0);
   decphase(zero);

   delay(tau2);

   decpower(d_co180);
   sim3shaped_pulse(Hshp,co_shp,"hard",pwhshp,pwco180,2.0*pwn,zero,zero,zero,4.0e-6,0.0);

   delay(TC2/2.0 - tau2 - POWER_DELAY - 4.0e-6 - WFG3_START_DELAY - pwco180
         - WFG3_STOP_DELAY - pwd1 
         - gt10 - gstab -2.0e-6 - POWER_DELAY
         - 4.0e-6 - WFG_START_DELAY);

   dec3rgpulse(pwd1,zero,0.0,0.0);

   delay(tau2);

   delay(2.0e-6);
   zgradpulse(gzlvl10,gt10);
   delay(gstab);

   initval(1.0,v4);
   decstepsize(ph_reb);
   dcplrphase(v4);

   decpower(d_reb);

   decshaped_pulse(shreb,pwreb,zero,4.0e-6,0.0);
   dcplrphase(zero);

   decphase(zero); decpower(dhpwr);
   
   delay(2.0e-6);
   zgradpulse(gzlvl10,gt10);
   delay(gstab);

   delay(TC2/2.0 - tau2 - WFG_STOP_DELAY - POWER_DELAY 
         - gt10 - gstab -2.0e-6); 

   decrgpulse(pwc,zero,0.0,0.0);

   dec3rgpulse(pwd1,two,4.0e-6,0.0);

   }

  if(CT_flg[A] == 'y' && n_shift[A] == 'y') {

   dec2phase(t2); delay(2.0e-6);

   dec2rgpulse((pwn-pwc)/2.0,t2,0.0,0.0);
   sim3pulse(0.0e-6,pwc,pwc,zero,t2,t2,0.0,0.0);
   dec2rgpulse((pwn-pwc)/2.0,t2,0.0,0.0);

   decphase(zero);

   delay(tau2);

   decphase(zero);
   decpower(d_co180);
   sim3shaped_pulse(Hshp,co_shp,"hard",pwhshp,pwco180,0.0e-6,zero,zero,zero,4.0e-6,2.0e-6);

   decpower(d_ibca);
   decshaped_pulse(shibca,pwibca,zero,4.0e-6,0.0);
   decphase(zero);

   delay(TC2/2.0 - tau2 - POWER_DELAY - 4.0e-6 - WFG3_START_DELAY - pwco180
         - WFG3_STOP_DELAY - 2.0e-6 - POWER_DELAY - WFG_START_DELAY
         - 4.0e-6 - pwibca - WFG_STOP_DELAY - pwd1 
         - gt10 - gstab -2.0e-6 - POWER_DELAY
         - 4.0e-6 - WFG3_START_DELAY);

   dec3rgpulse(pwd1,zero,0.0,0.0);

   delay(tau2);

   delay(2.0e-6);
   zgradpulse(gzlvl10,gt10);
   delay(gstab);

   initval(1.0,v4);
   decstepsize(ph_reb1);
   dcplrphase(v4);

   decpower(d_reb);

   sim3shaped_pulse("hard",shreb,"hard",0.0e-6,pwreb,2.0*pwn,zero,zero,zero,4.0e-6,0.0);
   dcplrphase(zero);

   decphase(t7); decpower(d_ibca);
   decshaped_pulse(shibcai,pwibca,t7,4.0e-6,0.0);
   decpower(dhpwr); decphase(zero);
   
   delay(2.0e-6);
   zgradpulse(gzlvl10,gt10);
   delay(gstab);

   delay(TC2/2.0 - tau2 - WFG3_STOP_DELAY - POWER_DELAY 
         - 4.0e-6 - WFG_START_DELAY - pwibca - WFG_STOP_DELAY 
         - POWER_DELAY
         - gt10 - gstab -2.0e-6); 

   dec2rgpulse((pwn-pwc)/2.0,zero,0.0,0.0);
   sim3pulse(0.0e-6,pwc,pwc,zero,zero,zero,0.0,0.0);
   dec2rgpulse((pwn-pwc)/2.0,zero,0.0,0.0);

   dec3rgpulse(pwd1,two,4.0e-6,0.0);

   }

   if(CT_flg[A] == 'n' && n_shift[A] == 'n') {

      txphase(one);
      decrgpulse(pwc,t2,0.0,0.0);

      if(c180_flg[A] == 'n')
    {

      decphase(zero);

      /* seduce on */
      decpower(dpwrsed);
      decprgon(codecseq,pwcodec,dressed);
      decon();
      /* seduce on */

      delay(tau2);

      rgpulse(pw,one,0.0,0.0);
      rgpulse(2.0*pw,zero,2.0e-6,0.0);
      rgpulse(pw,one,2.0e-6,0.0);

      dec2rgpulse(2.0*pwn,zero,0.0,0.0);

      delay(tau2); 

      /* seduce off */
      decoff();
      decprgoff();
      decpower(dhpwr);
      /* seduce off */

    }

      else
         decrgpulse(2.0*pwc,zero,4.0e-6,0.0);

      decrgpulse(pwc,zero,4.0e-6,0.0);

   }

   if(CT_flg[A] == 'n' && n_shift[A] == 'y') {

      txphase(one); dec2phase(t2);

      dec2rgpulse((PI-2.0)/PI*(pwn-pwc),t2,2.0e-6,0.0);
      sim3pulse(0.0e-6,pwc,pwc,zero,t2,t2,0.0,0.0);
      dec2rgpulse((2.0/PI)*(pwn-pwc),t2,0.0,0.0);

      if(c180_flg[A] == 'n')
    {

      decphase(zero);

      /* seduce on */
      decpower(dpwrsed);
      decprgon(codecseq,pwcodec,dressed);
      decon();
      /* seduce on */

      delay(tau2);

      rgpulse(pw,one,0.0,0.0);
      rgpulse(2.0*pw,zero,2.0e-6,0.0);
      rgpulse(pw,one,2.0e-6,0.0);

      delay(tau2); 

      /* seduce off */
      decoff();
      decprgoff();      /* note that ca-n evolves ; keep t2,max <= 9.5ms */
      decpower(dhpwr);
      /* seduce off */

    }

      else
         sim3pulse(0.0,2.0*pwc,2.0*pwn,zero,zero,zero,4.0e-6,0.0);

      dec2rgpulse((2.0/PI)*(pwn-pwc),zero,4.0e-6,0.0);
      sim3pulse(0.0e-6,pwc,pwc,zero,zero,zero,0.0,0.0);
      dec2rgpulse((PI-2.0)/PI*(pwn-pwc),zero,0.0,0.0);

   }

   delay(2.0e-6);
   zgradpulse(gzlvl11,gt11);
   delay(gstab);

   lk_sample();

   rgpulse(pw,t8,4.0e-6,0.0);                    /* 90 deg 1H pulse */

   delay(2.0e-6);
   zgradpulse(gzlvl12,gt12);
   delay(2.0e-6);

   decpower(d_ib);

   if(n_shift[A] == 'n') {

   delay(taua - gt12 - 4.0e-6 - WFG2_START_DELAY - POWER_DELAY);
   simshaped_pulse(Hshp,shib,pwhshp,pwib,t8,zero,0.0,0.0);
   decphase(zero);
   }

   else {
 delay(taua - gt12 - 4.0e-6 - WFG3_START_DELAY - POWER_DELAY);                 
 sim3shaped_pulse(Hshp,shib,"hard",pwhshp,pwib,2.0*pwn,t8,zero,zero,0.0,0.0);
    }

   delay(2.0e-6);
   zgradpulse(gzlvl12,gt12);
   delay(2.0e-6);

   if(n_shift[A] == 'n')
     delay(taua - gt12 - 4.0e-6 - WFG2_STOP_DELAY - 2.0*POWER_DELAY);
   else
     delay(taua - gt12 - 4.0e-6 - WFG3_STOP_DELAY - 2.0*POWER_DELAY);

   decpower(dpwr);  /* Set power for decoupling */
   dec2power(dpwr2);  /* Set power for decoupling */

   rgpulse(pw,t8,0.0,rof2);

/* BEGIN ACQUISITION */

status(C);
setreceiver(t9);

}
Example #10
0
pulsesequence()
{

/* DECLARE VARIABLES */

char
        SE[MAXSTR],          /* coherence gradients & sensitivity enhance */
        CT[MAXSTR],                                /* constant time in t1 */
        CCdseq[MAXSTR],
        CChomodec[MAXSTR],          /* Setup for C-imino - C-H6 */

	C13refoc[MAXSTR],                         /* C13 pulse in middle of t1*/
	f1180[MAXSTR],                        /* Flag to start t1 @ halfdwell */
	f2180[MAXSTR];                        /* Flag to start t1 @ halfdwell */

int	icosel,
        ni2 = getval("ni2"),
	t1_counter,
	t2_counter;

double  tau1,                                                /*  t1 delay */
        tau2,                                                /*  t2 delay */
	lambda = 0.94/(4.0*getval("JCH")),        /* 1/4J C-H INEPT delay */
        CTdelay = getval("CTdelay"),     /* total constant time evolution */

        CCdpwr = getval("CCdpwr"),    /*   power level for CC decoupling */
        CCdres = getval("CCdres"),    /*   dres for CC decoupling */
        CCdmf = getval("CCdmf"),      /*   dmf for CC decoupling */

        pwClvl = getval("pwClvl"),              /* coarse power for C13 pulse */
        pwC = getval("pwC"),          /* C13 90 degree pulse length at pwClvl */
	compC = getval("compC"),  /* adjustment for C13 amplifier compression */

        pwNlvl = getval("pwNlvl"),                    /* power for N15 pulses */
        pwN = getval("pwN"),          /* N15 90 degree pulse length at pwNlvl */
        pwZa,                                   /* the largest of 2.0*pw and 2.0
*pwN */

        tpwr = getval("tpwr"),    	               /* power for H1 pulses */
        pw = getval("pw"),               /* H1 90 degree pulse length at tpwr */
	compH = getval("compH"),   /* adjustment for H1 amplifier compression */

	ncyc_cc = getval("ncyc_cc"), /* number of DIPSI3 cycles for CC spinlock */

        tof_75,                  /* tof shifted to 7.5 ppm for H4-N4 transfer */
        tof_12,                   /* tof shifted to 12 ppm for H3-N3 transfer */

	dof_80,		 /* dof shifted to 169 ppm for N3-C4 transfer */
	dof_92p5,		 /* dof shifted to 92.5ppm */

/* p_d is used to calculate the isotropic mixing */
        p_d,                 /* 50 degree pulse for DIPSI-3 at rfdC */
        p_d2,                /* 50 degree pulse for DIPSI-3 at rfd */
        rfd,             /* fine C13 power for 10 kHz rf for 500MHz magnet */

	sw1 = getval("sw1"),
        sw2 = getval("sw2"),
        gstab = getval("gstab"),

        pwHs = getval("pwHs"),         /* H1 90 degree pulse length at tpwrs */
        tpwrs,                   /* power for the pwHs ("rna_H2Osinc") pulse */

        pwHs2 = getval("pwHs2"),       /* H1 90 degree pulse length at tpwrs2 */
        tpwrs2,                           /* power for the pwHs2 square pulse */

        gt1 = getval("gt1"),                   /* coherence pathway gradients */
        gzlvl1 = getval("gzlvl1"),
        gzlvl2 = getval("gzlvl2"),

  gzlvl0 = getval("gzlvl0"),
  gzlvl3 = getval("gzlvl3"),
  gt3 = getval("gt3"),
  gzlvl4 = getval("gzlvl4"),
  gt4 = getval("gt4"),
  gzlvl5 = getval("gzlvl5"),
  gzlvl6 = getval("gzlvl6"),
  gt5 = getval("gt5"),
  gzlvlr = getval("gzlvlr");

    getstr("SE",SE);
    getstr("CT",CT);

  getstr("CChomodec",CChomodec);

  getstr("CCdseq",CCdseq);

  getstr("C13refoc",C13refoc);
  getstr("f1180",f1180);
  getstr("f2180",f2180);


/* LOAD PHASE TABLE */
 
	settable(t1,2,phi1);
	settable(t3,8,phi3);
	settable(t4,16,phi4);
	settable(t9,1,phi9);
	settable(t10,1,phi10);
	settable(t5,4,phi5);
	settable(t11,8,rec1);


/* INITIALIZE VARIABLES */

/* different offset values tof=H2O, dof=110ppm, dof2=200ppm */

	tof_75 = tof + 2.5*sfrq;        /* tof shifted to nH2 */
	tof_12 = tof + 8.0*sfrq;	/* tof shifted to nH */
	dof_92p5 = dof - 17.5*dfrq;	/* dof shifted to C1' */
	dof_80 = dof - 30*dfrq;	        /* dof shifted to C6 */

/* 1.9 kHz DIPSI-3 at 500MHz scaled to this sfrq*/
        p_d = (5.0)/(9.0*4.0*1900.0*(sfrq/500.0));

/* 7 kHz DIPSI-3 at 500MHz scaled to this sfrq*/
        p_d2 = (5.0)/(9.0*4.0*7000.0*(sfrq/500.0));
        ncyc_cc = (int) (ncyc_cc + 0.5);
        if (ncyc_cc > 0 )
         {
           printf("CC-mixing time is %f ms.\n",(ncyc_cc*51.8*4*p_d2));
         }
        if( ncyc_cc > 12 )
         {
           text_error("check C->C dipsi-3 time !! ");
           psg_abort(1);
         }
        initval(ncyc_cc,v2);

/* fine C13 power for dipsi-3 isotropic mixing */
        rfd = (compC*4095.0*pwC*5.0)/(p_d2*9.0);
        rfd = (int) (rfd + 0.5);

/* selective H20 one-lobe sinc pulse */
        tpwrs = tpwr - 20.0*log10(pwHs/(compH*pw*1.69));   /* needs 1.69 times more */
        tpwrs = (int) (tpwrs);                   /* power than a square pulse */

/* selective H20 square pulse */
        tpwrs2 = tpwr - 20.0*log10(pwHs2/(compH*pw));
        tpwrs2 = (int) (tpwrs2);

  if (2.0*pw > 2.0*pwN) pwZa = 2.0*pw;
  else pwZa = 2.0*pwN;

  if ((CT[A]=='y') && (ni2/(4.0*sw2) > CTdelay))
  { text_error( " ni2 is too big. Make ni2 equal to %d or less.\n",
      ((int)(CTdelay*sw2*4.0)) );                                       psg_abort(1); }




/* PHASES AND INCREMENTED TIMES */

/*  Phase incrementation for hypercomplex 2D data, States-Haberkorn element */

    if (phase1 == 2)
         tsadd(t5,1,4);

/* Calculate modifications to phases for States-TPPI acquisition          */

   if( ix == 1) d2_init = d2;
   t1_counter = (int) ( (d2-d2_init)*sw1 + 0.5 );
   if(t1_counter % 2)
        { tsadd(t5,2,4); tsadd(t11,2,4); }

/*  Set up f1180  */

    tau1 = d2;
    if((f1180[A] == 'y') && (ni > 1.0))
        { tau1 += ( 1.0 / (2.0*sw1) ); if(tau1 < 0.2e-6) tau1 = 0.0; }
    tau1 = tau1/2.0;


        icosel=1;

  if (SE[A]=='y')
   {
        if (phase2 == 2)
        {
                tsadd(t10,2,4);
                icosel = -1;
        }
   }

/*  Set up f2180  */
       tau2 = d3;
  if((f2180[A] == 'y') && (ni2 > 1.0))
   {
        tau2 += ( 1.0 / (2.0*sw2) );
        if(tau2 < 0.2e-6) tau2 = 0.0;
   }

        tau2 = tau2/2.0;

/* Calculate modifications to phases for States-TPPI acquisition          */
  if( ix == 1) d3_init = d3;

        t2_counter = (int) ( (d3-d3_init)*sw2 + 0.5 );

  if(t2_counter % 2)
   {
        tsadd(t3,2,4);
        tsadd(t11,2,4);
   }


/* CHECK VALIDITY OF PARAMETER RANGE */


    if( sfrq > 610 )
        { printf("Power Levels at 750/800 MHz may be too high for probe");
          psg_abort(1); }

    if( dpwrf < 4095 )
        { printf("reset dpwrf=4095 and recalibrate C13 90 degree pulse");
          psg_abort(1); }

    if( dpwrf2 < 4095 )
        { printf("reset dpwrf2=4095 and recalibrate N15 90 degree pulse");
          psg_abort(1); }

    if((dm[A] == 'y' || dm[B] == 'y'))
    {
        printf("incorrect dec1 decoupler flag! Should be 'nny' or 'nnn' ");
        psg_abort(1);
    }

    if((dm2[A] == 'y' || dm2[B] == 'y'))
    {
        printf("incorrect dec2 decoupler flags! Should be 'nnn' or 'nny' ");
        psg_abort(1);
    }

    if( ((dm[C] == 'y') && (dm2[C] == 'y') && (at > 0.18)) )
    {
        text_error("check at time! Don't fry probe !! ");
        psg_abort(1);
    }

    if( dpwr > 50 )
    {
        printf("don't fry the probe, DPWR too large!  ");
        psg_abort(1);
    }

   if( dpwr2 > 50 )
    {
        printf("don't fry the probe, DPWR2 too large!  ");
        psg_abort(1);
    }

    if( pw > 20.0e-6 )
    {
        printf("dont fry the probe, pw too high ! ");
        psg_abort(1);
    }

    if( pwC > 40.0e-6 )
    {
        printf("dont fry the probe, pwC too high ! ");
        psg_abort(1);
    }

    if( pwN > 100.0e-6 )
    {
        printf("dont fry the probe, pwN too high ! ");
        psg_abort(1);
    }

    if (gzlvlr > 500 || gzlvlr < -500)
    {
	text_error(" RDt1-gzlvlr must be -500 to 500 (0.5G/cm) \n");
	psg_abort(1);
    }

/* BEGIN ACTUAL PULSE SEQUENCE */

status(A);

        obspower(tpwr);
	obsstepsize(0.5);
        decpower(pwClvl);
	decstepsize(0.5);
	obsoffset(tof);
        dec2power(pwNlvl);
	dec2stepsize(0.5);

        decoffset(dof_80);	/* Preset the carbon frequency for the C1' carbons */

        txphase(zero);
        decphase(zero);
        dec2phase(zero);

        delay(d1);
        rcvroff();

        dec2rgpulse(pwN, zero, 0.0, 0.0);  /*destroy N15 and C13 magnetization*/
        decrgpulse(pwC, zero, 0.0, 0.0);
        zgradpulse(gzlvl0, 0.5e-3);
        delay(1.0e-4);
        dec2rgpulse(pwN, one, 0.0, 0.0);
        decrgpulse(pwC, one, 0.0, 0.0);
        zgradpulse(0.7*gzlvl0, 0.5e-3);
        delay(5.0e-4);

	delay(lambda);

	simpulse(2*pw, 2*pwC, zero, zero, 0.0, 0.0);
	dec2phase(t5);

	delay(lambda - SAPS_DELAY);

	simpulse(pw, pwC, zero, t5, 0.0, 0.0); /* 2x, -2x*/
	dec2phase(zero);
        txphase(one);

	zgradpulse(gzlvl5,gt5);
	delay(lambda - SAPS_DELAY - gt5);

	simpulse(2*pw, 2*pwC, one, zero, 0.0, 0.0);

	zgradpulse(gzlvl5,gt5);
        delay(lambda - 2*SAPS_DELAY - gt5 - 2*POWER_DELAY);


	decpwrf(4095.0);


	txphase(zero);
	decphase(zero);

  if (C13refoc[A]=='y')
   {

        if (tau1 > (2.0*GRADIENT_DELAY + pwN + 0.64*pw + 5.0*SAPS_DELAY))
        {
        zgradpulse(gzlvlr, 0.8*(tau1 - 2.0*GRADIENT_DELAY - pwN - 0.64*pw));
        delay(0.2*(tau1 - 2.0*GRADIENT_DELAY - pwN - 0.64*pw) - SAPS_DELAY);
        sim3pulse(2.0*pw, 0.0, 2.0*pwN, zero, zero, zero, 0.0, 0.0);
        zgradpulse(-1.0*gzlvlr, 0.8*(tau1 - 2.0*GRADIENT_DELAY - pwN - 0.64*pw));
        delay(0.2*(tau1 - 2.0*GRADIENT_DELAY - pwN - 0.64*pw));
        }
        else if (tau1 > (0.64*pw + 0.5*SAPS_DELAY))
        delay(2.0*tau1 - 2.0*0.64*pw - SAPS_DELAY );
   }
  else
   {
        if (tau1 > (2.0*GRADIENT_DELAY + pwN + 0.64*pw + 5.0*SAPS_DELAY))
        {
        zgradpulse(gzlvlr, 0.8*(tau1 - 2.0*GRADIENT_DELAY - pwN - 0.64*pw));
        delay(0.2*(tau1 - 2.0*GRADIENT_DELAY - pwN - 0.64*pw) - SAPS_DELAY);
        dec2rgpulse(2.0*pwN, zero, 0.0, 0.0);
        zgradpulse(-1.0*gzlvlr, 0.8*(tau1 - 2.0*GRADIENT_DELAY - pwN - 0.64*pw));
        delay(0.2*(tau1 - 2.0*GRADIENT_DELAY - pwN - 0.64*pw));
        }
        else if (tau1 > (0.64*pw + 0.5*SAPS_DELAY))
        delay(2.0*tau1 - 2.0*0.64*pw - SAPS_DELAY );
   }


	decrgpulse(pwC,three,0.0,0.0);   /* flip transferred 13C-magn. to z */
	decrgpulse(pwC,one,0.0,0.0);   /* flip transferred 13C-magn. to z */

        decphase(zero);
        decpwrf(rfd);

        starthardloop(v2);
    decrgpulse(6.4*p_d2,zero,0.0,0.0);
    decrgpulse(8.2*p_d2,two,0.0,0.0);
    decrgpulse(5.8*p_d2,zero,0.0,0.0);
    decrgpulse(5.7*p_d2,two,0.0,0.0);
    decrgpulse(0.6*p_d2,zero,0.0,0.0);
    decrgpulse(4.9*p_d2,two,0.0,0.0);
    decrgpulse(7.5*p_d2,zero,0.0,0.0);
    decrgpulse(5.3*p_d2,two,0.0,0.0);
    decrgpulse(7.4*p_d2,zero,0.0,0.0);

    decrgpulse(6.4*p_d2,two,0.0,0.0);
    decrgpulse(8.2*p_d2,zero,0.0,0.0);
    decrgpulse(5.8*p_d2,two,0.0,0.0);
    decrgpulse(5.7*p_d2,zero,0.0,0.0);
    decrgpulse(0.6*p_d2,two,0.0,0.0);
    decrgpulse(4.9*p_d2,zero,0.0,0.0);
    decrgpulse(7.5*p_d2,two,0.0,0.0);
    decrgpulse(5.3*p_d2,zero,0.0,0.0);
    decrgpulse(7.4*p_d2,two,0.0,0.0);

    decrgpulse(6.4*p_d2,two,0.0,0.0);
    decrgpulse(8.2*p_d2,zero,0.0,0.0);
    decrgpulse(5.8*p_d2,two,0.0,0.0);
    decrgpulse(5.7*p_d2,zero,0.0,0.0);
    decrgpulse(0.6*p_d2,two,0.0,0.0);
    decrgpulse(4.9*p_d2,zero,0.0,0.0);
    decrgpulse(7.5*p_d2,two,0.0,0.0);
    decrgpulse(5.3*p_d2,zero,0.0,0.0);
    decrgpulse(7.4*p_d2,two,0.0,0.0);

    decrgpulse(6.4*p_d2,zero,0.0,0.0);
    decrgpulse(8.2*p_d2,two,0.0,0.0);
    decrgpulse(5.8*p_d2,zero,0.0,0.0);
    decrgpulse(5.7*p_d2,two,0.0,0.0);
    decrgpulse(0.6*p_d2,zero,0.0,0.0);
    decrgpulse(4.9*p_d2,two,0.0,0.0);
    decrgpulse(7.5*p_d2,zero,0.0,0.0);
    decrgpulse(5.3*p_d2,two,0.0,0.0);
    decrgpulse(7.4*p_d2,zero,0.0,0.0);
        endhardloop();


	decphase(t3);

        decpwrf(4095.0);

        decrgpulse(pwC,three,0.0,0.0);  /* flip transferred 13C-magnetization to z */
        decoffset(dof_92p5);	/* Preset the carbon frequency for the C1' carbon */

	decrgpulse(pwC,t3,0.0,0.0);  /* 4x,-4x  flip transferred 13C-magnetization to x */


if (SE[A]=='y') 
{
 /*****************     CONSTANT TIME EVOLUTION      *****************/
      if (CT[A]=='y') {
     /***************/

        initval(90.0, v9);
        decstepsize(1.0);
        dcplrphase(v9);
        decphase(t9);
        delay(CTdelay/2.0 - tau2);

    decrgpulse(2.0*pwC, t9, 0.0, 0.0);
    dcplrphase(zero);
    decphase(t10);

          if (tau2 < gt1 + gstab)
               {delay(CTdelay/2.0 - pwZa - gt1 - gstab);
                 zgradpulse(icosel*gzlvl1, gt1);        /* 2.0*GRADIENT_DELAY */
                delay(gstab - 2.0*GRADIENT_DELAY);
                sim3pulse(2.0*pw, 0.0, 2.0*pwN, zero, zero, zero, 0.0, 0.0);
                delay(tau2);}

          else {delay(CTdelay/2.0 - pwZa);
                sim3pulse(2.0*pw, 0.0, 2.0*pwN, zero, zero, zero, 0.0, 0.0);
                delay(tau2 - gt1 - gstab);
                 zgradpulse(icosel*gzlvl1, gt1);        /* 2.0*GRADIENT_DELAY */
                delay(gstab - 2.0*GRADIENT_DELAY);}


     /***************/
                      }
     /********************************************************************/

     /*****************         NORMAL EVOLUTION         *****************/
      else            {
     /***************/

if (CChomodec[A]=='y')

    {
    decpower(CCdpwr); decphase(zero);
    decprgon(CCdseq,1.0/CCdmf,CCdres);
    decon();  /* CC decoupling on */
    }

decphase(zero);
delay(tau2);

         sim3pulse(2.0*pw, 0.0, 2.0*pwN, zero, zero, zero, 0.0, 0.0);

         decphase(t9);
         delay(gt1 + gstab - pwZa);
         delay(tau2);

if 	(CChomodec[A]=='y')
        {
        decoff(); decprgoff();        /* CC decoupling off */
        decpower(pwClvl);
        }

         decrgpulse(2.0*pwC, t9, 0.0, 0.0);

          zgradpulse(icosel*gzlvl1, gt1);               /* 2.0*GRADIENT_DELAY */
         decphase(t10);
         delay(gstab - 2.0*GRADIENT_DELAY);


     /***************/
                      }
     /********************************************************************/

/*  xxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxx  */

        decrgpulse(pwC, zero, 0.0, 0.0);

        decphase(zero);
        zgradpulse(gzlvl5, gt5);
        delay(lambda - 0.5*pwC - gt5);

        simpulse(2.0*pw, 2.0*pwC, zero, zero, 0.0, 0.0);

        zgradpulse(gzlvl5, gt5);
        txphase(one);
        decphase(t10);
        delay(lambda  - 0.5*pwC - gt5);

        simpulse(pw, pwC, one, t10, 0.0, 0.0);

        txphase(zero);
        decphase(zero);
        zgradpulse(gzlvl6, gt5);
        delay(lambda - 0.5*pwC - gt5);

        simpulse(2.0*pw, 2.0*pwC, zero, zero, 0.0, 0.0);
        txphase(two);
        zgradpulse(gzlvl6, gt5);
        delay(lambda - 0.5*pwC - gt5);

        simpulse(pw, pwC, two, zero, 0.0, 0.0);
        txphase(zero);
        delay(lambda - 0.5*pwC);

        simpulse(2.0*pw, 2.0*pwC, zero, zero, 0.0, 0.0);

        dcplrphase(zero);                                       /* SAPS_DELAY */
        zgradpulse(gzlvl2, gt1/4.0);                   /* 2.0*GRADIENT_DELAY */
        delay(lambda - gt1/4.0 - 0.5*pwC - 2.0*GRADIENT_DELAY - 2*POWER_DELAY - SAPS_DELAY);

}

else
{
        decphase(zero);
        zgradpulse(gzlvl5,gt5);

        delay(lambda - gt5);
        simpulse(2*pw,2*pwC,zero,zero,0.0,0.0);
        zgradpulse(gzlvl5,gt5);
        delay(lambda - gt5);

	decrgpulse(pwC,zero,0.0,0.0);

	zgradpulse(gzlvl3,gt3);
	delay(gstab);

        obspower(tpwrs);
        shaped_pulse("rna_H2Osinc", pwHs, zero, 5.0e-4, 0.0);
        obspower(tpwr);

	rgpulse(pw, zero, 2*rof1, 0.0);
	txphase(two);
	obspower(tpwrs2);
	
	zgradpulse(gzlvl4,gt4);
        delay(gstab - 2*SAPS_DELAY - 2*POWER_DELAY - GRADIENT_DELAY);

        rgpulse((lambda-gstab-gt4-pwC), two, 0.0, 0.0);
        simpulse(pwC,pwC,two,three,0.0,0.0);
        simpulse(2*pwC,2*pwC,two,zero,0.0,0.0);
        simpulse(pwC,pwC,two,three,0.0,0.0);
        rgpulse((pwHs2-2*pwC-(lambda-gstab-gt4-pwC)), two, 0.0, 0.0);

        txphase(zero);
        obspower(tpwr);
        rgpulse(2*pw, zero, 0.0, 0.0);
        obspower(tpwrs2);

        rgpulse(pwHs2, two, 4.0e-6, 0.0);
        decphase(t4);

        zgradpulse(gzlvl4,gt4);
        delay(gstab-2*pwC-2*SAPS_DELAY - POWER_DELAY - GRADIENT_DELAY);

        decrgpulse(pwC,t4,0.0,0.0);
        decrgpulse(pwC,zero,0.0,0.0);
}
        dec2power(dpwr2);               /* 2*POWER_DELAY */
        decpower(dpwr);

status(C);

 setreceiver(t11);
}
Example #11
0
pulsesequence() {

// Define Variables and Objects and Get Parameter Values

   CP hx = getcp("HX",0.0,0.0,0,1);
   strncpy(hx.fr,"dec",3);
   strncpy(hx.to,"obs",3);
   putCmd("frHX='dec'\n");
   putCmd("toHX='obs'\n");

   MPSEQ c7 = getpostc7("c7X",0,0.0,0.0,0,1);
   MPSEQ c7ref = getpostc7("c7X",c7.iSuper,c7.phAccum,c7.phInt,1,1);
   strncpy(c7.ch,"obs",3);
   putCmd("chXc7='obs'\n");

   DSEQ dec = getdseq("H");
   strncpy(dec.t.ch,"dec",3);
   putCmd("chHtppm='dec'\n"); 
   strncpy(dec.s.ch,"dec",3);
   putCmd("chHspinal='dec'\n");

// Set Constant-time Period for d2. 

   if (d2_index == 0) d2_init = getval("d2");
   double d2_ = (ni - 1)/sw1 + d2_init;
   putCmd("d2acqret = %f\n",roundoff(d2_,12.5e-9));
   putCmd("d2dwret = %f\n",roundoff(1.0/sw1,12.5e-9));

//--------------------------------------
// Copy Current Parameters to Processed
//-------------------------------------

   putCmd("groupcopy('current','processed','acquisition')");

// Dutycycle Protection

   DUTY d = init_dutycycle();
   d.dutyon = getval("pwH90") + getval("tHX") + 2.0* getval("pwX90") + c7.t + c7ref.t;
   d.dutyoff = d1 + 4.0e-6 + 2.0*getval("tZF");
   d.c1 = d.c1 + (!strcmp(dec.seq,"tppm"));
   d.c1 = d.c1 + ((!strcmp(dec.seq,"tppm")) && (dec.t.a > 0.0));
   d.t1 = d2_ +  getval("rd") + getval("ad") + at;
   d.c2 = d.c2 + (!strcmp(dec.seq,"spinal"));
   d.c2 = d.c2 + ((!strcmp(dec.seq,"spinal")) && (dec.s.a > 0.0));
   d.t2 = d2_ +  getval("rd") + getval("ad") + at;
   d = update_dutycycle(d);
   abort_dutycycle(d,10.0);

// Set Phase Tables

   settable(phH90,4,table1);
   settable(phXhx,4,table2);
   settable(phHhx,4,table3);
   settable(phXmix1,4,table4);
   settable(phXmix2,4,table5);
   settable(phRec,4,table6);

// Add STATES-TPPI (STATES + "FAD")

   double obsstep = 360.0/(PSD*8192);
   if (phase1 == 2)
      initval((45.0/obsstep),v1);
   else
      initval(0.0,v1);

   initval((d2*c7.of[0]*360.0/obsstep),v2);
   obsstepsize(obsstep);
   setreceiver(phRec);

// Begin Sequence

   txphase(phXhx); decphase(phH90);
   obspwrf(getval("aXhx")); decpwrf(getval("aH90")); 
   obsunblank(); decunblank(); _unblank34();
   delay(d1);
   sp1on(); delay(2.0e-6); sp1off(); delay(2.0e-6);

// H to X Cross Polarization

   decrgpulse(getval("pwH90"),phH90,0.0,0.0);
   decphase(phHhx);
    _cp_(hx,phHhx,phXhx);
   obspwrf(getval("aX90"));

// Mixing with C7 Recoupling-Period One

   rgpulse(getval("pwX90"),phXmix1,0.0,0.0);
   obspwrf(getval("aXc7"));
   decoff();
   xmtrphase(v1); txphase(phXmix1);
   delay(getval("tZF"));
   decpwrf(getval("aHmix"));
   decunblank();
   decon();
   _mpseq(c7, phXmix1);
   decoff();

// F1 Indirect Period For X

   xmtrphase(v2); txphase(phXmix2);
   _dseqon(dec);
   delay(d2);
   _dseqoff(dec);

// Mixing with C7 Recoupling-Period Two

   decpwrf(getval("aHmix"));
   decunblank();
   decon();
   _mpseq(c7ref, phXmix2);
   decoff();
   obspwrf(getval("aX90"));
   xmtrphase(zero); txphase(phXmix2);
   delay(getval("tZF"));
   rgpulse(getval("pwX90"),phXmix2,0.0,0.0);

// Begin Acquisition

   _dseqon(dec);
   obsblank(); _blank34();
   delay(getval("rd"));
   startacq(getval("ad"));
   acquire(np, 1/sw);
   endacq();
   _dseqoff(dec);
   obsunblank(); decunblank(); _unblank34();
}
Example #12
0
pulsesequence()
{

    /* DECLARE AND LOAD VARIABLES */

    char        f1180[MAXSTR],   		      /* Flag to start t1 @ halfdwell */
                mag_flg[MAXSTR],      /* magic-angle coherence transfer gradients */
                C13refoc[MAXSTR],		/* C13 sech/tanh pulse in middle of t1*/
                NH2only[MAXSTR],		       /* spectrum of only NH2 groups */
                amino[MAXSTR],                     /* select amino nitrogens      */
                imino[MAXSTR],                     /* select imino nitrogens      */
                T1[MAXSTR],				/* insert T1 relaxation delay */
                T1rho[MAXSTR],		     /* insert T1rho relaxation delay */
                T2[MAXSTR],				/* insert T2 relaxation delay */
                bottom[MAXSTR],
                right[MAXSTR],
                TROSY[MAXSTR];			    /* do TROSY on N15 and H1 */

    int         icosel,          			  /* used to get n and p type */
                t1_counter,  		        /* used for states tppi in t1 */
                rTnum,			/* number of relaxation times, relaxT */
                rTcounter;		    /* to obtain maximum relaxT, ie relaxTmax */

    double      tau1,         				         /*  t1 delay */
                lambda = 0.91/(4.0*getval("JNH")), 	   /* 1/4J H1 evolution delay */
                tNH = 1.0/(4.0*getval("JNH")),	  /* 1/4J N15 evolution delay */
                relaxT = getval("relaxT"),		     /* total relaxation time */
                rTarray[1000], 	    /* to obtain maximum relaxT, ie relaxTmax */
                maxrelaxT = getval("maxrelaxT"),    /* maximum relaxT in all exps */
                ncyc,			 /* number of pulsed cycles in relaxT */

                /* the sech/tanh pulse is automatically calculated by the macro "rna_cal", */  /* and is called directly from your shapelib.                  		      */
                pwClvl = getval("pwClvl"), 	  	        /* coarse power for C13 pulse */
                pwC = getval("pwC"),     	      /* C13 90 degree pulse length at pwClvl */
                rfC,            	          /* maximum fine power when using pwC pulses */
                rfst,	                       /* fine power for the rna_stC140 pulse */
                /* temporary Pbox parameters */
                bw, pws, ofs, ppm, nst,     /* bandwidth, pulsewidth, offset, ppm, # steps */

                compH = getval("compH"),        /* adjustment for H1 amplifier compression */
                compN = getval("compN"),       /* adjustment for N15 amplifier compression */
                compC = getval("compC"),       /* adjustment for C13 amplifier compression */

                calH = getval("calH"), /* multiplier on a pw pulse for H1 calibration */
                pwHs = getval("pwHs"),	        /* H1 90 degree pulse length at tpwrs */
                tpwrs,	  	              /* power for the pwHs ("H2Osinc") pulse */

                pwNlvl = getval("pwNlvl"),	              /* power for N15 pulses */
                pwN = getval("pwN"),          /* N15 90 degree pulse length at pwNlvl */
                calN = getval("calN"),   /* multiplier on a pwN pulse for calibration */
                slNlvl,					   /* power for N15 spin lock */
                slNrf = 1500.0,        /* RF field in Hz for N15 spin lock at 600 MHz */
                dof2a,                                      /* offset for imino/amino */

                sw1 = getval("sw1"),

                gt1 = getval("gt1"),  		       /* coherence pathway gradients */
                gzcal = getval("gzcal"),               /* dac to G/cm conversion      */
                gzlvl1 = getval("gzlvl1"),
                gzlvl2 = getval("gzlvl2"),

                BPpwrlimits,                    /*  =0 for no limit, =1 for limit */

                gt0 = getval("gt0"),				   /* other gradients */
                gt3 = getval("gt3"),
                gt4 = getval("gt4"),
                gt5 = getval("gt5"),
                gzlvl0 = getval("gzlvl0"),
                gzlvl3 = getval("gzlvl3"),
                gzlvl4 = getval("gzlvl4"),
                gzlvl5 = getval("gzlvl5");

    P_getreal(GLOBAL,"BPpwrlimits",&BPpwrlimits,1);
    getstr("f1180",f1180);
    getstr("mag_flg",mag_flg);
    getstr("C13refoc",C13refoc);
    getstr("NH2only",NH2only);
    getstr("T1",T1);
    getstr("T1rho",T1rho);
    getstr("T2",T2);
    getstr("bottom",bottom);
    getstr("right",right);
    getstr("TROSY",TROSY);
    getstr("imino",imino);
    getstr("amino",amino);



    /*   LOAD PHASE TABLE    */

    settable(t3,2,phi3);
    if (TROSY[A]=='y')
    {   settable(t1,1,ph_x);

        if (bottom[A]=='y')
            settable(t4,1,phx);
        else
            settable(t4,1,ph_x);
        if (right[A]=='y')
            settable(t10,1,phy);
        else
            settable(t10,1,ph_y);

        settable(t9,1,phx);
        settable(t11,1,phx);
        settable(t12,2,recT);
    }
    else
    {   settable(t1,1,phx);
        settable(t4,1,phx);
        settable(t9,8,phi9);
        settable(t10,1,phx);
        settable(t11,1,phy);
        settable(t12,4,rec);
    }



    /*   INITIALIZE VARIABLES   */
    dof2a=dof2;
    /* IMINO-region setting of dof2 */
    if (imino[A] == 'y') dof2a=dof2-45*dfrq2;
    if (amino[A] == 'y') dof2a=dof2-115*dfrq2;
    if ((imino[A] == 'n') && (amino[A] == 'n')) dof2a=dof2;

    /* maximum fine power for pwC pulses (and initialize rfst) */
    rfC = 4095.0;
    rfst=0.0;


    setautocal();                        /* activate auto-calibration flags */

    if (autocal[0] == 'n')
    {
        /* 180 degree adiabatic C13 pulse covers 140 ppm */
        if (C13refoc[A]=='y')
        {   rfst = (compC*4095.0*pwC*4000.0*sqrt((21.0*sfrq/600.0+7.0)/0.35));
            rfst = (int) (rfst + 0.5);
            if ( 1.0/(4000.0*sqrt((21.0*sfrq/600.0+7.0)/0.35)) < pwC )
            {   text_error( " Not enough C13 RF. pwC must be %f usec or less.\n",
                            (1.0e6/(4000.0*sqrt((21.0*sfrq/600.0+7.0)/0.35))) );
                psg_abort(1);
            }
        }

        /* selective H20 one-lobe sinc pulse */
        tpwrs = tpwr - 20.0*log10(pwHs/(compH*pw*1.69));   /*needs 1.69 times more*/
        tpwrs = (int) (tpwrs);                   	  /*power than a square pulse */
    }
    else        /* if autocal = 'y'(yes), 'q'(quiet), r(read), or 's'(semi) */
    {
        if(FIRST_FID)                                            /* call Pbox */
        {
            ppm = getval("dfrq");
            bw = 140.0*ppm;
            pws = 0.001;
            ofs = 0.0;
            nst = 1000.0;
            if (C13refoc[A]=='y')
                stC140 = pbox_makeA("rna_stC140", "sech", bw, pws, ofs, compC*pwC, pwClvl, nst);
            H2Osinc = pbox_Rsh("rna_H2Osinc", "sinc90", pwHs, 0.0, compH*pw, tpwr);
            if (dm3[B] == 'y') H2ofs = 3.2;
            ofs_check(H1ofs, C13ofs, N15ofs, H2ofs);
        }
        if (C13refoc[A]=='y') rfst = stC140.pwrf;
        pwHs = H2Osinc.pw;
        tpwrs = H2Osinc.pwr;
    }

    /* power level for N15 spinlock (90 degree pulse length calculated first) */
    slNlvl = 1/(4.0*slNrf*sfrq/600.0) ;
    slNlvl = pwNlvl - 20.0*log10(slNlvl/(pwN*compN));
    slNlvl = (int) (slNlvl + 0.5);

    /* use 1/8J times for relaxation measurements of NH2 groups */
    if ( (NH2only[A]=='y') && ((T1[A]=='y') || (T1rho[A]=='y') || (T2[A]=='y')) )
    {
        tNH = tNH/2.0;
    }

    /* reset calH and calN for 2D if inadvertently left at 2.0 */
    if (ni>1.0) {
        calH=1.0;
        calN=1.0;
    }



    /* CHECK VALIDITY OF PARAMETER RANGES */

    if ( ((imino[A] == 'y') && (amino[A] == 'y')) )
    {
        printf(" Choose ONE of the cases: imino='y' OR amino='y' ");
        psg_abort(1);
    }

    if ( ((imino[A] == 'y') && (NH2only[A] == 'y')) )
    {
        printf(" NH2only='y' only valide for  amino='y' ");
        psg_abort(1);
    }

    if ((TROSY[A]=='y') && (gt1 < -2.0e-4 + pwHs + 1.0e-4 + 2.0*POWER_DELAY))
    {   text_error( " gt1 is too small. Make gt1 equal to %f or more.\n",
                    (-2.0e-4 + pwHs + 1.0e-4 + 2.0*POWER_DELAY) );
        psg_abort(1);
    }

    if((dm[A] == 'y' || dm[B] == 'y' || dm[C] == 'y' ))
    {
        text_error("incorrect dec1 decoupler flags! Should be 'nnn' ");
        psg_abort(1);
    }

    if((dm2[A] == 'y' || dm2[B] == 'y'))
    {
        text_error("incorrect dec2 decoupler flags! Should be 'nny' ");
        psg_abort(1);
    }

    if( dpwr2 > 50 )
    {
        text_error("don't fry the probe, DPWR2 too large!  ");
        psg_abort(1);
    }

    if( pw > 50.0e-6 )
    {
        text_error("dont fry the probe, pw too high ! ");
        psg_abort(1);
    }

    if( (pwN > 100.0e-6) && (pwNlvl > 54) )
    {
        text_error("dont fry the probe, pwN too high ! ");
        psg_abort(1);
    }



    /*  RELAXATION TIMES AND FLAGS */

    /* evaluate maximum relaxT, relaxTmax chosen by the user */
    rTnum = getarray("relaxT", rTarray);
    relaxTmax = rTarray[0];
    for (rTcounter=1; rTcounter<rTnum; rTcounter++)
        if (relaxTmax < rTarray[rTcounter]) relaxTmax = rTarray[rTcounter];


    /* compare relaxTmax with maxrelaxT */
    if (maxrelaxT > relaxTmax)  relaxTmax = maxrelaxT;




    if ( ((T1rho[A]=='y') || (T2[A]=='y')) && (relaxTmax > d1) )
    {
        text_error("Maximum relaxation time, relaxT, is greater than d1 ! ");
        psg_abort(1);
    }

    if ( ((T1[A]=='y') && (T1rho[A]=='y'))   ||   ((T1[A]=='y') && (T2[A]=='y')) ||
            ((T1rho[A]=='y') && (T2[A]=='y')) )
    {
        text_error("Choose only one relaxation measurement ! ");
        psg_abort(1);
    }


    if ( ((T1[A]=='y') || (T1rho[A]=='y')) &&
            ((relaxT*100.0 - (int)(relaxT*100.0+1.0e-4)) > 1.0e-6) )
    {
        text_error("Relaxation time, relaxT, must be zero or multiple of 10msec");
        psg_abort(1);
    }


    if ( (T2[A]=='y') &&
            (((relaxT+0.01)*50.0 - (int)((relaxT+0.01)*50.0+1.0e-4)) > 1.0e-6) )
    {
        text_error("Relaxation time, relaxT, must be odd multiple of 10msec");
        psg_abort(1);
    }

    if ( ((T1rho[A]=='y') || (T2[A]=='y'))  &&  (relaxTmax > 0.25) && (ix==1) )
    {
        printf("WARNING, sample heating may result in a reduced lock level for relaxT>0.25sec");
    }


    if ( ((T1rho[A]=='y') ||  (T2[A]=='y'))  &&  (relaxTmax > 0.5) )
    {
        text_error("relaxT greater than 0.5 seconds will heat sample");
        psg_abort(1);
    }


    if ( ((NH2only[A]=='y') || (T1[A]=='y') || (T1rho[A]=='y') || (T2[A]=='y'))
            &&  (TROSY[A]=='y') )
    {
        text_error("TROSY not implemented with NH2 spectrum, or relaxation exps.");
        psg_abort(1);
    }


    if ((TROSY[A]=='y') && (dm2[C] == 'y'))
    {
        text_error("Choose either TROSY='n' or dm2='nnn' ! ");
        psg_abort(1);
    }


    /* PHASES AND INCREMENTED TIMES */

    /*  Phase incrementation for hypercomplex 2D data, States-Haberkorn element */

    if (TROSY[A]=='y')
    {   if (phase1 == 1)   				      icosel = -1;
        else 	  {
            tsadd(t4,2,4);
            tsadd(t10,2,4);
            icosel = +1;
        }
    }
    else {
        if (phase1 == 1)  {
            tsadd(t10,2,4);
            icosel = +1;
        }
        else 			       icosel = -1;
    }


    /*  Set up f1180  */

    tau1 = d2;
    if((f1180[A] == 'y') && (ni > 1.0))
    {
        tau1 += ( 1.0 / (2.0*sw1) );
        if(tau1 < 0.2e-6) tau1 = 0.0;
    }
    tau1 = tau1/2.0;



    /* Calculate modifications to phases for States-TPPI acquisition          */

    if( ix == 1) d2_init = d2;
    t1_counter = (int) ( (d2-d2_init)*sw1 + 0.5 );
    if(t1_counter % 2)
    {
        tsadd(t3,2,4);
        tsadd(t12,2,4);
    }



    /*  Correct inverted signals for NH2 only spectra  */

    if ((NH2only[A]=='y') && (T1[A]=='n')  &&  (T1rho[A]=='n')  && (T2[A]=='n'))
    {
        tsadd(t3,2,4);
    }



    /* BEGIN PULSE SEQUENCE */

    status(A);

    obspower(tpwr);
    decpower(pwClvl);
    decpwrf(rfC);
    dec2power(pwNlvl);
    dec2offset(dof2a);
    txphase(zero);
    decphase(zero);
    dec2phase(zero);

    delay(d1);


    /*  xxxxxxxxxxxxxxxxx  CONSTANT SAMPLE HEATING FROM N15 RF xxxxxxxxxxxxxxxxx  */

    if  (T1rho[A]=='y')
    {   dec2power(slNlvl);
        dec2rgpulse(relaxTmax-relaxT, zero, 0.0, 0.0);
        dec2power(pwNlvl);
    }

    if  (T2[A]=='y')
    {   ncyc = 8.0*100.0*(relaxTmax - relaxT);
        if (BPpwrlimits > 0.5)
        {
            dec2power(pwNlvl-3.0);    /* reduce for probe protection */
            pwN=pwN*compN*1.4;
        }
        if (ncyc > 0)
        {   initval(ncyc,v1);
            loop(v1,v2);
            delay(0.625e-3 - pwN);
            dec2rgpulse(2*pwN, zero, 0.0, 0.0);
            delay(0.625e-3 - pwN);
            endloop(v2);
        }
        if (BPpwrlimits > 0.5)
        {
            dec2power(pwNlvl);         /* restore normal value */
            pwN=getval("pwN");
        }
    }
    /*  xxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxx  */
    rcvroff();
    if (TROSY[A]=='n')    dec2rgpulse(pwN, zero, 0.0, 0.0);
    decrgpulse(pwC, zero, 0.0, 0.0);   /*destroy N15 and C13 magnetization*/
    zgradpulse(gzlvl0, 0.5e-3);
    delay(1.0e-4);
    if (TROSY[A]=='n')    dec2rgpulse(pwN, one, 0.0, 0.0);
    decrgpulse(pwC, one, 0.0, 0.0);
    zgradpulse(0.7*gzlvl0, 0.5e-3);
    decpwrf(rfst);
    txphase(t1);
    delay(5.0e-4);

    if(dm3[B] == 'y')				  /*optional 2H decoupling on */
    {   lk_hold();
        dec3unblank();
        dec3rgpulse(1/dmf3, one, 0.0, 0.0);
        dec3unblank();
        setstatus(DEC3ch, TRUE, 'w', FALSE, dmf3);
    }

    rgpulse(calH*pw,t1,0.0,0.0);                 /* 1H pulse excitation */

    txphase(zero);
    dec2phase(zero);
    zgradpulse(gzlvl0, gt0);
    delay(lambda - gt0);

    sim3pulse(2.0*pw, 0.0, 2.0*pwN, zero, zero, zero, 0.0, 0.0);

    txphase(one);
    zgradpulse(gzlvl0, gt0);
    delay(lambda - gt0);

    rgpulse(pw, one, 0.0, 0.0);
    txphase(two);
    obspower(tpwrs);
    shaped_pulse("rna_H2Osinc", pwHs, two, 5.0e-5, 0.0);
    obspower(tpwr);
    zgradpulse(gzlvl3, gt3);
    dec2phase(t3);
    delay(2.0e-4);
    dec2rgpulse(calN*pwN, t3, 0.0, 0.0);
    txphase(zero);
    decphase(zero);

    /*  xxxxxxxxxxxxxxxxxx    OPTIONS FOR N15 RELAXATION    xxxxxxxxxxxxxxxxxxxx  */

    if ( (T1[A]=='y') || (T1rho[A]=='y') || (T2[A]=='y') )
    {
        dec2phase(one);
        zgradpulse(gzlvl4, gt4);				/* 2.0*GRADIENT_DELAY */
        delay(tNH - gt4 - 2.0*GRADIENT_DELAY);

        sim3pulse(2.0*pw, 0.0, 2.0*pwN, zero, zero, one, 0.0, 0.0);

        zgradpulse(gzlvl4, gt4);				/* 2.0*GRADIENT_DELAY */
        delay(tNH - gt4 - 2.0*GRADIENT_DELAY);
    }

    /*   xxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxx    */

    if  (T1[A]=='y')
    {
        dec2rgpulse(pwN, one, 0.0, 0.0);
        dec2phase(three);

        zgradpulse(gzlvl0, gt0);				/* 2.0*GRADIENT_DELAY */
        delay(2.5e-3 - gt0 - 2.0*GRADIENT_DELAY - pw);
        rgpulse(2.0*pw, zero, 0.0, 0.0);
        delay(2.5e-3 - pw);

        ncyc = (100.0*relaxT);
        initval(ncyc,v4);
        if (ncyc > 0)
        {   loop(v4,v5);

            delay(2.5e-3 - pw);
            rgpulse(2.0*pw, two, 0.0, 0.0);
            delay(2.5e-3 - pw);

            delay(2.5e-3 - pw);
            rgpulse(2.0*pw, zero, 0.0, 0.0);
            delay(2.5e-3 - pw);

            endloop(v5);
        }

        dec2rgpulse(pwN, three, 0.0, 0.0);
    }

    /*   xxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxx    */

    /* Theory suggests 8.0 is better than 2PI as RF  */
    /* field multiplier and experiment confirms this.*/
    if  (T1rho[A]=='y')          /* Shift evolution of 2.0*pwN/PI for one pulse   */
    {   /* at end left unrefocused as for normal sequence*/
        delay(1.0/(8.0*slNrf) - pwN);
        decrgpulse(pwN, zero, 0.0, 0.0);
        dec2power(slNlvl);
        /* minimum 5ms spinlock to dephase */
        dec2rgpulse((2.5e-3-pw), zero, 0.0, 0.0);	         /*  spins not locked */
        sim3pulse(2.0*pw, 0.0, 2.0*pw, zero, zero, zero, 0.0, 0.0);
        dec2rgpulse((2.5e-3-pw), zero, 0.0, 0.0);

        ncyc = 100.0*relaxT;
        initval(ncyc,v4);
        if (ncyc > 0)
        {   loop(v4,v5);
            dec2rgpulse((2.5e-3-pw), zero, 0.0, 0.0);
            sim3pulse(2.0*pw, 0.0, 2.0*pw, two, zero, zero, 0.0, 0.0);
            dec2rgpulse((2.5e-3-pw), zero, 0.0, 0.0);
            dec2rgpulse((2.5e-3-pw), zero, 0.0, 0.0);
            sim3pulse(2.0*pw, 0.0, 2.0*pw, zero, zero, zero, 0.0, 0.0);
            dec2rgpulse((2.5e-3-pw), zero, 0.0, 0.0);
            endloop(v5);
        }

        dec2power(pwNlvl);
        decrgpulse(pwN, zero, 0.0, 0.0);
        delay(1.0/(8.0*slNrf) + 2.0*pwN/PI - pwN);
    }
    /*   xxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxx    */

    if  (T2[A]=='y')
    {
        dec2phase(zero);
        initval(0.0,v3);
        initval(180.0,v4);
        if (BPpwrlimits > 0.5)
        {
            dec2power(pwNlvl-3.0);    /* reduce for probe protection */
            pwN=pwN*compN*1.4;
        }

        ncyc = 100.0*relaxT;
        initval(ncyc,v5);

        loop(v5,v6);

        initval(3.0,v7);
        loop(v7,v8);
        delay(0.625e-3 - pwN);
        dec2rgpulse(2.0*pwN, zero, 0.0, 0.0);
        delay(0.625e-3 - pwN);
        endloop(v8);

        delay(0.625e-3 - pwN - SAPS_DELAY);
        add(v4,v3,v3);
        obsstepsize(1.0);
        xmtrphase(v3);	   	/* SAPS_DELAY */
        dec2rgpulse(2.0*pwN, zero, 0.0, 0.0);
        delay(0.625e-3 - pwN - pw);

        rgpulse(2*pw, zero, 0.0, 0.0);

        delay(0.625e-3 - pwN - pw );
        dec2rgpulse(2.0*pwN, zero, 0.0, 0.0);
        xmtrphase(zero);						/* SAPS_DELAY */
        delay(0.625e-3 - pwN - SAPS_DELAY);

        initval(3.0,v9);
        loop(v9,v10);
        delay(0.625e-3 - pwN);
        dec2rgpulse(2.0*pwN, zero, 0.0, 0.0);
        delay(0.625e-3 - pwN);
        endloop(v10);

        endloop(v6);
        if (BPpwrlimits > 0.5)
        {
            dec2power(pwNlvl);    /* restore normal value */
            pwN=getval("pwN");
        }
    }

    /*  xxxxxxxxxxxxxxxxxx    OPTIONS FOR N15 EVOLUTION    xxxxxxxxxxxxxxxxxxxxx  */
    txphase(zero);
    dec2phase(t9);

    if ( (NH2only[A]=='y') || (T1[A]=='y') || (T1rho[A]=='y') || (T2[A]=='y') )
    {
        delay(tau1);
        /* optional sech/tanh pulse in middle of t1 */
        if (C13refoc[A]=='y') 				   /* WFG_START_DELAY */
        {   decshaped_pulse("rna_stC140", 1.0e-3, zero, 0.0, 0.0);
            delay(tNH - 1.0e-3 - WFG_START_DELAY - 2.0*pw);
        }
        else
        {
            delay(tNH - 2.0*pw);
        }
        rgpulse(2.0*pw, zero, 0.0, 0.0);
        if (tNH < gt1 + 1.99e-4)  delay(gt1 + 1.99e-4 - tNH);

        delay(tau1);

        dec2rgpulse(2.0*pwN, t9, 0.0, 0.0);

        if (mag_flg[A] == 'y')  magradpulse(gzcal*gzlvl1, gt1);
        else  zgradpulse(gzlvl1, gt1);   	/* 2.0*GRADIENT_DELAY */
        txphase(t4);
        dec2phase(t10);
        if (tNH > gt1 + 1.99e-4)  delay(tNH - gt1 - 2.0*GRADIENT_DELAY);
        else   delay(1.99e-4 - 2.0*GRADIENT_DELAY);
    }

    else if (TROSY[A]=='y')
    {
        if ( (C13refoc[A]=='y') && (tau1 > 0.5e-3 + WFG2_START_DELAY) )
        {   delay(tau1 - 0.5e-3 - WFG2_START_DELAY);     /* WFG2_START_DELAY */
            decshaped_pulse("rna_stC140", 1.0e-3, zero, 0.0, 0.0);
            delay(tau1 - 0.5e-3);
        }
        else    delay(2.0*tau1);

        if (mag_flg[A] == 'y')  magradpulse(gzcal*gzlvl1, gt1);
        else  zgradpulse(gzlvl1, gt1);   	/* 2.0*GRADIENT_DELAY */
        delay(2.0e-4 - 2.0*GRADIENT_DELAY);

        dec2rgpulse(2.0*pwN, t9, 0.0, 0.0);

        delay(gt1 + 2.0e-4 - pwHs - 1.0e-4 - 2.0*POWER_DELAY);
        txphase(three);
        obspower(tpwrs);				       /* POWER_DELAY */
        shaped_pulse("rna_H2Osinc", pwHs, three, 5.0e-5, 0.0);
        txphase(t4);
        obspower(tpwr);					       /* POWER_DELAY */
        delay(5.0e-5);
    }

    else
    {   /* fully-coupled spectrum */
        if (dm2[C]=='n')  {
            rgpulse(2.0*pw, zero, 0.0, 0.0);
            pw=0.0;
        }

        if ( (C13refoc[A]=='y') && (tau1 > 0.5e-3 + WFG2_START_DELAY) )
        {   delay(tau1 - 0.5e-3 - WFG2_START_DELAY);     /* WFG2_START_DELAY */
            simshaped_pulse("", "rna_stC140", 2.0*pw, 1.0e-3, zero, zero, 0.0, 0.0);
            delay(tau1 - 0.5e-3);
            delay(gt1 + 2.0e-4);
        }
        else
        {   delay(tau1);
            rgpulse(2.0*pw, zero, 0.0, 0.0);
            delay(gt1 + 2.0e-4 - 2.0*pw);
            delay(tau1);
        }
        decphase(zero);
        pw=getval("pw");
        dec2rgpulse(2.0*pwN, t9, 0.0, 0.0);

        if (mag_flg[A] == 'y')  magradpulse(gzcal*gzlvl1, gt1);
        else  zgradpulse(gzlvl1, gt1);   	/* 2.0*GRADIENT_DELAY */
        txphase(t4);
        dec2phase(t10);
        delay(2.0e-4 - 2.0*GRADIENT_DELAY);
    }

    if  (T1rho[A]=='y')   delay(POWER_DELAY);


    /*  xxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxxx  */
    if (TROSY[A]=='y')  rgpulse(pw, t4, 0.0, 0.0);
    else                sim3pulse(pw, 0.0, pwN, t4, zero, t10, 0.0, 0.0);

    txphase(zero);
    dec2phase(zero);
    zgradpulse(gzlvl5, gt5);
    if (TROSY[A]=='y')   delay(lambda - 0.65*(pw + pwN) - gt5);
    else   delay(lambda - 1.3*pwN - gt5);

    sim3pulse(2.0*pw, 0.0, 2.0*pwN, zero, zero, zero, 0.0, 0.0);

    zgradpulse(gzlvl5, gt5);
    txphase(one);
    dec2phase(t11);
    delay(lambda - 1.3*pwN - gt5);

    sim3pulse(pw, 0.0, pwN, one, zero, t11, 0.0, 0.0);

    txphase(zero);
    dec2phase(zero);
    zgradpulse(1.5*gzlvl5, gt5);
    delay(lambda - 1.3*pwN - gt5);

    sim3pulse(2.0*pw, 0.0, 2.0*pwN, zero, zero, zero, 0.0, 0.0);

    dec2phase(t10);
    zgradpulse(1.5*gzlvl5, gt5);
    if (TROSY[A]=='y')   delay(lambda - 1.6*pwN - gt5);
    else   delay(lambda - 0.65*pwN - gt5);

    if (TROSY[A]=='y')   dec2rgpulse(pwN, t10, 0.0, 0.0);
    else    	     rgpulse(pw, zero, 0.0, 0.0);

    delay((gt1/10.0) + 1.0e-4 - 0.65*pw + 2.0*GRADIENT_DELAY + POWER_DELAY);

    if (dm3[B] == 'y')			         /*optional 2H decoupling off */
    {   dec3rgpulse(1/dmf3, three, 0.0, 0.0);
        dec3blank();
        setstatus(DEC3ch, FALSE, 'w', FALSE, dmf3);
        dec3blank();
    }

    rgpulse(2.0*pw, zero, 0.0, rof1);

    dec2power(dpwr2);				       /* POWER_DELAY */
    if (mag_flg[A] == 'y')	  magradpulse(icosel*gzcal*gzlvl2, 0.1*gt1);
    else   zgradpulse(icosel*gzlvl2, 0.1*gt1);		/* 2.0*GRADIENT_DELAY */
    rcvron();
    statusdelay(C,1.0e-4-rof1);

    if (dm3[B] == 'y') {
        delay(1/dmf3);
        lk_sample();
    }

    setreceiver(t12);
}
Example #13
0
pulsesequence()
{
double	gzlvl1  = getval("gzlvl1"),
	gt1     = getval("gt1"),
	gstab   = getval("gstab"),
	del     = getval("del"),
	tweek   = getval("tweek"),
	prgtime = getval("prgtime"),
        prgpwr  = getval("prgpwr"),
        satpwr = getval("satpwr"),
        satdly = getval("satdly"),
        gzlvl2 = getval("gzlvl2"),
        gt2 = getval("gt2"),
        gzlvlhs = getval("gzlvlhs"),
        hsgt = getval("hsgt"),
        wrefpwr = getval("wrefpwr"),
        wrefpw = getval("wrefpw"),
        wrefpwrf = getval("wrefpwrf"),
        dosytimecubed,dosyfrq,Ddelta;
char	delflag[MAXSTR],lkgate_flg[MAXSTR],alt_grd[MAXSTR],prg_flg[MAXSTR];
char	satmode[MAXSTR],sspul[MAXSTR],wrefshape[MAXSTR];

   getstr("delflag",delflag);
   getstr("lkgate_flg",lkgate_flg);
   getstr("alt_grd",alt_grd);
   getstr("prg_flg",prg_flg);
   getstr("satmode",satmode);
   getstr("sspul",sspul);
   getstr("wrefshape", wrefshape);

       //synchronize gradients to srate for probetype='nano'
       //   Preserve gradient "area"
          gt1 = syncGradTime("gt1","gzlvl1",1.0);
          gzlvl1 = syncGradLvl("gt1","gzlvl1",1.0);
          gt2 = syncGradTime("gt2","gzlvl2",1.0);
          gzlvl2 = syncGradLvl("gt2","gzlvl2",1.0);

   if (del<(3*gt1+3.0*gstab+2.0*rof1+pw*2.0))
   {  abort_message("DgcsteSL error: del is less than %f, too short!",
           (3*gt1+3.0*gstab+2.0*rof1+pw*2.0));
   }

   /* Safety check for the duration of the purge pulse */
   if (prgtime > 4.0e-2)
   {  text_error("prgtime has been reset to a maximum of 2 ms");
      prgtime = 2.0e-3;
   }
   dosyfrq=sfrq;
   Ddelta=gt1;             /* the diffusion-encoding pulse width is gt1 */
   dosytimecubed=Ddelta*Ddelta*(del-(Ddelta/3.0));
   putCmd("makedosyparams(%e,%e)\n",dosytimecubed,dosyfrq);

   /* phase cycling calculation */
   if (delflag[0]=='y')
   {  hlv(ct,v4);
      mod2(v4,v2);
      mod2(ct,v1);
      dbl(v1,v1);
      add(v2,v1,v1);
      mod4(v1,v1); 	/* 0 2 1 3 , 1st 90 */
      hlv(v4,v4);
      mod2(v4,v3);
      dbl(v3,v3);	/* (0)4 (2)4 */
      hlv(v4,v4);
      mod2(v4,v2);
      dbl(v2,v2);	/* (0)8 (2)8 */
      hlv(v4,v4);
      mod2(v4,v5);
      add(v5,v3,v3);
      mod4(v3,v3);	/* {(0)4 (2)4}2 {(1)4 (3)4}2, 3rd 90 */
      hlv(v4,v4);
      assign(v4,v6);
      mod2(v4,v4);
      add(v4,v2,v2);
      mod4(v2,v2);	/* {(0)8 (2)8}2 {(1)8 (3)8}2, 2nd 90 */
      mod2(ct,v10);	/* gradients change sign every increment */

      assign(v3,oph);
      add(oph,v2,oph);
      sub(oph,v1,oph);
      mod4(oph,oph);

      assign(oph,v5);
      add(one,v5,v5);
      mod2(ct,v7);
      dbl(v7,v7);
      hlv(v6,v6);
      mod2(v6,v6);
      dbl(v6,v6);
      add(v7,v5,v5);	/* the purge pulse is 90 deg. off the receiver phase */
      add(v6,v5,v5);	/* it is phase alternated every increment */
      mod4(v5,v5);	/* and also every 64 increments */
   }
   else
   {
      assign(ct,v4);
      assign(oph,v4);	/*v4 used only for normal s2pul- type sequence */
   }
   add(v3,two,v9);

   if (ni > 1.0)
   {  abort_message("DgcsteSL is a 2D, not a 3D dosy sequence:  please set ni to 0 or 1");
   }

   /* equilibrium period */
   status(A);
      obspower(tpwr);
      if (sspul[A] == 'y')
       {
         zgradpulse(gzlvlhs,hsgt);
         rgpulse(pw,zero,rof1,rof1);
         zgradpulse(gzlvlhs,hsgt);
       }
      if (satmode[0] == 'y')
       {
       if (d1 - satdly > 0)
         delay(d1 - satdly);
       else delay(0.02);
       obspower(satpwr);
       txphase(v1);
       rgpulse(satdly,zero,rof1,rof1);
       obspower(tpwr);
       delay(1.0e-5);
      }
     else
     {  delay(d1); }

   obspower(tpwr);

   status(B);
   /* first part of bppdel sequence */
   if(delflag[0] == 'y')
   {  rgpulse(pw, v1, rof1, 0.0);	/* first 90, v1 */

      if (lkgate_flg[0] == 'y') lk_hold();   /* turn lock sampling off */

      if (alt_grd[0] == 'y')
      {  ifzero(v10);
           zgradpulse(gzlvl1,gt1);
         elsenz(v10);
           zgradpulse(-1.0*gzlvl1,gt1);
	 endif(v10);
      }
      else
         zgradpulse(gzlvl1,gt1);
         delay(gstab);

      rgpulse(pw, v2, rof1, 0.0);	/* second 90, v2 */

      if (alt_grd[0] == 'y')
      {  ifzero(v10);			/* compensating AND CPS gradient */
   	   zgradpulse(-1.0*gzlvl1*(1.0-tweek),gt1);
	 elsenz(v10);
   	   zgradpulse(gzlvl1*(1.0-tweek),gt1);
	 endif(v10);
      }
      else  /* compensating AND CPS gradient */
	 zgradpulse(-1.0*gzlvl1*(1.0-tweek),gt1);

      delay(gstab);

      if (satmode[B] == 'y')
       { obspower(satpwr);
         rgpulse(del-3.0*(gt1+gstab)-2.0*rof1-pw*2.0,zero,rof1,rof1);
         obspower(tpwr);
       }
      else
          delay(del-3.0*(gt1+gstab)-2.0*rof1-pw*2.0); /* diffusion delay */

      if (alt_grd[0] == 'y')
      {
	 ifzero(v10);
   	   zgradpulse(-1.0*gzlvl1*(1.0+tweek),gt1);
	 elsenz(v10);
   	   zgradpulse(gzlvl1*(1.0+tweek),gt1);
	 endif(v10);
      }
      else
         zgradpulse(-1.0*gzlvl1*(1.0+tweek),gt1);
      delay(gstab);

      rgpulse(pw, v3, rof1, 0.0);	/* third 90, v3 */

      if (alt_grd[0] == 'y')
      {
	 ifzero(v10);
	   zgradpulse(gzlvl1,gt1);
	 elsenz(v10);
	   zgradpulse(-1.0*gzlvl1,gt1);
         endif(v10);
      }
      else
         zgradpulse(gzlvl1,gt1);
      delay(gstab);

     if (alt_grd[0] == 'y')
       { ifzero(v10); zgradpulse(gzlvl2,gt2);
              elsenz(v10); zgradpulse(-gzlvl2,gt2); endif(v10);}
     else zgradpulse(gzlvl2,gt2);
       obspower(wrefpwr+6); obspwrf(wrefpwrf);
       delay(gstab);
       shaped_pulse(wrefshape,wrefpw,v9,rof1,0.0);
       obspower(tpwr); obspwrf(4095.0);
       rgpulse(2.0*pw,v3,rof1,0.0);
     if (alt_grd[0] == 'y')
       { ifzero(v10); zgradpulse(gzlvl2,gt2);
              elsenz(v10); zgradpulse(-gzlvl2,gt2); endif(v10);}
     else zgradpulse(gzlvl2,gt2);
       obspower(wrefpwr+6); obspwrf(wrefpwrf);
       delay(gstab);
     if (alt_grd[0] == 'y')
       { ifzero(v10); zgradpulse(1.2*gzlvl2,gt2);
              elsenz(v10); zgradpulse(-1.2*gzlvl2,gt2); endif(v10); }
     else zgradpulse(1.2*gzlvl2,gt2);
       delay(gstab);
       shaped_pulse(wrefshape,wrefpw,v9,rof1,0.0);
       obspower(tpwr); obspwrf(4095.0);
       rgpulse(2.0*pw,v3,rof1,rof1);
     if (alt_grd[0] == 'y')
       { ifzero(v10); zgradpulse(1.2*gzlvl2,gt2);
              elsenz(v10); zgradpulse(-1.2*gzlvl2,gt2); endif(v10); }
     else zgradpulse(1.2*gzlvl2,gt2);
       delay(gstab+2.0*pw/3.14);
      if (lkgate_flg[0] == 'y') lk_sample(); /* turn lock sampling on */

      /* purge pulse to scramble any magnetisation that 
		is not in phase with the receiver */
      if (prg_flg[0] == 'y')
      {  obspower(prgpwr);
         rgpulse(prgtime, v5, rof1, 0.0);
      }
   }
   else
      rgpulse(pw, v4, rof1, rof2);	/* first 90, v1 */

   status(C);
}
Example #14
0
pulsesequence()
{
/* DECLARE VARIABLES */

 char      
	     satmode[MAXSTR],
	     f1180[MAXSTR],
	     abfilter[MAXSTR];	    /* set 'a' for inphase and 'b' for antiphase */


 int	     t1_counter,icosel,first_FID;

 double      /* DELAYS */
             tau1,                      /* t1/2 */
             tauhn,taunco,taucoca,taunca,tauhaca,taucaha,taucacb,

	     /* COUPLINGS */ 
             jhn = getval("jhn"),
             jnco = getval("jnco"),
             jcoca = getval("jcoca"),
             jnca = getval("jnca"),
             jhaca = getval("jhaca"),
             jcaha = getval("jcaha"),
             jcacb = getval("jcacb"),
   
	     /* PULSES */
             pwN = getval("pwN"),               /* PW90 for N-nuc */
             pwC = getval("pwC"),               /* PW90 for C-nuc */
             pwHs = getval("pwHs"),

	     /* POWER LEVELS */
             satpwr = getval("satpwr"),       /* low power level for presat */
             tpwrsf_d = getval("tpwrsf_d"),       /* fine power level for first pwHs */
             tpwrsf_u = getval("tpwrsf_u"),       /* fine power level for second pwHs */
             tpwrs,
             pwClvl = getval("pwClvl"),         /* power level for C hard pulses */ 
             compC = getval("compC"),         /* amplifier compression factor */ 
             compH = getval("compH"),         /* amplifier compression factor */ 
             pwNlvl = getval("pwNlvl"),         /* power level for N hard pulses */
             rf90onco,pw90onco,              /* power level/pw for CO 90 pulses */ 
             rf180onco,pw180onco,            /* power level/pw for CO 180 pulses */
             rf180offca,pw180offca,          /* power level/pw for CA 180 pulses */

             /* CONSTANTS */
             kappa,
   	     lambda = getval("lambda"),         /* scaling factor for JNCa */
 
	     /* GRADIENT DELAYS AND LEVELS */
             gt0 = getval("gt0"),               /* gradient time */
             gt1 = getval("gt1"),               /* gradient time */
             gt3 = getval("gt3"),               /* gradient time */
             gt5 = getval("gt5"),
             gstab = getval("gstab"),
             gzlvl0 = getval("gzlvl0"),         /* level of gradient */
             gzlvl1 = getval("gzlvl1"),
             gzlvl2 = getval("gzlvl2"),
             gzlvl3 = getval("gzlvl3"),
             gzlvl5 = getval("gzlvl5");

/* LOAD VARIABLES */

  getstr("satmode",satmode); 
  getstr("f1180",f1180);
  getstr("abfilter",abfilter);

/* check validity of parameter range */

    if ((dm[A] == 'y' || dm[B] == 'y' || dm[C] == 'y' ))
	{
	printf("incorrect Dec1 decoupler flags!  ");
	psg_abort(1);
    } 

    if ((dm2[A] == 'y' || dm2[B] == 'y' || dm2[C] == 'y' ))
	{
	printf("incorrect Dec2 decoupler flags!  ");
	psg_abort(1);
    } 

    if ( satpwr > 8 )
    {
	printf("satpwr too large !!!  ");
	psg_abort(1);
    }

    if ( dpwr > 50 )
    {
	printf("don't fry the probe, dpwr too large!  ");
	psg_abort(1);
    }

    if ( dpwr2 > 50 )
    {
	printf("don't fry the probe, dpwr2 too large!  ");
	psg_abort(1);
    }

/* LOAD VARIABLES */

  settable(t1, 1, phi1);
  settable(t2, 1, phi2);
  settable(t3, 1, phi3);
  settable(t4, 2, phi4);
  settable(t6, 4, phi6);
  settable(t7, 2, phi7);

/* INITIALIZE VARIABLES AND POWER LEVELS FOR PULSES */

   tauhn = ((jhn != 0.0) ? 1/(4*(jhn)) : 2.25e-3);
   taunco = ((jnco !=0.0) ? 1/(4*(jnco)) : 16.6e-3);
   taucoca = ((jcoca !=0.0) ? 1/(4*(jcoca)) : 4.5e-3);
   taunca =  ((jnca  !=0.0)  ? 1/(4*(jnca))  : 12e-3);
   tauhaca = ((jhaca !=0.0)  ? 1/(4*(jhaca)) : 12e-3);
   taucaha = ((jcaha !=0.0)  ? 1/(4*(jcaha)) : 12e-3);
   taucacb = ((jcacb !=0.0)  ? 1/(4*(jcacb)) : 12e-3);


       if((getval("arraydim") < 1.5) || (ix==1))
         first_FID = 1;
       else
         first_FID = 0;

    /* 90 degree pulse on CO, null at Ca 118ppm away */

        pw90onco = sqrt(15.0)/(4.0*118.0*dfrq);
        rf90onco = (4095.0*pwC*compC)/pw90onco;
        rf90onco = (int) (rf90onco + 0.5);
        if(rf90onco > 4095.0)
        {
          if(first_FID)
            printf("insufficient power for pw90onco -> rf90onco (%.0f)\n", rf90onco);
          rf90onco = 4095.0;
          pw90onco = pwC;
        }

    /* 180 degree pulse on CO, null at Ca 118ppm away */

        pw180onco = sqrt(3.0)/(2.0*118.0*dfrq);
        rf180onco = (4095.0*pwC*compC*2.0)/pw180onco;
        rf180onco = (int) (rf180onco + 0.5);
        if(rf180onco > 4095.0)
        {
          if(first_FID)
            printf("insufficient power for pw180onco -> rf180onco (%.0f)\n", rf180onco);
          rf180onco = 4095.0;
          pw180onco = pwC*2.0;
        }
        pw180offca = pw180onco;        rf180offca = rf180onco;
      
/* Phase incrementation for hypercomplex data */
    
     kappa=(taunco - tauhn - gt1 - gstab)/(0.5*ni/sw1)-0.001;
      if (kappa > 1.0) 
     {  
	              kappa=1.0-0.01;
     }   

       if ( phase1 == 1) /* Hypercomplex in t2 */
     {
	                icosel = -1;
	                tsadd(t2, 2, 4);
	                tsadd(t3, 2, 4);
     }  
      else icosel = 1;   
      
      if (ix == 1)
      printf("semi constant-time factor %4.6f\n",kappa); 
   
/* calculate modification to phases based on current t1 values
   to achieve States-TPPI acquisition */
 
   if (ix == 1)
      d2_init = d2;
      t1_counter = (int) ( (d2-d2_init)*sw1 + 0.5);

      if (t1_counter %2)  /* STATES-TPPI */
      {
        tsadd(t1,2,4);
        tsadd(t7,2,4);
      }

/* set up so that get (-90,180) phase corrects in F1 if f1180 flag is y */

   tau1 = d2;
   if (f1180[A] == 'y')  tau1 += ( 1.0/(2.0*sw1));
   tau1 = tau1/2.0;


/* selective H20 one-lobe sinc pulse */
  tpwrs = tpwr - 20.0*log10(pwHs/(compH*pw*1.69));   /*needs 1.69 times more*/
  tpwrs = (int) (tpwrs);                   	  /*power than a square pulse */
  if (tpwrsf_d<4095.0) tpwrs=tpwrs+6.0; /* allow for fine power control via tpwrsf_d */

/* BEGIN ACTUAL PULSE SEQUENCE */

status(A);
   obspower(satpwr);            /* Set power for presaturation    */
   decpower(pwClvl);              /* Set decoupler1 power to pwClvl  */
   decpwrf(rf90onco);
   dec2power(pwNlvl);            /* Set decoupler2 power to pwNlvl */

/* Presaturation Period */


  if (satmode[0] == 'y')
    {
      rgpulse(d1,zero,rof1,rof1);
      obspower(tpwr);              /* Set power for hard pulses  */
    }
  else  
    {
      obspower(tpwr);              /* Set power for hard pulses  */
      delay(d1);
    }

status(B);

  rcvroff();
     /* eliminate all magnetization originating on 13C */
   
     decpwrf(rf90onco); 
     decrgpulse(pw90onco,zero,0.0,0.0);
      
     zgradpulse(gzlvl0,gt0);
     delay(gstab);
  
/* shaped pulse for water flip-back */
      obspower(tpwrs); obspwrf(tpwrsf_d);
      shaped_pulse("H2Osinc_d",pwHs,one,rof1,0.0);
      delay(2.0e-6);
      obspower(tpwr); obspwrf(4095.0);
  /* shaped pulse */   
   
  /* transfer from HN to N by INEPT */

  rgpulse(pw,zero,rof1,0.0); /* 90 for 1H */

  zgradpulse(gzlvl0*1.3,gt0);
  delay(gstab);
   
  delay(tauhn - gt0 - gstab);        /* 1/4JHN */
   
  sim3pulse(2.0*pw,0.0,2.0*pwN,zero,zero,zero,0.0,0.0);  /* 180 for 1H and 15N */

  delay(tauhn - gt0 - gstab);       /* 1/4JHN */
   
  zgradpulse(gzlvl0*1.3,gt0);
  delay(gstab);

  rgpulse(pw,three,rof1,0.0);
      
  zgradpulse(gzlvl3,gt3);
  delay(gstab);
   
/* start transfer from N to CO */
      
  dec2rgpulse(pwN,zero,0.0,0.0);
    
  delay(taunco - gt0 - gstab - POWER_DELAY - 0.5*pw180onco);	 /* 1/4J(NCO) */
	  
  decpwrf(rf180onco);              	/* Set decoupler1 power to rf180onco */

  zgradpulse(gzlvl0,gt0);
  delay(gstab);

  sim3pulse(0.0,pw180onco,2.0*pwN,zero,zero,zero,rof1,rof1);  /* 180 for 13C' and 15N */

  zgradpulse(gzlvl0,gt0);
  delay(gstab);

  decpwrf(rf90onco);            /* Set decoupler1 power to rf90onco */

  delay(taunco - gt0 - gstab - POWER_DELAY - 0.5*pw180onco); 	    /* 1/4J(NCO) */

  dec2rgpulse(pwN,one,0.0,0.0);  /* 90 for 15N */
   
  zgradpulse(gzlvl3*1.1,gt3);
  delay(gstab);
   
  decphase(t4);
  decrgpulse(pw90onco,t4,0.0,0.0);  /* 90 for 13C' */
      
   if (abfilter[0] == 'b')
     {
	  decpwrf(rf180offca);    /* Set decoupler1 power to rf180offca */
	  decshaped_pulse("offC3",pw180offca,zero,0.0,0.0); 
	   
          decpwrf(rf180onco);           /* Set decoupler1 power to rf180onco */

	  delay(taucoca - gt0 - gstab - 0.5*pw180onco - pw180offca - 2.0*POWER_DELAY);  /* 1/4J(COCA) */

          zgradpulse(gzlvl0*0.9,gt0);
          delay(gstab);
	
          decrgpulse(pw180onco,zero,0.0,0.0);  /* 180 13C' */
  	  decpwrf(rf180offca);              	     /* Set decoupler1 power to rf180offca */
	  decshaped_pulse("offC3",pw180offca,zero,0.0,0.0); 
    
          zgradpulse(gzlvl0*0.9,gt0);
          delay(gstab);

	  delay(taucoca - gt0 - gstab - 0.5*pw180onco - pw180offca - 2.0*POWER_DELAY);   /* 1/4J(NCO) */

          decpwrf(rf90onco);    /* Set decoupler1 power to rf90onco */

          decrgpulse(pw90onco,one,0.0,0.0); /* 90 for 13C' do not touch alpha's */

          /* Field crusher gradient */
          zgradpulse(gzlvl3*0.9,gt3);
          delay(gstab);
	  /* Field crusher gradient */

        }

      if (abfilter[0] == 'a')
     {
        zgradpulse(gzlvl0*0.9,gt0);
        delay(gstab);
		  
        decpwrf(rf180offca);   /* Set decoupler1 power to rf180offca */

	delay(0.5*taucoca - gt0 - gstab - POWER_DELAY - 0.5*pw180offca);                   /* 1/8J(COCA) */
	 
	decshaped_pulse("offC3",pw180offca,zero,0.0,0.0); 

	delay(0.5*taucoca - gt0 - gstab - POWER_DELAY - 0.5*pw180offca - 0.5*pw180onco);     /* 1/8J(COCA) */
	
        decpwrf(rf180onco);   /* Set decoupler1 power to rf180onco */

        zgradpulse(gzlvl0*0.9,gt0);
        delay(gstab);

        decrgpulse(pw180onco,zero,0.0,0.0);   /* 180 13C' */

        zgradpulse(gzlvl0*0.9,gt0);
        delay(gstab);
	
	decpwrf(rf180offca);      

	delay(0.5*taucoca - gt0 - gstab - POWER_DELAY - 0.5*pw180onco - 0.5*pw180offca); 	  /* 1/8J(COCA) */
	      
        decshaped_pulse("offC3",pw180offca,zero,0.0,0.0);
	 
	delay(0.5*taucoca - gt0 - gstab - POWER_DELAY - 0.5*pw180offca); /* 1/8J(COCA) */

        decpwrf(rf90onco);         /* Set decoupler1 power to rf90onco */

        zgradpulse(gzlvl0*0.9,gt0);
        delay(gstab);


        decrgpulse(pw90onco,zero,0.0,0.0);  /* 90 for 13C' */

        /* Field crusher gradient */
           zgradpulse(gzlvl3*0.9,gt3);
           delay(gstab);
	/* Field crusher gradient */

      }  
 
     dec2rgpulse(pwN,t1,0.0,0.0); /* 90 15N */
  
     if (lambda>0.0)
      { 
        delay(lambda*tau1);  /* (lambda)t1/2 */
   
        decpwrf(rf180offca);   
        sim3shaped_pulse("","offC3","",0.0,pw180offca,2.0*pwN,zero,zero,zero,rof1,rof1);

        delay(lambda*tau1);  /* (lambda)t1/2 */
      }

     delay(tau1);                             /* t1/2 */
     delay(taunco - tauhn - pw180onco);  

     decpwrf(rf180onco);
     decrgpulse(pw180onco,zero,0.0,0.0);     /* 180 for 13C' */

     delay((1-kappa)*tau1);                  /* (1-k)t1/2 */

     dec2rgpulse(2.0*pwN,zero,0.0,0.0);     /* 180 for 15N */
   
     delay((taunco - tauhn - gt1 - gstab) - kappa*tau1);  /* 1/4J(NCO) - 1/4J(NH) - kt1/2 */
          
     zgradpulse(gzlvl1,gt1);
     delay(gstab);
   
   /* start TROSY transfer from N to HN */
      
         
     sim3pulse(pw,0.0,0.0,t2,zero,zero,rof1,rof1);

     zgradpulse(gzlvl5,gt5);
     delay(gstab);
 
     delay(tauhn - gt5 - gstab - POWER_DELAY);
   
      
     decpwrf(rf180onco);
     sim3pulse(2.0*pw,pw180onco,2*pwN,zero,zero,zero,rof1,rof1);
   
     delay(tauhn - gt5 - gstab - POWER_DELAY);
   
      
     zgradpulse(gzlvl5,gt5);
     delay(gstab);
   
     decpwrf(rf90onco);
     sim3pulse(pw,pw90onco,pwN,one,t6,zero,rof1,rof1);
   
      /* shaped pulse WATERGATE */
         obspower(tpwrs); obspwrf(tpwrsf_u);
         shaped_pulse("H2Osinc_u",pwHs,t2,rof1,0.0);
         obspower(tpwr); obspwrf(4095.0);
       /* shaped pulse */
   
     zgradpulse(gzlvl5*0.8,gt5);
     delay(gstab);
      
     delay(tauhn - gt5 - gstab - 2.0*POWER_DELAY - pwHs);
   
     sim3pulse(2*pw,0.0,2*pwN,zero,zero,zero,rof1,rof1);
   
      
     delay(tauhn - gt5 - gstab - 2.0*POWER_DELAY);
   
      decpower(dpwr);
      
     zgradpulse(gzlvl5*0.8,gt5);
     delay(gstab);
   
     dec2rgpulse(pwN,t3,0.0,0.0);  /* 90 for 15N */
      
     dec2power(dpwr2);
      
     delay((gt1/10.0) -pwN + gstab - POWER_DELAY);
      
     rgpulse(2.0*pw, zero, rof1, rof1);
      
     zgradpulse(gzlvl2*icosel,gt1/10.0);
     delay(gstab);
      
   status(C);
     setreceiver(t7);
}
Example #15
0
pulsesequence()

{
/* DECLARE AND LOAD VARIABLES */

char        f1180[MAXSTR],
            bottom[MAXSTR],
            right[MAXSTR],
            C13refoc[MAXSTR];


int	    t1_counter;

double       tau1,                 				  /* t1 delay */
             taua=getval("taua"),  		      /* < 1 / 4J(NH) 2.25 ms */
             taub=getval("taub"),  			/* 1 / 4J(NH) 2.75 ms */
   pwClvl = getval("pwClvl"),                   /* coarse power for C13 pulse */
   pwC = getval("pwC"),               /* C13 90 degree pulse length at pwClvl */
   compH = getval("compH"),        /* adjustment for H1 amplifier compression */
   compN = getval("compN"),       /* adjustment for N15 amplifier compression */
   compC = getval("compC"),       /* adjustment for C13 amplifier compression */

        pwHs = getval("pwHs"),          /* H1 90 degree pulse length at tpwrs */
        tpwrs,                        /* power for the pwHs ("H2Osinc") pulse */
	finepwrf = getval("finepwrf"), 		     /* fine power adjustment */
        pwNlvl = getval("pwNlvl"),                    /* power for N15 pulses */
        pwN = getval("pwN"),          /* N15 90 degree pulse length at pwNlvl */

        sw1 = getval("sw1"),

	gt3 = getval("gt3"),
	gt4 = getval("gt4"),
	gt5 = getval("gt5"),
        gzlvlr = getval("gzlvlr"),
        gzlvl3 = getval("gzlvl3"),
        gzlvl4 = getval("gzlvl4"),
        gzlvl5 = getval("gzlvl5");

  getstr("f1180",f1180);
  getstr("bottom",bottom);
  getstr("right",right);
  getstr("C13refoc",C13refoc);

/*   INITIALIZE VARIABLES   */

compN=compN;
compC=compC;

/* selective H20 one-lobe sinc pulse */
    tpwrs = tpwr - 20.0*log10(pwHs/(compH*pw*1.69));   /*needs 1.69 times more*/
    tpwrs = (int) (tpwrs);                        /*power than a square pulse */
    tpwrs = tpwrs+6;        /* increase attenuator setting so that
           	fine power control can be varied about the nominal 2048 value */



/* check validity of parameter range */

    if((dm[A] == 'y' || dm[B] == 'y' || dm[C] == 'y'))
	{
	printf("incorrect Dec1 decoupler flags!  ");
	psg_abort(1);
    } 

    if((dm2[A] == 'y' || dm2[B] == 'y' || dm2[C] == 'y'))
	{
	printf("incorrect Dec2 decoupler flags!  ");
	psg_abort(1);
    } 

    if( dpwr > 50 )
    {
	printf("don't fry the probe, dpwr too large!  ");
	psg_abort(1);
    }

    if( dpwr2 > 50 )
    {
	printf("don't fry the probe, dpwr2 too large!  ");
	psg_abort(1);
    }

   if( pwNlvl > 63 )
    {
        printf("don't fry the probe, pwNlvl too large !");
        psg_abort(1);
    }

   if( pwClvl > 63 )
    {
        printf("don't fry the probe, pwClvl too large !");
        psg_abort(1);
    }

   if( gzlvlr > 500 )
    {
        printf("don't fry the probe, gzlvl0 too large !");
        psg_abort(1);
    }

/* LOAD VARIABLES */

  settable(t1, 8, phi1);
        if (bottom[A]=='y')
{
  settable(t2, 1, ph_y);
  settable(t5, 2, phi5);
  settable(t7, 2, phi6);
}
	else
{
  settable(t2, 1, phy);
  settable(t5, 2, phi6);
  settable(t7, 2, phi5);
}
	if (right[A]=='y')
  settable(t3, 1, ph_y);
	else
  settable(t3, 1, phy);
  settable(t4, 8, phi4);
  settable(t6, 8, rec);


/* Set up f1180  */

   tau1 = d2;
   if(f1180[A] == 'y' && C13refoc[A] == 'n') 

        tau1 += ( 1.0 / (2.0*sw1) - pw);

   if(f1180[A] == 'y' && C13refoc[A] == 'y') 

        tau1 += ( 1.0 / (2.0*sw1) - 2.0*pwC - 4.0e-6 - pw);

   if(f1180[A] == 'n' && C13refoc[A] == 'n') 

        tau1 = tau1 - pw;

   if(f1180[A] == 'n' && C13refoc[A] == 'y') 

        tau1 = ( tau1 - 2.0*pwC - 4.0e-6 - pw);

   if(tau1 < 0.2e-6) tau1 = 0.2e-6;

/* set up for complex FID */

   if (phase1 == 2)
   {
      tsadd(t2,2,4);
      tsadd(t3,2,4);
      tsadd(t6,2,4);
   }


/* Calculate modifications to phases for States-TPPI acquisition  */
 
   if( ix == 1 ) d2_init = d2;
   t1_counter = (int) ( (d2-d2_init)*sw1 + 0.5 );
   if( t1_counter %2 ) {
      tsadd(t1,2,4);
      tsadd(t4,2,4);
      tsadd(t6,2,4);
   }
    


/* BEGIN ACTUAL PULSE SEQUENCE */


status(A);
        obsoffset(tof);
        decoffset(dof+(50*dfrq));	/* 160 ppm for DEC */
        dec2offset(dof2-(45*dfrq2));	/* Middle of imino-N15 = 155 ppm */
	obspower(tpwr);
        obspwrf(4095.0);
        decpower(pwClvl);
        dec2power(pwNlvl);
        txphase(two);
        decphase(zero);
        dec2phase(zero);

        delay(d1);
	rcvroff();
   	delay(20.0e-6);

	rgpulse(pw,two,0.0,0.0);
	txphase(zero);
	
	zgradpulse(gzlvl5, gt5);
	delay(taua - gt5 - 2.0*GRADIENT_DELAY);	/* delay < 1/4J(XH)   */

  	sim3pulse(2*pw,0.0,2*pwN,zero,zero,zero,0.0,0.0);
	txphase(one);

	zgradpulse(gzlvl5, gt5);
        delay(taua - gt5 - 2.0*GRADIENT_DELAY);

    if (phase1 == 1)
  	sim3pulse(pw,0.0,pwN,one,zero,t1,0.0,0.0);
    if (phase1 == 2) 
  	sim3pulse(pw,0.0,pwN,one,zero,t4,0.0,0.0);

   	txphase(zero);
	decphase(zero);

   if (C13refoc[A] == 'y')
    {
        if (tau1>0.001)
        {
         zgradpulse(gzlvlr,(0.8*tau1/2.0 - 2.0*GRADIENT_DELAY ));
         delay(0.2*tau1/2.0 );
        }
        else
         delay(tau1/2.0);
	decrgpulse(pwC,zero,0.0,0.0);
	decrgpulse(2.0*pwC,one,2.0e-6,0.0);
	decrgpulse(pwC,zero,2.0e-6,0.0);
        if (tau1>0.001)
        {
         zgradpulse(-gzlvlr,(0.8*tau1/2.0 - 2.0*GRADIENT_DELAY ));
         delay(0.2*tau1/2.0 );
        }
        else
         if ((tau1/2.0)>0.0) delay(tau1/2.0);
    }
    else
    {
        if (tau1>0.001)
        {
         zgradpulse(gzlvlr,(0.8*tau1 - 2.0*GRADIENT_DELAY));
         delay(0.2*tau1);
         zgradpulse(-gzlvlr,(0.8*tau1 - 2.0*GRADIENT_DELAY ));
         delay(0.2*tau1);
        }
        else
         delay(tau1);
     }

 
   	rgpulse(pw,t2,0.0,0.0);
  	txphase(zero);
	dec2phase(zero);

	zgradpulse(gzlvl3,gt3);
  	delay(taub - gt3 - 2.0*GRADIENT_DELAY);

  	sim3pulse(2*pw,0.0,2*pwN,zero,zero,zero,0.0,0.0);
  	dec2phase(t3);

	zgradpulse(gzlvl3,gt3);
	delay(taub - gt3 - 2.0*GRADIENT_DELAY);

	sim3pulse(pw,0.0,pwN,zero,zero,t3,0.0,0.0);
	txphase(t5);
	dec2phase(zero);
        obspower(tpwrs);
        obspwrf(finepwrf);

        zgradpulse(gzlvl4,gt4);
	delay(taub - gt4 - 4.0*POWER_DELAY - rof1 - 2.0*GRADIENT_DELAY - pwHs);

	shaped_pulse("H2Osinc",pwHs,t5,0.0,0.0);
	txphase(t7);
        obspower(tpwr);
        obspwrf(4095.0);

        sim3pulse(2.0*pw,0.0e-6,2.0*pwN,t7,zero,zero,rof1,rof1);
	txphase(t5);
        obspwrf(finepwrf);
        obspower(tpwrs);

	shaped_pulse("H2Osinc",pwHs,t5,0.0,0.0);
	txphase(zero);
	obspower(tpwr);
        obspwrf(4095.0);

	zgradpulse(gzlvl4,gt4);
	delay(taub - gt4 - 6.0*POWER_DELAY - rof1 - 2.0*GRADIENT_DELAY 
		- 0.5*(pwN-pw)	- pwHs);

  	dec2rgpulse(pwN,zero,0.0,0.0);
	decpower(dpwr);
	dec2power(dpwr2);
	
/* acquire data */
status(C);
     	setreceiver(t6);
}
Example #16
0
pulsesequence()
{
/* DECLARE VARIABLES */

 char       satmode[MAXSTR],
	    fscuba[MAXSTR],
            fc180[MAXSTR],    /* Flag for checking sequence              */
	    cbdecseq[MAXSTR];

 int         icosel,
             ni = getval("ni"),
             t1_counter;   /* used for states tppi in t1           */ 

 double      tau1,         /*  t1 delay */
             tau2,         /*  t2 delay */
             tau3,         /*  t2 delay */
             taua,         /*  ~ 1/4JNH =  2.25 ms */
             taub,         /*  ~ 1/4JNH =  2.25 ms */
             tauc,         /*  ~ 1/4JCaC' =  4 ms */
             taud,         /*  ~ 1/4JCaC' =  4.5 ms if bigTCo can be set to be
				less than 4.5ms and then taud can be smaller*/
             zeta,        /* time for C'-N to refocuss set to 0.5*24.0 ms */
             bigTCa,      /* Ca T period */
             bigTCo,      /* Co T period */
             bigTN,       /* nitrogen T period */
             BigT1,       /* delay to compensate for gradient gt5 */
             satpwr,     /* low level 1H trans.power for presat  */
             sw1,          /* sweep width in f1                    */             
             sw2,          /* sweep width in f2                    */             
	     sphase,       /* small angle phase shift */
	     cbpwr,        /* power level for selective CB decoupling */
	     cbdmf,        /* pulse width for selective CB decoupling */
	     cbres,        /* decoupling resolution of CB decoupling */

   pwS1,                                         /* length of square 90 on Ca */
   phshift,        /*  phase shift induced on Ca by 180 on CO in middle of t1 */
   pwS2,                                               /* length of 180 on CO */
   pwS3,                                              /* length of 180 on Ca  */
   pwS4,                                             /* length of 90 on CO */
   pwS = getval("pwS"), /* used to change 180 on CO in t1 for 1D calibrations */
   pwZ,                                    /* the largest of pwS2 and 2.0*pwN */
   pwZ1,                /* the largest of pwS2 and 2.0*pwN for 1D experiments */

             gt1,
             gt2,
             gt3,
             gt4,
             gt5,
             gt6,
             gt7,
             gt8,
             gt9,
             gt10,
             gt11,
             gt12,
             gstab,
             gzlvl1,
             gzlvl2,
             gzlvl3,
             gzlvl4,
             gzlvl5,
             gzlvl6,
             gzlvl7, 
             gzlvl8, 
             gzlvl9, 
             gzlvl10, 
             gzlvl11, 
             gzlvl12,

             compH = getval("compH"),         /* adjustment for amplifier compression */
             pwHs = getval ("pwHs"),         /* H1 90 degree pulse at tpwrs */
             tpwrs,                          /* power for pwHs ("H2osinc") pulse */
             waltzB1 = getval("waltzB1"),

             pwClvl = getval("pwClvl"),                 /* coarse power for C13 pulse */
             pwC = getval("pwC"),             /* C13 90 degree pulse length at pwClvl */

             pwNlvl = getval("pwNlvl"),                       /* power for N15 pulses */
             pwN = getval("pwN"),             /* N15 90 degree pulse length at pwNlvl */

	     swCa = getval("swCa"),
	     swCO = getval("swCO"),
	     swN  = getval("swN"),
	     swTilt,      /* This is the sweep width of the tilt vector */

	     cos_N, cos_CO, cos_Ca,
	     angle_N, angle_CO, angle_Ca;
             angle_N=0.0;                      /*initialize variable*/

/* LOAD VARIABLES */


  getstr("satmode",satmode);
  getstr("fc180",fc180);
  getstr("fscuba",fscuba);

  taua   = getval("taua"); 
  taub   = getval("taub"); 
  tauc   = getval("tauc"); 
  taud   = getval("taud"); 
  zeta  = getval("zeta");
  bigTCa = getval("bigTCa");
  bigTCo = getval("bigTCo");
  bigTN = getval("bigTN");
  BigT1 = getval("BigT1");
  tpwr = getval("tpwr");
  satpwr = getval("satpwr");
  dpwr = getval("dpwr");
  sw1 = getval("sw1");
  sw2 = getval("sw2");
  sphase = getval("sphase");

  gt1 = getval("gt1");
  gt2 = getval("gt2");
  gt3 = getval("gt3");
  gt4 = getval("gt4");
  gt5 = getval("gt5");
  gt6 = getval("gt6");
  gt7 = getval("gt7");
  gt8 = getval("gt8");
  gt9 = getval("gt9");
  gt10 = getval("gt10");
  gt11 = getval("gt11");
  gt12 = getval("gt12");

  gstab = getval("gstab");
  gzlvl1 = getval("gzlvl1");
  gzlvl2 = getval("gzlvl2");
  gzlvl3 = getval("gzlvl3");
  gzlvl4 = getval("gzlvl4");
  gzlvl5 = getval("gzlvl5");
  gzlvl6 = getval("gzlvl6");
  gzlvl7 = getval("gzlvl7");
  gzlvl8 = getval("gzlvl8");
  gzlvl9 = getval("gzlvl9");
  gzlvl10 = getval("gzlvl10");
  gzlvl11 = getval("gzlvl11");
  gzlvl12 = getval("gzlvl12");

  /* Load variable */
     cbpwr = getval("cbpwr");
     cbdmf = getval("cbdmf");
     cbres = getval("cbres");
     tau1 = 0;
     tau2 = 0;
     tau3 = 0;
     cos_N = 0;
     cos_CO = 0;
     cos_Ca = 0;

     getstr("cbdecseq", cbdecseq);

/* LOAD PHASE TABLE */

  settable(t1,1,phi1);
  settable(t2,1,phi2);
  settable(t3,4,phi3);
  settable(t4,1,phi4);
  settable(t5,1,phi5);
  settable(t7,4,phi7);
  settable(t8,4,phi8);
  settable(t6,4,rec);

   kappa = 5.4e-3;

   /* get calculated pulse lengths of shaped C13 pulses */
        pwS1 = c13pulsepw("ca", "co", "square", 90.0);
        pwS2 = c13pulsepw("co", "ca", "sinc", 180.0);
        pwS3 = c13pulsepw("ca","co","square",180.0);
        pwS4 = c13pulsepw("co", "ca", "sinc", 90.0);

    /* the 180 pulse on CO at the middle of t1 */
        if (pwS2 > 2.0*pwN) pwZ = pwS2; else pwZ = 2.0*pwN;
        if ((pwS==0.0) && (pwS2>2.0*pwN)) pwZ1=pwS2-2.0*pwN; else pwZ1=0.0;
        if ( ni > 1 )     pwS = 180.0;
        if ( pwS > 0 )   phshift = 140.0;
        else             phshift = 0.0;

   tpwrs = tpwr - 20.0*log10(pwHs/(compH*pw*1.69));   /*needs 1.69 times more*/
   tpwrs = (int) (tpwrs);                          /*power than a square pulse */
   widthHd = 2.681*waltzB1/sfrq;  /* bandwidth of H1 WALTZ16 decoupling */
   pwHd = h1dec90pw("WALTZ16", widthHd, 0.0);     /* H1 90 length for WALTZ16 */


/* CHECK VALIDITY OF PARAMETER RANGES */

    if((dm[A] == 'y' || dm[B] == 'y' || dm[C] == 'y' ))
    {
        printf("incorrect dec1 decoupler flags!  ");
        psg_abort(1);
    }

    if((dm2[A] == 'y' || dm2[B] == 'y' ))
    {
        printf("incorrect dec2 decoupler flags! Should be 'nny' ");
        psg_abort(1);
    }

    if( satpwr > 6 )
    {
        printf("TSATPWR too large !!!  ");
        psg_abort(1);
    }

    if( dpwr > 46 )
    {
        printf("don't fry the probe, DPWR too large!  ");
        psg_abort(1);
    }

    if( dpwr2 > 46 )
    {
        printf("don't fry the probe, DPWR2 too large!  ");
        psg_abort(1);
    }

    if( pwClvl > 62 )
    {
        printf("don't fry the probe, pwClvl too large!  ");
        psg_abort(1);
    }

    if( pw > 200.0e-6 )
    {
        printf("dont fry the probe, pw too high ! ");
        psg_abort(1);
    } 
    if( pwN > 200.0e-6 )
    {
        printf("dont fry the probe, pwN too high ! ");
        psg_abort(1);
    } 
    if( pwC > 200.0e-6 )
    {
        printf("dont fry the probe, pwC too high ! ");
        psg_abort(1);
    } 

    if( pwS3 > 200.0e-6 )
    {
        printf("dont fry the probe, pwS3 too high ! ");
        psg_abort(1);
    }

    if( gt3 > 2.5e-3 ) 
    {
        printf("gt3 is too long\n");
        psg_abort(1);
    }
    if( gt1 > 10.0e-3 || gt2 > 10.0e-3 || gt4 > 10.0e-3 || gt5 > 10.0e-3
        || gt6 > 10.0e-3 || gt7 > 10.0e-3 || gt8 > 10.0e-3
	|| gt9 > 10.0e-3 || gt10 > 10.0e-3 || gt11 > 50.0e-6)
    {
        printf("gt values are too long. Must be < 10.0e-3 or gt11=50us\n");
        psg_abort(1);
    } 


/* PHASES AND INCREMENTED TIMES */


   /* Set up angles and phases */

   angle_CO=getval("angle_CO");  cos_CO=cos(PI*angle_CO/180.0);
   angle_Ca=getval("angle_Ca");  cos_Ca=cos(PI*angle_Ca/180.0);

   if ( (angle_CO < 0) || (angle_CO > 90) )
   {  printf ("angle_CO must be between 0 and 90 degree.\n"); psg_abort(1); }

   if ( (angle_Ca < 0) || (angle_Ca > 90) )
   {  printf ("angle_Ca must be between 0 and 90 degree.\n"); psg_abort(1); }

   if ( 1.0 < (cos_CO*cos_CO + cos_Ca*cos_Ca) )
   {
       printf ("Impossible angles.\n"); psg_abort(1);
   }
   else
   {
           cos_N=sqrt(1.0- (cos_CO*cos_CO + cos_Ca*cos_Ca));
           angle_N = 180.0*acos(cos_N)/PI;
   }

   swTilt=swCO*cos_CO + swCa*cos_Ca + swN*cos_N;

   if (ix ==1)
   {
      printf("\n\nn\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n\n");
      printf ("Maximum Sweep Width: \t\t %f Hz\n", swTilt);
      printf ("Angle_CO:\t%6.2f\n", angle_CO);
      printf ("Angle_Ca:\t%6.2f\n", angle_Ca);
      printf ("Angle_N :\t%6.2f\n", angle_N );
   }

/* Set up hyper complex */

   /* sw1 is used as symbolic index */
   if ( sw1 < 1000 ) { printf ("Please set sw1 to some value larger than 1000.\n"); psg_abort(1); }

   if (ix == 1) d2_init = d2;
   t1_counter = (int) ( (d2-d2_init)*sw1 + 0.5 );
   if (t1_counter % 2)  { tsadd(t2,2,4); tsadd(t6,2,4); }

   if (phase1 == 1)  { ;}                                                  /* CC */
   else if (phase1 == 2)  { tsadd(t5,1,4);}                                /* SC */
   else if (phase1 == 3)  { tsadd(t1,1,4); }                               /* CS */
   else if (phase1 == 4)  { tsadd(t5,1,4); tsadd(t1,1,4); }                /* SS */
   else { printf ("phase1 can only be 1,2,3,4. \n"); psg_abort(1); }

   if (phase2 == 2)  { tsadd(t4,2,4); icosel = 1; }                      /* N  */
            else                       icosel = -1;

   tau1 = 1.0*t1_counter*cos_Ca/swTilt;
   tau2 = 1.0*t1_counter*cos_CO/swTilt;
   tau3 = 1.0*t1_counter*cos_N/swTilt;

   tau1 = tau1/2.0;  tau2 = tau2/2.0;  tau3 = tau3/2.0;


/* CHECK VALIDITY OF PARAMETER RANGES */

    if (bigTN - 0.5*ni*(cos_N/swTilt) + pwS2 < 0.2e-6)
       { printf(" ni is too big. Make ni equal to %d or less.\n",
         ((int)((bigTN + pwS2)*2.0*swTilt/cos_N)));              psg_abort(1);}


     if (bigTCo - 0.5*ni*(cos_CO/swTilt) - 4.0e-6 - POWER_DELAY < 0.2e-6)
       {
        printf(" ni is too big for CO. Make ni equal to %d or less.\n",
        (int) ((bigTCo -  4.0e-6 - POWER_DELAY) / (0.5*cos_CO/swTilt)) );
        psg_abort(1);
        }


/* BEGIN ACTUAL PULSE SEQUENCE */

status(A);
   obsoffset(tof);
   set_c13offset("ca");		/* set Dec1 carrier at Co		      */
   obspower(satpwr);      /* Set transmitter power for 1H presaturation */
   obspwrf(4095.0);
   decpower(pwClvl);       /* Set Dec1 power for hard 13C pulses         */
   decpwrf(4095.0);
   dec2power(pwNlvl);      /* Set Dec2 power for hard 15N pulses         */
   dec2pwrf(4095.0);
   sim3_c13pulse("", "ca", "co", "sinc", "", 0.0, 180.0, 0.0, /* to produce shape  */
                             zero, zero, zero, 2.0e-6, 2.0e-4);
   set_c13offset("co");		/* set Dec1 carrier at Co		      */

/* Presaturation Period */

   if (satmode[0] == 'y')
   {
	delay(2.0e-5);
        rgpulse(d1,zero,2.0e-6,2.0e-6); /* presaturation */
   	obspower(tpwr);      /* Set transmitter power for hard 1H pulses */
	delay(2.0e-5);
	if(fscuba[0] == 'y')
	{
		delay(2.2e-2);
		rgpulse(pw,zero,2.0e-6,0.0);
		rgpulse(2*pw,one,2.0e-6,0.0);
		rgpulse(pw,zero,2.0e-6,0.0);
		delay(2.2e-2);
	}
   }
   else
   {
    delay(d1);
   }
   obspower(tpwr);           /* Set transmitter power for hard 1H pulses */
   txphase(three);
   dec2phase(zero);
   delay(1.0e-5);

/* Begin Pulses */

status(B);

   rcvroff();
   shiftedpulse("sinc", pwHs, 90.0, 0.0, three, 2.0e-6, 2.0e-6);
   txphase(zero);


/*   xxxxxxxxxxxxxxxxxxxxxx    1HN to 15N TRANSFER   xxxxxxxxxxxxxxxxxx    */

   rgpulse(pw,zero,0.0,0.0);                    /* 90 deg 1H pulse */

   delay(0.2e-6);
   zgradpulse(gzlvl1, gt1);
   delay(2.0e-6);

   delay(taua - gt1 - 2.2e-6);   /* taua <= 1/4JNH */ 

   sim3pulse(2*pw,0.0,2*pwN,zero,zero,zero,0.0,0.0);

   txphase(one); dec2phase(zero); decphase(zero); 

   delay(taua - gt1 - gstab -0.2e-6 - 2.0e-6);

   delay(0.2e-6);
   zgradpulse(gzlvl1, gt1);
   delay(gstab);

/*   xxxxxxxxxxxxxxxxxxxxxx    15N to 13CO TRANSFER   xxxxxxxxxxxxxxxxxx    */

   rgpulse(pw,one,2.0e-6,0.0);

   delay(0.2e-6);
   zgradpulse(gzlvl2, gt2);
   delay(gstab);

   dec2rgpulse(pwN,zero,0.0,0.0);

   delay(kappa - POWER_DELAY - PWRF_DELAY - pwHd - 4.0e-6 - PRG_START_DELAY);
                            /* delays for h1waltzon subtracted */
   h1waltzon("WALTZ16", widthHd, 0.0);
   decphase(zero);
   dec2phase(zero);
   delay(zeta - kappa - WFG3_START_DELAY);

   dec2rgpulse(2*pwN,zero,0.0,0.0);
   c13pulse("co", "ca", "sinc", 180.0, zero, 0.0, 0.0);
   dec2phase(zero);

   delay(zeta - 2.0e-6);

   dec2rgpulse(pwN,zero,2.0e-6,0.0);

   h1waltzoff("WALTZ16", widthHd, 0.0);

   dec2phase(zero); decphase(zero);

   delay(0.2e-6);
/* CHECK Negative gradient */
   zgradpulse(-gzlvl3, gt3);
   delay(gstab);

/* xxxxxxxxxxxxxxxxxxxxx 13CO to 13CA TRANSFER xxxxxxxxxxxxxxxxxxxxxxx  */

   c13pulse("co", "ca", "sinc", 90.0, zero, 2.0e-6, 0.0);

                delay(2.0e-7);
                zgradpulse(gzlvl10, gt10);

  delay(tauc -  gt10 - 0.2e-6 - (0.5*10.933*pwC));

        decrgpulse(pwC*158.0/90.0, zero, 0.0, 0.0);
        decrgpulse(pwC*171.2/90.0, two, 0.0, 0.0);
        decrgpulse(pwC*342.8/90.0, zero, 0.0, 0.0);      /* Shaka 6 composite */
        decrgpulse(pwC*145.5/90.0, two, 0.0, 0.0);
        decrgpulse(pwC*81.2/90.0, zero, 0.0, 0.0);
        decrgpulse(pwC*85.3/90.0, two, 0.0, 0.0);

                delay(2.0e-7);
                zgradpulse(gzlvl10, gt10);

      delay(tauc -  4.0e-6 - gt10 - 0.2e-6 - (0.5*10.933*pwC));

   c13pulse("co", "ca", "sinc", 90.0, one, 4.0e-6, 0.0);

   set_c13offset("ca");   /* change Dec1 carrier to Ca (55 ppm) */
   delay(0.2e-6);
   zgradpulse(gzlvl9, gt9);
   decphase(t5);
   delay(gstab);

/* xxxxxxxxxxxxxxxxxx 13CA EVOLUTION xxxxxxxxxxxxxxxxxxxxxx */

   h1waltzon("WALTZ16", widthHd, 0.0);
   c13pulse("ca", "co", "square", 90.0, t5, 2.0e-6, 0.0);      /*  pwS1  */

 if (fc180[A]=='n')
  {
   if ((ni>1.0) && (tau1>0.0))
    {
     if (tau1 - 2.0*pwS1/PI - WFG3_START_DELAY - PRG_START_DELAY - 2*POWER_DELAY -
        PRG_STOP_DELAY - 2.0*PWRF_DELAY - 0.5*pwZ > 0.0)
      {
       decpower(cbpwr);
       decphase(zero);
       decprgon(cbdecseq,1/cbdmf,cbres);
       decon();

       delay(tau1 - 2.0*pwS1/PI - WFG3_START_DELAY - PRG_START_DELAY - 2*POWER_DELAY -
        PRG_STOP_DELAY - 2.0*PWRF_DELAY - 0.5*pwZ);
       decoff();
       decprgoff();

       decpower(pwClvl);
       decphase(zero); dec2phase(zero);

       sim3_c13pulse("", "co", "ca", "sinc", "", 0.0, 180.0, 2.0*pwN,
                             zero, zero, zero, 2.0e-6, 2.0e-6);

       decpower(cbpwr);
       decphase(zero);
       decprgon(cbdecseq,1/cbdmf,cbres);
       decon();

       delay(tau1 - 2.0*pwS1/PI - PRG_START_DELAY - 2*POWER_DELAY -
        PRG_STOP_DELAY - WFG_START_DELAY - 2.0*PWRF_DELAY - 0.5*pwZ);
       decoff();
       decprgoff();
       decpower(pwClvl);

       initval(140.0, v9);
       decstepsize(1.0);
       dcplrphase(v9);

      }
       else
      {
       tsadd(t6,2,4);
       delay(2.0*tau1);
       delay(10.0e-6); 
       sim3_c13pulse("", "ca", "co", "sinc", "", 0.0, 180.0, 2.0*pwN,
                             zero, zero, zero, 2.0e-6, 2.0e-6);

       delay(10.0e-6);
      }
    }
     else
    {

       tsadd(t6,2,4);
       delay(10.0e-6);
	    sim3_c13pulse("", "co", "ca", "sinc", "", 0.0, 180.0, 2.0*pwN,
                             zero, zero, zero, 2.0e-6, 2.0e-6);
       delay(10.0e-6);
    }
  }
   else
  {
   /* for checking sequence */
   c13pulse("ca", "co", "square", 180.0, zero, 2.0e-6, 0.0);
  }

   decphase(t7);
   c13pulse("ca", "co", "square", 90.0, t7, 4.0e-6, 0.0);      /*  pwS1  */
   dcplrphase(zero);
   h1waltzoff("WALTZ16", widthHd, 0.0);
 
   set_c13offset("co");   /* set carrier back to Co */

   delay(0.2e-6);

   zgradpulse(gzlvl12, gt12);
   delay(gstab);


/* xxxxxxxxxxxxxxx  13CA to 13CO TRANSFER and CT 13CO EVOLUTION xxxxxxxxxxxxxxxxx */

   c13pulse("co", "ca", "sinc", 90.0, t1, 2.0e-6, 0.0);

   delay(tau2);
   dec2rgpulse(pwN,one,0.0,0.0);
   dec2rgpulse(2*pwN,zero,0.0,0.0);
   dec2rgpulse(pwN,one,0.0,0.0);

   delay(taud - 4.0*pwN - POWER_DELAY
         - 0.5*(WFG_START_DELAY + pwS3 + WFG_STOP_DELAY));

   c13pulse("ca", "co", "square", 180.0, zero, 2.0e-6, 0.0);
   decphase(t8);

                initval(1.0,v4);
                decstepsize(sphase);
                dcplrphase(v4);

      delay(bigTCo - taud
            - 0.5*(WFG_START_DELAY + pwS3 + WFG_STOP_DELAY) );

      c13pulse("co", "ca", "sinc", 180.0, t8, 2.0e-6, 0.0);
      dcplrphase(zero); decphase(one);

    delay(bigTCo - tau2 - POWER_DELAY - 4.0e-6);

   c13pulse("co", "ca", "sinc", 90.0, one, 4.0e-6, 0.0);

   delay(0.2e-6);
   zgradpulse(gzlvl4, gt4);
   delay(gstab);

   h1waltzon("WALTZ16", widthHd, 0.0);

/* t3 period */
   dec2rgpulse(pwN,t2,2.0e-6,0.0);

   dec2phase(t3);

   delay(bigTN - tau3 + pwS2);


     dec2rgpulse(2*pwN,t3,0.0,0.0);
     c13pulse("co", "ca", "sinc", 180.0, zero, 0.0, 0.0);

   dec2phase(t4);

   if (tau3 > (kappa + PRG_STOP_DELAY + pwHd + 2.0e-6))
   {
       delay(bigTN - pwS3 - WFG_START_DELAY - 2.0*POWER_DELAY
                                - 2.0*PWRF_DELAY - 2.0e-6);

      c13pulse("ca", "co", "square", 180.0, zero, 2.0e-6, 0.0);

       delay(tau3 - kappa - PRG_STOP_DELAY - pwHd - 2.0e-6 - POWER_DELAY
                                         - PWRF_DELAY);
       h1waltzoff("WALTZ16", widthHd, 0.0);
       txphase(zero);

       delay(kappa - gt5 - 2.0*GRADIENT_DELAY - 1.0e-4);
       zgradpulse(gzlvl5, gt5);        /* 2.0*GRADIENT_DELAY */
       delay(1.0e-4);
   }
   else if (tau3 > (kappa - pwS3 - WFG_START_DELAY - 2.0*POWER_DELAY
                                - 2.0*PWRF_DELAY - 2.0e-6))
   {
      delay(bigTN + tau3 - kappa - PRG_STOP_DELAY - pwHd - 2.0e-6
                                 - POWER_DELAY - PWRF_DELAY);
      h1waltzoff("WALTZ16", widthHd, 0.0);
      txphase(zero);

      c13pulse("ca", "co", "square", 180.0, zero, 2.0e-6, 0.0);

      delay(kappa - pwS3 - WFG_START_DELAY - 2.0*POWER_DELAY
            - 2.0*PWRF_DELAY - 2.0e-6 - gt5 - 2.0*GRADIENT_DELAY - 1.0e-4);
      zgradpulse(gzlvl5, gt5);        /* 2.0*GRADIENT_DELAY */
      delay(1.0e-4);
   }
   else if (tau3 > gt5 + 2.0*GRADIENT_DELAY + 1.0e-4)
   {
      delay(bigTN + tau3 - kappa - PRG_STOP_DELAY - pwHd - 2.0e-6
                                 - POWER_DELAY - PWRF_DELAY);
      h1waltzoff("WALTZ16", widthHd, 0.0);
      txphase(zero);
      delay(kappa - tau3 - pwS3 - WFG_START_DELAY - 2.0*POWER_DELAY
                                   - 2.0*PWRF_DELAY - 2.0e-6);

      c13pulse("ca", "co", "square", 180.0, zero, 2.0e-6, 0.0);

      delay(tau3 - gt5 - 2.0*GRADIENT_DELAY - 1.0e-4);
      zgradpulse(gzlvl5, gt5);        /* 2.0*GRADIENT_DELAY */
      delay(1.0e-4);
   }
   else
   {
      delay(bigTN + tau3 - kappa - PRG_STOP_DELAY - pwHd - 2.0e-6
                                 - POWER_DELAY - PWRF_DELAY);
      h1waltzoff("WALTZ16", widthHd, 0.0);
      txphase(zero);
      delay(kappa - tau3 - pwS3 - WFG_START_DELAY - 2.0*POWER_DELAY
            - 2.0*PWRF_DELAY - 2.0e-6 - gt5 - 2.0*GRADIENT_DELAY - 1.0e-4);
      zgradpulse(gzlvl5, gt5);        /* 2.0*GRADIENT_DELAY */
      delay(1.0e-4);

      c13pulse("ca", "co", "square", 180.0, zero, 2.0e-6, 0.0);
      delay(tau3);
   }

   sim3pulse(pw,0.0,pwN,zero,zero,t4,0.0,0.0);

   delay(0.2e-6);
   zgradpulse(gzlvl6, gt6);
   delay(2.0e-6);

   dec2phase(zero);
   delay(taub - gt6 - 2.2e-6);

   sim3pulse(2.0*pw,0.0,2.0*pwN,zero,zero,zero,0.0,0.0);

   delay(0.2e-6);
   zgradpulse(gzlvl6, gt6);
   delay(200.0e-6);
   
   txphase(one);
   dec2phase(one);

   delay(taub - gt6 - 200.2e-6);

   sim3pulse(pw,0.0,pwN,one,zero,one,0.0,0.0);

   delay(0.2e-6);
   zgradpulse(gzlvl7, gt7);
   delay(2.0e-6);
 
   txphase(zero);
   dec2phase(zero);

   delay(taub - gt7 - 2.2e-6);

   sim3pulse(2.0*pw,0.0,2.0*pwN,zero,zero,zero,0.0,0.0);

   delay(0.2e-6);
   zgradpulse(gzlvl7, gt7);
   delay(200.0e-6);

   delay(taub - gt7 - 200.2e-6);

   rgpulse(pw, zero, 0.0, 0.0);
   delay(gt8 + 1.0e-4 + 1.0e-4 - 0.3*pw + 2.0*GRADIENT_DELAY
                                   + POWER_DELAY);

   rgpulse(2*pw,zero,0.0,0.0);
   dec2power(dpwr2);
   decpower(dpwr);
   zgradpulse(icosel*gzlvl8, gt8);
   delay(1.0e-4);
   

/*   rcvron();  */          /* Turn on receiver to warm up before acq */

/* BEGIN ACQUISITION */

statusdelay(C, 1.0e-4);
         setreceiver(t6);
}
Example #17
0
pulsesequence()
{

  double j1min = getval("j1min"),
         j1max = getval("j1max"),
         gzlvlE = getval("gzlvlE"),
         gtE = getval("gtE"),
         mult = getval("mult"),
	 pwx180 = getval("pwx180"),
	 pwxlvl180 = getval("pwxlvl180"),
	 pw180 = getval("pw180"),
         pwx180r = getval("pwx180r"),
         pwxlvl180r = getval("pwxlvl180r"),
	 tpwr180 = getval("tpwr180"),
         EDratio = getval("EDratio"),
         hsglvl = getval("hsglvl"),
         hsgt = getval("hsgt"),
         gstab = getval("gstab"),
         dmfct = getval("dmfct"),
         dpwrct = getval("dpwrct"),
         tau,
	 tau1,
	 tau3,
	 taug,
         bigT = getval("BigT");

  char   pwx180ad[MAXSTR],
	 pw180ad[MAXSTR],
	 dmct[MAXSTR],
	 bipflg[MAXSTR],
         pwx180ref[MAXSTR],
         dmmct[MAXSTR];

  int	 icosel,
         igcorr,
         prgcycle = (int)(getval("prgcycle")+0.5),
	 phase1 = (int)(getval("phase")+0.5);

//synchronize gradients to srate for probetype='nano'
//   Preserve gradient "area"
        gtE = syncGradTime("gtE","gzlvlE",1.0);
        gzlvlE = syncGradLvl("gtE","gzlvlE",1.0);

  getstr("pwx180ad",pwx180ad);
  getstr("pw180ad",pw180ad);
  getstr("dmct",dmct);
  getstr("pwx180ref", pwx180ref);
  getstr("dmmct", dmmct);

  getstr("bipflg",bipflg);
  if (bipflg[0] == 'y')
  {
        tpwr180=getval("tnbippwr");
        pw180=getval("tnbippw");
        getstr("tnbipshp",pw180ad);
  }
  if (bipflg[1] == 'y')
  {
        pwxlvl180=getval("dnbippwr");
        pwx180=getval("dnbippw");
        getstr("dnbipshp",pwx180ad);
  }

  tau1 = 1/(2*(j1min + 0.07*(j1max - j1min)));
  tau3 = 1/(2*(j1max - 0.07*(j1max - j1min)));
  tau = 1 / (j1min+j1max);

  taug = tau + getval("tauC");

  icosel = 1;
  igcorr = 2;
  
  if (mult > 0.5)
    igcorr = 1;

  assign(ct,v17);
  assign(zero,v18);
  assign(zero,v19);

  if (getflag("prgflg") && (satmode[0] == 'y') && (prgcycle > 1.5))
    {
        hlv(ct,v17);
        mod2(ct,v18); dbl(v18,v18);
        if (prgcycle > 2.5)
           {
                hlv(v17,v17);
                hlv(ct,v19); mod2(v19,v19); dbl(v19,v19);
           }
     }

  settable(t1, 4, ph1);
  settable(t2, 8, ph2);
  settable(t3, 16, ph3);
  settable(t6, 2, ph6);
  getelem(t1, v17, v1);
  getelem(t3, v17, v3);
  getelem(t2, v17, v2);
  getelem(t6, v17, oph);
  assign(zero, v4);

  assign(zero,v6);
  add(oph,v18,oph);
  add(oph,v19,oph);

  initval(2.0*(double)(((int)(d2*getval("sw1")+0.5)%2)),v14);
/*
  mod2(id2, v14);
  dbl(v14,v14);
*/
  add(v2, v14, v2);
  add(v4, v14, v4);
  add(oph, v14, oph);

  if ((phase1 == 2) || (phase1 == 5))
    icosel = -1;

  status(A);

   delay(5.0e-5);
   if (getflag("sspul"))
        steadystate();

   if (satmode[0] == 'y')
     {
        if ((d1-satdly) > 0.02)
                delay(d1-satdly);
        else
                delay(0.02);
        if (getflag("slpsat"))
           {
                shaped_satpulse("relaxD",satdly,zero);
                if (getflag("prgflg"))
                   shaped_purge(v6,zero,v18,v19);
           }
        else
           {
                satpulse(satdly,zero,rof1,rof1);
                if (getflag("prgflg"))
                   purge(v6,zero,v18,v19);
           }
     }
   else
        delay(d1);

   if (getflag("wet"))
     wet4(zero,one);

    obspower(tpwr);
    decpower(pwxlvl);

    if (getflag("nullflg"))
    {
      decpower(pwxlvl180);
      rgpulse(0.5 * pw, zero, rof1, rof1);
      obspower(tpwr180);
      delay(tau/2.0);
      simshaped_pulse(pw180ad,pwx180ad,pw180,pwx180,zero,zero,rof1,rof1);
      delay(tau/2.0+POWER_DELAY+rof1);
      delay(tau/2.0+POWER_DELAY+rof1);
      simshaped_pulse(pw180ad,pwx180ad,pw180,pwx180,two,two,rof1,rof1);
      obspower(tpwr);
      delay(tau/2.0);
      rgpulse(0.5 * pw, zero, rof1, rof1);
      decpower(pwxlvl);
      zgradpulse(hsglvl, 1.4*hsgt);
      delay(1e-3);
    }

  status(B);

    rgpulse(pw, zero, rof1, rof1);
  if (getflag("dmct"))
  {
    decpower(dpwrct);
    decprgon("garp1",1/dmfct,1.0);
/*
    setstatus(DECch, FALSE, 'g', FALSE, dmfct);
*/
    decunblank();
    decon();
  }
    obspower(tpwr180);
    delay(bigT/2 - d2/2  - tau - taug - pwx180r);
    delay(pw180+WFG_START_DELAY+WFG_STOP_DELAY);
    shaped_pulse(pw180ad,pw180,zero,rof1,rof1);
    delay(bigT/2 - d2/2  - tau - taug - pwx180r);
    delay(4*pw/PI+2*rof1+POWER_DELAY+4*pwx/PI+2*POWER_DELAY);
  if (getflag("dmct"))
  {
    decoff();
    decblank();
    decprgoff();
/*
    setstatus(DECch, FALSE, 'c', FALSE, dmf);
*/
    decpower(pwxlvl);
  }

    if (mult > 0.5)
    {
     delay(tau-gtE-2*GRADIENT_DELAY-gstab);
     zgradpulse(icosel*gzlvlE,gtE);
     delay(gstab);
    }
    else
    {
     delay(tau);
    }

    decrgpulse(pwx,v2,rof1,rof1);

    if (mult > 0.5)
    {
    decpower(pwxlvl180r);
    delay(taug);
    decshaped_pulse(pwx180ref, pwx180r, v4, rof1, rof1);

    delay(d2/2);
    shaped_pulse(pw180ad,pw180,zero,rof1,rof1);
    delay(d2/2);
    zgradpulse(icosel*gzlvlE,gtE);

    delay(taug-gtE-2*GRADIENT_DELAY+(4*pwx/PI+2*rof1+2*POWER_DELAY-(WFG_START_DELAY+pw180+WFG_STOP_DELAY+2*rof1)));
    decshaped_pulse(pwx180ref, pwx180r, v3, rof1, rof1);
    }

    else
    {
    decpower(pwxlvl180);
    delay(taug/2+(pwx180r-pwx180)/2);
    decshaped_pulse(pwx180ad, pwx180, v4, rof1, rof1);
    delay(taug/2+(pwx180r-pwx180)/2.0-gtE-2*GRADIENT_DELAY-gstab);

    zgradpulse(icosel*gzlvlE,gtE);
    delay(gstab);

    delay(d2/2);
    shaped_pulse(pw180ad,pw180,zero,rof1,rof1);
    delay(d2/2);

    zgradpulse(icosel*gzlvlE,gtE);

    delay(taug/2+(pwx180r-pwx180)/2.0+(4*pwx/PI+2*rof1+2*POWER_DELAY-WFG_START_DELAY-pw180-WFG_STOP_DELAY-2*rof1)-gtE-2*GRADIENT_DELAY);
    decshaped_pulse(pwx180ad, pwx180, v3, rof1, rof1);
  
    delay(taug/2+(pwx180r-pwx180)/2);
    }

    decpower(pwxlvl);
    decrgpulse(pwx,v1,rof1,rof1);

    obspower(tpwr);

    delay(tau);

    rgpulse(pw,one,rof1,rof2);
    decrgpulse(pwx,zero,rof1,rof1);
    obspower(tpwr180);
    zgradpulse(igcorr*3*gzlvlE/(10*EDratio),gtE);
    delay(tau3 - gtE - 2*GRADIENT_DELAY);
    decrgpulse(pwx,zero,rof1,rof1);
    zgradpulse(igcorr*7*gzlvlE/(10*EDratio),gtE);
    delay(tau - gtE - 2*GRADIENT_DELAY);
    decrgpulse(pwx,zero,rof1,rof1);
    shaped_pulse(pw180ad,pw180,zero,rof1,rof1);
    zgradpulse(igcorr*2*gzlvlE/EDratio,gtE);
    delay(tau1 - gtE - 2*GRADIENT_DELAY - POWER_DELAY);
    decpower(dpwr);

  status(C);

    delay(tau+tau3+3*pwx+6*rof1-tau1+WFG_START_DELAY+WFG_STOP_DELAY);
}
Example #18
0
pulsesequence()
{
 char       f1180[MAXSTR],   
            f2180[MAXSTR],  
            mag_flg[MAXSTR],
            flg_3919[MAXSTR],
            ref_flg[MAXSTR];

 int         phase, ni2,
             t1_counter,   
             t2_counter;   

 double      gzcal = getval("gzcal"),
             factor = 0.08, /* used for 3-9-19 water gate */
             tau_3919 = getval("tau_3919"),
             flipphase = getval("flipphase"),
             tau1,         /*  t1 delay */
             tau2,         /*  t2 delay */
             taua,         /*  1/4JNH   ~ 2.3 ms   */
             taub,        /*  1/4JNH    ~ 2.3 ms  */
             bigT,         /* ~ 19  ms   */

             pwNlvl,       
             pwN,  
             gt1,
             gt2,
             gt3,
             gt4,
             gt5,
             gt6,
             gt7,
             gt8,
             gzlvl1,
             gzlvl2,
             gzlvl3,
             gzlvl4,
             gzlvl5,
             gzlvl6,
             gzlvl7,
             gzlvl8,


  compH = getval("compH"),         /* adjustment for C13 amplifier compression */
  pwHs = getval("pwHs"),	        /* H1 90 degree pulse length at tpwrs */
  tpwrsf = getval("tpwrsf"),     /* fine power adjustment for flipback pulse   */
  tpwrs;	  	              /* power for the pwHs ("H2Osinc") pulse */
	
/* LOAD VARIABLES */

  getstr("f1180",f1180);
  getstr("f2180",f2180);
  getstr("flg_3919", flg_3919);
  getstr("mag_flg", mag_flg);
  getstr("ref_flg", ref_flg);

  taua   = getval("taua"); 
  taub   = getval("taub"); 
  bigT   = getval("bigT");
   
  tpwr = getval("tpwr");
  pwNlvl = getval("pwNlvl");
  pwN = getval("pwN");
  
  dpwr = getval("dpwr");
  dpwr2 = getval("dpwr2");
  phase = (int)( getval("phase") + 0.5);
  phase2 = (int)( getval("phase2") + 0.5);
  sw1 = getval("sw1");
  sw2 = getval("sw2");  
  ni = getval("ni");
  ni2 = getval("ni2");
  
  gt1 = getval("gt1");
  gt2 = getval("gt2");
  gt3 = getval("gt3");
  gt4 = getval("gt4");
  gt5 = getval("gt5");
  gt6 = getval("gt6");
  gt7 = getval("gt7");
  gt8 = getval("gt8");
  
  gzlvl1 = getval("gzlvl1");
  gzlvl2 = getval("gzlvl2");
  gzlvl3 = getval("gzlvl3");
  gzlvl4 = getval("gzlvl4");
  gzlvl5 = getval("gzlvl5");
  gzlvl6 = getval("gzlvl6");
  gzlvl7 = getval("gzlvl7");
  gzlvl8 = getval("gzlvl8");

/* LOAD PHASE TABLE */
           
  settable(t1,4,phi1);
  settable(t2,2,phi2);
  settable(t3,8,phi3);
  settable(t4,16, phi4);

  if (ref_flg[A] == 'y')
  {
     settable(t10,8,ref);
  }
  else
  {
     settable(t10,8,rec);
  }
  

/* selective H20 one-lobe sinc pulse */
    tpwrs = tpwr - 20.0*log10(pwHs/(compH*pw*1.69));   /*needs 1.69 times more*/
    tpwrs = (int) (tpwrs);                   	  /*power than a square pulse */

/* CHECK VALIDITY OF PARAMETER RANGES */

    if (ref_flg[A] == 'y' && ni > 1)
    {
       printf(" Incorrect setting of ni and ref_flg.\n");
       printf(" Please choose either ni=1 or ref_flg=n.\n");
       psg_abort(1);
    }
    
    if (ref_flg[A] == 'y' && dps_flag)
    {
       printf(" Please use phase2 and ni2 for 2D reference spectrum\n");
       if (ni2/sw2 > 2.0*(2.0*bigT - gt5 - 200.0e-6))
       {
           printf("ni2 is too big, should be < %f\n", 2.0*sw2*(2.0*bigT-gt5-200.0e-6));
           psg_abort(1);
       }
    }

    if ((ni2/sw2 > 2.0*(bigT -  gt5 - 200.0e-6)) && (ref_flg[A] !='y'))
    {
       printf(" ni2 is too big, should be < %f\n", 2.0*sw2*(bigT-gt6-200.0e-6));
       psg_abort(1);
    }

    if(dpwr2 > 50)
    {
        printf("don't fry the probe, dpwr2 is  too large!  ");
        psg_abort(1);
    }

    if((dm[A] == 'y' || dm[B] == 'y' || dm[C] == 'y'))
    {
       printf("incorrect dec1 decoupler flags! should be 'nnn' ");
       psg_abort(1);
    }

    if((dm2[A] == 'y' || dm2[B] == 'y' ))
    {
        printf("incorrect dec2 decoupler flags! Should be 'nny' ");
        psg_abort(1);
    }

/*  Phase incrementation for hypercomplex 2D data */

    if (phase == 2)
    {
       tsadd(t1,1,4);
    }
  
    if (phase2 == 2)
    {
       tsadd(t2,1,4);   
    }

/*  Set up f1180  half_dwell time (1/sw1)/2.0           */
   
    tau1 = d2 - (4.0*pw/PI + 2.0*pwN);
    if(f1180[A] == 'y')
    {
        tau1 += (1.0/(2.0*sw1));
    }
    if(tau1 < 0.2e-6) tau1 = 0.0;
    tau1 = tau1/2.0;

/*  Set up f2180   half dwell time (1/sw2)/2.0              */

    tau2 = d3;
    if(f2180[A] == 'y')
    {
        tau2 += (1.0/(2.0*sw2)); 
    }
    if(tau2 < 0.2e-6) tau2 = 0.0;
    tau2 = tau2/2.0;


/* Calculate modifications to phases for States-TPPI acquisition          */

   if( ix == 1) d2_init = d2 ;
 
   t1_counter = (int)((d2-d2_init)*sw1 + 0.5);
   if(t1_counter % 2) 
   {
      tsadd(t1,2,4);     
      tsadd(t10,2,4);    
   }
   
   if( ix == 1) d3_init = d3 ;
   t2_counter = (int)((d3-d3_init)*sw2 + 0.5);
   if(t2_counter % 2) 
   {
      tsadd(t2,2,4);  
      tsadd(t10,2,4);    
   }

   if (flipphase < -0.01)  flipphase = flipphase + 360.0;
   initval(flipphase, v10);
   obsstepsize(0.25);


/* BEGIN ACTUAL PULSE SEQUENCE */

status(A);
   obspower(tpwr);
   dec2power(pwNlvl);
   txphase(zero);
   dec2phase(zero);

   delay(d1);

   if(gt1 > 0.2e-6)
   {
      dec2rgpulse(pwN, zero, 0.2e-6, 0.0);
      delay(2.0e-6);
      zgradpulse(gzlvl1, gt1);
      delay(0.001);
   }
   rcvroff();

status(B);

   rgpulse(pw, zero,rof1, 0.0);
   delay(2.0e-6);
   if (gt2 > 0.2e-6)
      zgradpulse(gzlvl2,gt2);
   delay(taua - gt2 - 2.0e-6);
   sim3pulse(2.0*pw,(double)0.0,2.0*pwN, zero, zero, zero, 0.0, 0.0);
   delay(taua - gt2 - 400.0e-6);
   if (gt2 > 0.2e-6)
   {
      zgradpulse(gzlvl2,gt2);
   }
   txphase(one);
   dec2phase(t2);
   delay(400.0e-6);
   rgpulse(pw, one, 0.0, 0.0);
   if (gt3 > 0.2e-6)
   {
      delay(2.0e-6);
      zgradpulse(gzlvl3, gt3);
      delay(200.0e-6);
   }
   txphase(zero);
   dec2rgpulse(pwN, t2, 0.0, 0.0);

   if (ref_flg[A] == 'y')
   {
      delay(tau2);
      rgpulse(2.0*pw, zero, 0.0, 0.0);
      dec2phase(t3);
      if (gt5 > 0.2e-6)
      {
         delay(2.0*bigT - gt5 - 2.0*pw - 1.0e-3);
         zgradpulse(gzlvl5, gt5);
         delay(1.0e-3);
         dec2rgpulse(2.0*pwN, t3, 0.0, 0.0);
         delay(2.0e-6);
         zgradpulse(gzlvl5, gt5);
         delay(2.0*bigT - tau2 - gt5 - 2.0e-6);
      }
      else
      {
         delay(2.0*bigT - 2.0*pw);
         dec2rgpulse(2.0*pwN, t3, 0.0, 0.0);
         delay(2.0*bigT - tau2);
      }
   }
   else
   {
      dec2phase(zero);
      if (gt4 > 0.2e-6)
      {
         delay(2.0e-6);
         zgradpulse(gzlvl4, gt4);
         delay(bigT - gt4 - 2.0e-6);
         sim3pulse(2.0*pw,(double)0.0, 2.0*pwN, zero,zero, zero, 0.0, 0.0);
         delay(2.0e-6);
         zgradpulse(gzlvl4, gt4);
         delay(1.0e-3 - 2.0e-6);
      }
      else
      {
         delay(bigT);
         sim3pulse(2.0*pw,(double)0.0, 2.0*pwN, zero,zero, zero, 0.0, 0.0);
         delay(1.0e-3);
         gt4 = 0.0;
      }

      zgradpulse(gzlvl5, gt5);
      txphase(t1);
      delay(bigT - gt4 - gt5 - 1.0e-3 - 2.0*GRADIENT_DELAY);

      rgpulse(pw, t1, 0.0, 0.0);
      delay(tau1);
      dec2rgpulse(2.0*pwN, t3, 0.0, 0.0);
      txphase(zero);
      delay(tau1);
      rgpulse(pw, zero, 0.0, 0.0);

      delay(2.0e-6);
      zgradpulse(gzlvl5, gt5);
      dec2phase(t4);

      if (gt6 > 0.2e-6)
      {
         delay(tau2 + 100.0e-6);
         zgradpulse(gzlvl6, gt6);
         delay(bigT - gt5 - gt6 - 100.0e-6 - 2.0*GRADIENT_DELAY);
         sim3pulse(2.0*pw,(double)0.0, 2.0*pwN, zero,zero, t4, 0.0, 0.0);
         delay(2.0e-6);
         dec2phase(zero);
         zgradpulse(gzlvl6, gt6);
         delay(bigT - tau2 - gt6 - 2.0e-6);
      }
      else
      {
         delay(bigT + tau2 - gt5 - 2.0*GRADIENT_DELAY);
         sim3pulse(2.0*pw,(double)0.0, 2.0*pwN, zero,zero, t4, 0.0, 0.0);
         dec2phase(zero);
         delay(bigT - tau2);
      }
   }

   if (gt7 > 0.2e-6)
   {
      dec2rgpulse(pwN, zero, 0.0,2.0e-6);
      zgradpulse(gzlvl7, gt7);
      txphase(zero);
      
      delay(200.0e-6);
      if (pwHs > 0.2e-6)
      {
         xmtrphase(v10);
         if (tpwrsf<4095.0) {obspower(tpwrs+6.0); obspwrf(tpwrsf);}
          else obspower(tpwrs);
         txphase(two);
         shaped_pulse("H2Osinc", pwHs, two, 2.0e-6, 0.0);
         xmtrphase(zero);
         obspower(tpwr); obspwrf(4095.0);
      }
      rgpulse(pw, zero, 2.0e-6, 0.0);
   }
   else
   {
      sim3pulse(pw,(double)0.0, pwN, zero,zero, zero, 0.0, 0.0);
   }


   delay(2.0e-6);
   if(mag_flg[A] == 'y')
   {
      magradpulse(gzcal*gzlvl8, gt8);
   }
   else
   {
      zgradpulse(gzlvl8, gt8);
   }
   if (flg_3919[A] == 'y')
   {
      delay(taub - 31.0*factor*pw - 2.5*tau_3919 - gt8 - 2.0e-6);
      rgpulse(pw*factor*3.0, two, 0.0, 0.0);
      delay(tau_3919);
      rgpulse(pw*factor*9.0, two, 0.0, 0.0);
      delay(tau_3919);
      rgpulse(pw*factor*19.0, two, 0.0, 0.0);
      delay(tau_3919/2.0 - pwN);
      dec2rgpulse(2.0*pwN, zero, 0.0, 0.0);
      delay(tau_3919/2.0 - pwN);
      rgpulse(pw*factor*19.0, zero, 0.0, 0.0);
      delay(tau_3919);
      rgpulse(pw*factor*9.0, zero, 0.0, 0.0);
      delay(tau_3919);
      rgpulse(pw*factor*3.0, zero, 0.0, 0.0);
      delay(taub - 31.0*factor*pw - 2.5*tau_3919 - gt8 - POWER_DELAY - 402.0e-6);
   }
   else
   {
      if (tpwrsf<4095.0) {obspower(tpwrs+6.0); obspwrf(tpwrsf);}
       else obspower(tpwrs);
      txphase(two);
      xmtrphase(v10);
      delay(taub - pwHs - gt8 - 2.0*POWER_DELAY - 2.0e-6);
      shaped_pulse("H2Osinc", pwHs, two, 0.0, 0.0);
      obspower(tpwr); obspwrf(4095.0);
      xmtrphase(zero);
      txphase(zero);
      sim3pulse(2.0*pw, (double)0.0, 2.0*pwN, zero, zero, zero, 2.0e-6, 0.0);
      if (tpwrsf<4095.0) {obspower(tpwrs+6.0); obspwrf(tpwrsf);}
       else obspower(tpwrs);
      txphase(two);
      xmtrphase(v10);
      shaped_pulse("H2Osinc", pwHs, two, 2.0e-6, 0.0);
      xmtrphase(zero);
      obspower(tpwr); obspwrf(4095.0);
      dec2power(dpwr2);
      delay(taub - pwHs  - gt8 - 3.0*POWER_DELAY - 402.0e-6);
   }
   dec2power(dpwr2);
   if(mag_flg[A] == 'y')
   {
      magradpulse(gzcal*gzlvl8, gt8);
   }
   else
   {
      zgradpulse(gzlvl8, gt8);
   }
   delay(400.0e-6);

status(C);
   setreceiver(t10);
   rcvron();
}
Example #19
0
pulsesequence()

{

    double   hsglvl = getval("hsglvl"),
             hsgt = getval("hsgt"),
             tau,
             taug,
             evolcorr,
             pwx180 = getval("pwx180"),
             pwxlvl180 = getval("pwxlvl180"),
             pwx180r = getval("pwx180r"),
             pwxlvl180r = getval("pwxlvl180r"),
             mult = getval("mult"),
             null = getval("null");
    int	    phase1 = (int)(getval("phase")+0.5),
            prgcycle = (int)(getval("prgcycle")+0.5),
            ZZgsign;

    char      pwx180ad[MAXSTR],
              pwx180adR[MAXSTR],
              pwx180ref[MAXSTR];

    getstr("pwx180ad", pwx180ad);
    getstr("pwx180adR", pwx180adR);
    getstr("pwx180ref", pwx180ref);
    tau  = 1/(4*(getval("j1xh")));
    evolcorr = (4*pwx/PI) + 2*pw + 8.0e-6;

    if (mult > 0.5)
        taug = 2*tau + getval("tauC");
    else
        taug = 0.0;
    ZZgsign=-1;
    if (mult == 2) ZZgsign=1;

    assign(ct,v17);
    assign(zero,v18);
    assign(zero,v19);

    if (getflag("prgflg") && (satmode[0] == 'y') && (prgcycle > 1.5))
    {
        hlv(ct,v17);
        mod2(ct,v18);
        dbl(v18,v18);
        if (prgcycle > 2.5)
        {
            hlv(v17,v17);
            hlv(ct,v19);
            mod2(v19,v19);
            dbl(v19,v19);
        }
    }

    settable(t1, 4, ph1);
    settable(t2, 2, ph2);
    settable(t3, 8, ph3);
    settable(t4, 16, ph4);
    settable(t5, 16, ph5);

    getelem(t1, v17, v1);
    getelem(t3, v17, v3);
    getelem(t4, v17, v4);
    getelem(t2, v17, v2);
    getelem(t5, v17, oph);

    assign(zero,v6);
    add(oph,v18,oph);
    add(oph,v19,oph);

    if (phase1 == 2)
        incr(v2);

    /*
      mod2(id2,v14);
      dbl(v14, v14);
    */
    initval(2.0*(double)(((int)(d2*getval("sw1")+0.5)%2)),v14);

    add(v2, v14, v2);
    add(oph, v14, oph);

    status(A);

    obspower(tpwr);

    delay(5.0e-5);
    if (getflag("sspul"))
        steadystate();

    if (satmode[0] == 'y')
    {
        if ((d1-satdly) > 0.02)
            delay(d1-satdly);
        else
            delay(0.02);
        if (getflag("slpsat"))
        {
            shaped_satpulse("relaxD",satdly,zero);
            if (getflag("prgflg"))
                shaped_purge(v6,zero,v18,v19);
        }
        else
        {
            satpulse(satdly,zero,rof1,rof1);
            if (getflag("prgflg"))
                purge(v6,zero,v18,v19);
        }
    }
    else
        delay(d1);

    if (getflag("wet"))
        wet4(zero,one);

    decpower(pwxlvl);

    status(B);

    if ((getflag("PFGflg")) && (getflag("nullflg")))
    {
        rgpulse(0.5 * pw, zero, rof1, rof1);
        delay(2 * tau);
        decpower(pwxlvl180);
        decshaped_pulse(pwx180ad, pwx180, zero, rof1, rof1);
        rgpulse(2.0 * pw, zero, rof1, rof1);
        delay(2 * tau + 2 * POWER_DELAY);
        decshaped_pulse(pwx180adR, pwx180, zero, rof1, rof1);
        decpower(pwxlvl);
        rgpulse(1.5 * pw, two, rof1, rof1);
        zgradpulse(hsglvl, hsgt);
        delay(1e-3);
    }
    else if (null != 0.0)
    {
        rgpulse(pw, zero, rof1, rof1);
        delay(2 * tau);
        decpower(pwxlvl180);
        decshaped_pulse(pwx180ad, pwx180, zero, rof1, rof1);
        rgpulse(2.0 * pw, zero, rof1, rof1);
        delay(2 * tau + 2 * POWER_DELAY);
        decshaped_pulse(pwx180adR, pwx180, zero, rof1, rof1);
        decpower(pwxlvl);
        rgpulse(pw, two, rof1, rof1);
        if (satmode[1] == 'y')
        {
            if (getflag("slpsat"))
                shaped_satpulse("BIRDnull",null,zero);
            else
                satpulse(null,zero,rof1,rof1);
        }
        else
            delay(null);
    }

    rgpulse(pw, v6, rof1, rof1);
    delay(tau);
    decpower(pwxlvl180);
    decshaped_pulse(pwx180ad, pwx180, zero, rof1, rof1);
    rgpulse(2.0 * pw, zero, rof1, rof1);
    delay(tau + 2 * POWER_DELAY);
    decshaped_pulse(pwx180adR, pwx180, zero, rof1, rof1);
    decpower(pwxlvl);
    rgpulse(pw, v1, rof1, rof1);
    if (getflag("PFGflg"))
    {
        zgradpulse(hsglvl, 2 * hsgt);
        delay(1e-3);
    }
    decrgpulse(pwx, v2, rof1, 2.0e-6);

    delay(d2/2);
    rgpulse(2*pw,zero,2.0e-6,2.0e-6);
    delay(d2/2);
    if (mult>0.5)
    {
        delay(taug);
        decpower(pwxlvl180r);
        decshaped_pulse(pwx180ref, pwx180r, zero, rof1, rof1);
        rgpulse(mult * pw, zero, rof1, rof1);
        delay(taug - mult*pw - 2*rof1 + 2*POWER_DELAY + evolcorr);
        decshaped_pulse(pwx180ref, pwx180r, zero, rof1, rof1);
    }
    else
    {
        decpower(pwxlvl180);
        decshaped_pulse(pwx180ad, pwx180, zero, rof1, rof1);
        delay(2*POWER_DELAY + evolcorr);
        decshaped_pulse(pwx180ad, pwx180, zero, rof1, rof1);
    }
    decpower(pwxlvl);

    decrgpulse(pwx, v4, 2.0e-6, rof1);
    if (getflag("PFGflg"))
    {
        zgradpulse(ZZgsign*0.6 * hsglvl, 1.2 * hsgt);
        delay(1e-3);
    }
    rgpulse(pw, v3, rof1, rof1);
    decpower(pwxlvl180);
    decshaped_pulse(pwx180adR, pwx180, zero, rof1, rof1);
    decpower(dpwr);
    delay(tau - 2*rof1 - (2*pw/PI));
    rgpulse(2 * pw, zero, rof1, rof2);
    decpower(pwxlvl180);
    decshaped_pulse(pwx180ad, pwx180, zero, rof1, rof1);
    decpower(dpwr);
    delay(tau);
    status(C);
}
Example #20
0
void pulsesequence()
{
  double j1min,
  	 j1max,
         pwxlvl,
         pwx,
         gzlvl0,
         gt0,
	 gzlvl1,
	 gt1,
         gzlvl3,
         gt3,
	 bird,
         gstab,
         hsglvl,
         hsgt,
         satdly,
         tauX,
         tau,
         tautau,
         t1max,
	 tauA,
	 tauB,
         tau1,
         tau2,
         taumb;
  char   sspul[MAXSTR],
  	 accord[MAXSTR],
  	 satmode[MAXSTR];
  int    ijscaleU,
  	 ijscaleD,
  	 t1_counter;

  j1min = getval("j1min");
  j1max = getval("j1max");
  pwxlvl = getval("pwxlvl");
  pwx = getval("pwx");
  getstr("sspul",sspul);
  getstr("accord",accord);
  gzlvl0 = getval("gzlvl0");
  gt0 = getval("gt0");
  gzlvl1 = getval("gzlvl1");
  gt1 = getval("gt1");
  gzlvl3 = getval("gzlvl3");
  gt3 = getval("gt3");
  gstab = getval("gstab");
  hsglvl = getval("hsglvl");
  hsgt = getval("hsgt");
  satdly = getval("satdly");
  getstr("satmode",satmode);
  tauX = 1/(2*(getval("jnmax")));
  tauA = 1/(2*(j1min + 0.146*(j1max - j1min)));
  tauB = 1/(2*(j1max - 0.146*(j1max - j1min)));
  bird = (tauA+tauB)/2;
  ijscaleD = (int)(getval("jscaleD") + 0.5);
  ijscaleU = (int)(getval("jscaleU") + 0.5);
  t1max = ((getval("ni")-1)/getval("sw1")) + 0.0005;
  tautau = ((ijscaleU - 1)*d2);
  taumb = 1/(2*(getval("jnmin")));
   if(ix == 1)
     d2_init = d2;
   t1_counter = (int) ( (d2-d2_init)*(getval("sw1")) + 0.5);

  if (accord[0] == 'y')
  {
  if ((taumb - tauX) < t1max/2)
    taumb = tauX + t1max/2;  
  tau = ((taumb - tauX)*t1_counter/ni);
  }
  else
  {
    taumb = 1/(2*(getval("jnxh")));
    if (ijscaleU > 0) 
      tau = 0.0;
    else
      tau = t1max/2;
  }

  tau1 = ijscaleD * d2;
  tau2 = (ijscaleD*t1max) - tau1;
  
  if ((ijscaleD > 0) && (ijscaleU > 0))
  {
    printf("Either jscaleD or jscaleU must be set to zero.\n");
    psg_abort(1);
  }

  settable(t1,1,ph1);
  settable(t3,2,ph3);
  settable(t4,1,ph4);
  settable(t5,4,ph5);
  settable(t6,4,ph6);

  getelem(t3,ct,v3);
  getelem(t6,ct,oph);

  initval(2.0*(double)((int)(d2*getval("sw1")+0.5)%2),v10);
  add(v3,v10,v3);
  add(oph,v10,oph);

  status(A);
     decpower(pwxlvl);
     if (sspul[0] == 'y')
     {
        zgradpulse(hsglvl*1.3,hsgt);
        rgpulse(pw,zero,rof1,rof1);
        zgradpulse(hsglvl*1.3,hsgt);
     }

     if (satmode[0] == 'y')
      {
       if (d1 - satdly > 0)
         delay(d1 - satdly);
       else
       delay(0.02);
       obspower(satpwr);
        if (satfrq != tof)
         obsoffset(satfrq);
        rgpulse(satdly,zero,rof1,rof1);
        if (satfrq != tof)
         obsoffset(tof);
       obspower(tpwr);
       delay(1.0e-5);
      }
     else
     {  delay(d1); }

   if (getflag("wet")) 
     wet4(zero,one);

  status(B);
     rgpulse(pw,t1,rof1,rof2);

/* Start of J filter  */
     zgradpulse(gzlvl0/2,gt0);
     delay(tauA - gt0);
     decrgpulse(pwx, zero, rof1, rof1);
     zgradpulse(-gzlvl0/3,gt0);
     delay(tauB - gt0);
     decrgpulse(pwx, zero, rof1, rof1);
     zgradpulse(-gzlvl0/6,gt0);
     delay(gstab);
/* End of J filter */


/* Start of STARR */
/* rev-BIRD in the middle of tau2 - 180 for C13-H and 360 for C12-H  */
/*      -   decouple long-range CH                                   */
/* 	    evolution and let HH evolution continue except for       */
/* 	         2-bond correlations				     */

       delay(tau2/2);
        zgradpulse(gzlvl0*1.5,gt0);
        delay(gstab);
        rgpulse(pw,zero,rof1,rof1);
        delay(bird);
        simpulse(2*pw,2*pwx,zero,zero,rof1,rof1);
        delay(bird);
        rgpulse(pw,zero,rof1,rof2);
        zgradpulse(-gzlvl0*1.5,gt0);
        delay(gstab);
       delay(tau2/2);
       
/* Simple C 180 in the middle of tau1 - decouple */
/*	CH evolution and let HH evolution continue  */
/* AND   Start of CT-VD */
    
    if (!((accord[0] == 'n') && (ijscaleU == 1)))
      {
       delay(tau1/2 + tau/2 + tautau/4);
        zgradpulse(gzlvl0,gt0);
        delay(gstab);
        decrgpulse(2*pwx,two,rof1,rof1);
        zgradpulse(-gzlvl0,gt0);
        delay(gstab);
       delay(tau1/2 + tau/2 + tautau/4);
      }
       
/* End of STARR  */

    if (accord[0] == 'y')
     delay(taumb - tau);
    else
     delay(taumb);
     
/* End of CT-VD */

     decrgpulse(pwx,v3,rof1,rof1);
     zgradpulse(gzlvl1,gt1);
     delay(gstab);
     delay(d2/2);
     rgpulse(pw*2.0,t4,rof1,rof1);
     delay(d2/2);
     zgradpulse(gzlvl1,gt1);
     delay(gstab);
     decrgpulse(pwx,t5,rof1,rof1);

     zgradpulse(gzlvl3,gt3);
     decpower(dpwr);
     delay(t1max/2 + tautau/2);
  status(C);
}
Example #21
0
pulsesequence() {

// =========================================================
// Define Variables and Objects and Get Parameter Values
// =========================================================
   
// --------------------------------
// Acquisition Decoupling
// -------------------------------

   char Hseq[MAXSTR];
   getstr("Hseq",Hseq);
   DSEQ dec = getdseq("H");
   strncpy(dec.t.ch,"dec",3);
   putCmd("chHtppm='dec'\n"); 
   strncpy(dec.s.ch,"dec",3);
   putCmd("chHspinal='dec'\n"); 

// ---------------------------------------------
// Determine taur, One Rotor Cycle and Set tHrr.
// ---------------------------------------------

   double srate = getval("srate");
   double taur = 0.0;
   if (srate >= 500.0)
      taur = roundoff((1.0/srate), 0.125e-6);
   else {
      abort_message("ABORT: Spin Rate (srate) must be greater than 500\n");
   }
   double tHrr = getval("nHrr")*taur;
   double tHrrret= 2.0*tHrr;
   putCmd("tHrrret = %f\n",tHrrret*1.0e6);

//--------------------------------------
// Copy Current Parameters to Processed
//-------------------------------------

   putCmd("groupcopy('current','processed','acquisition')");

//------------------------------
// Dutycycle Protection
//------------------------------
   
   DUTY d = init_dutycycle();
   d.dutyon = getval("pwX90");
   d.dutyoff = d1 + 4.0e-6;
   if (getval("aHrr") > 0.0)
     d.dutyon += 2.0*tHrr;
   d.c1 = d.c1 + (!strcmp(Hseq,"tppm"));
   d.c1 = d.c1 + ((!strcmp(Hseq,"tppm")) && (dec.t.a > 0.0));
   d.t1 = getval("rd") + getval("ad") + at;
   d.c2 = d.c2 + (!strcmp(Hseq,"spinal"));
   d.c2 = d.c2 + ((!strcmp(Hseq,"spinal")) && (dec.s.a > 0.0));
   d.t2 = getval("rd") + getval("ad") + at;
   d = update_dutycycle(d);
   abort_dutycycle(d,10.0);
   
//---------------------------
// Set Phase Tables
//---------------------------
 
   settable(phX90,4,tblX90);
   settable(phHrr,4,tblHrr);
   settable(ph1Hrr,4,tblHrr2);
   settable(phRec,4,tblRec);
   setreceiver(phRec);

//===========================    
// Begin Sequence
//===========================

   txphase(phX90); decphase(zero);
   obspwrf(getval("aX90"));   
   obsunblank(); decunblank(); _unblank34();
   delay(d1);  
   sp1on(); delay(2.0e-6); sp1off(); delay(2.0e-6);

//----------------------------   
// X Direct Polarization 
//----------------------------
   
   rgpulse(getval("pwX90"),phX90,0.0,0.0);
   obsunblank();

// -----------------------------
// Begin Rotary Resonance
// -----------------------------

   if(getval("aHrr") > 0.0) {
      obspwrf(getval("aHrr"));
      txphase(phHrr);
      xmtron();
      delay(tHrr);
      txphase(ph1Hrr);
      delay(tHrr);
      xmtroff();
   }

//===========================
// Begin Acquisition 
//===========================
   
   _dseqon(dec);
   obsblank(); _blank34();
   delay(getval("rd"));
   startacq(getval("ad"));
   acquire(np, 1/sw);
   endacq();
   _dseqoff(dec);
   obsunblank(); decunblank(); _unblank34();
}
Example #22
0
pulsesequence()
{
   double	   mixN = getval("mixN"),
		   gzlvlC = getval("gzlvlC"),
		   gtC = getval("gtC"),
		   gstab = getval("gstab"),
                   selpwrA = getval("selpwrA"),
                   selpwA = getval("selpwA"),
                   gzlvlA = getval("gzlvlA"),
                   gtA = getval("gtA"),
                   selpwrB = getval("selpwrB"),
                   selpwB = getval("selpwB"),
                   gzlvlB = getval("gzlvlB"),
                   gtB = getval("gtB"),
		   selfrq = getval("selfrq"),
		   zqfpw3 = getval("zqfpw3"),
		   zqfpwr3 = getval("zqfpwr3"),
		   gzlvlzq3 = getval("gzlvlzq3"),
		   mixNcorr,
		   sweeppw = getval("sweeppw"),
		   sweeppwr = getval("sweeppwr");
   char		   sweepshp[MAXSTR],
                   selshapeA[MAXSTR],
                   selshapeB[MAXSTR],
		   zqfpat3[MAXSTR];
//synchronize gradients to srate for probetype='nano'
//   Preserve gradient "area"
        gtC = syncGradTime("gtC","gzlvlC",1.0);
        gzlvlC = syncGradLvl("gtC","gzlvlC",1.0);
        gtA = syncGradTime("gtA","gzlvlA",1.0);
        gzlvlA = syncGradLvl("gtA","gzlvlA",1.0);
        gtB = syncGradTime("gtB","gzlvlB",1.0);
        gzlvlB = syncGradLvl("gtB","gzlvlB",1.0);

   getstr("sweepshp",sweepshp);
   getstr("selshapeA",selshapeA);
   getstr("selshapeB",selshapeB);
   getstr("zqfpat3",zqfpat3);

   mixNcorr=0.0;
   if (getflag("Gzqfilt"))
	mixNcorr=getval("zqfpw3");

   hlv(ct,v1); hlv(v1,v1); hlv(v1,v1); hlv(v1,v1); mod4(v1,v1);
   mod4(ct,v2); add(v1,v2,v2);
   hlv(ct,v3); hlv(v3,v3); mod4(v3,v3); add(v1,v3,v3); dbl(v3,v4);
   dbl(v2,oph); add(oph,v4,oph); add(oph,v1,oph);


/* BEGIN THE ACTUAL PULSE SEQUENCE */
   status(A);
   obspower(tpwr);
   delay(5.0e-5);

   delay(5.0e-5);
   if (getflag("sspul"))
        steadystate();

   if (satmode[0] == 'y')
     {
        if ((d1-satdly) > 0.02)
                delay(d1-satdly);
        else
                delay(0.02);
        satpulse(satdly,zero,rof1,rof1);
     }
   else
        delay(d1);

   if (getflag("wet"))
     wet4(zero,one);

   status(B);
      if (selfrq != tof)
       obsoffset(selfrq);
      rgpulse(pw, v1, rof1, rof1);

      if (selfrq != tof)
        obsoffset(selfrq);

        zgradpulse(gzlvlA,gtA);
        delay(gstab);
        obspower(selpwrA);
        shaped_pulse(selshapeA,selpwA,v2,rof1,rof1);
        obspower(tpwr);
        zgradpulse(gzlvlA,gtA);
        delay(gstab);

      if (selfrq != tof)
        delay(2*OFFSET_DELAY);

        zgradpulse(gzlvlB,gtB);
        delay(gstab);
        obspower(selpwrB);
        shaped_pulse(selshapeB,selpwB,v3,rof1,rof1);
        obspower(tpwr);
        zgradpulse(gzlvlB,gtB);
        delay(gstab);

      if (selfrq != tof)
        obsoffset(tof);

      rgpulse(pw,v1,rof1,rof1);

        obspower(sweeppwr);
	delay(0.31*mixN);
	zgradpulse(gzlvlC,gtC);
	delay(gstab);
	shaped_pulse(sweepshp,sweeppw,zero,rof1,rof1);
	delay(gstab);
	zgradpulse(-gzlvlC,gtC);
	delay(0.49*mixN);
	zgradpulse(-gzlvlC,2*gtC);
	delay(gstab);
        if (getflag("Gzqfilt"))
           {
                obspower(zqfpwr3);
                rgradient('z',gzlvlzq3);
                delay(100.0e-6);
                shaped_pulse(zqfpat3,zqfpw3,zero,rof1,rof1);
                delay(100.0e-6);
                rgradient('z',0.0);
           }
        else
                shaped_pulse(sweepshp,sweeppw,zero,rof1,rof1);
        delay(gstab);
        zgradpulse(gzlvlC,2*gtC);
        delay(0.2*mixN);
        obspower(tpwr);

      rgpulse(pw,v1,rof1,rof2);

   status(C);
}
Example #23
0
pulsesequence()
{
        double gzlvl1,qlvl,grise,gstab,gt1,taud2,tau1;
	int icosel;

        grise=getval("grise");
        gstab=getval("gstab");
        gt1=getval("gt1");
        gzlvl1=getval("gzlvl1");
        qlvl=getval("qlvl");
	tau1 = getval("tau1");
	taud2 = getval("taud2");

  if (phase1 == 2) 
    { 
     icosel=-1;          
     if (ix==1) 
     fprintf(stdout,"P-type MQCOSY\n");
    }
  else
    { 
     icosel=1;         /* Default to N-type experiment */ 
     if (ix==1) 
     fprintf(stdout,"N-type MQCOSY\n");
    }

  qlvl++ ; 

     status(A);
	obspower(satpwr);
	delay(d1);
	rgpulse(satdly,zero,rof1,rof2);
	obspower(tpwr);
      	delay(1.0e-6);

	rgpulse(pw,oph,rof1,rof2);
        delay(d2);

        rgradient('z',gzlvl1);
	delay(gt1+grise);
	rgradient('z',0.0);
        txphase(oph);
	delay(grise);

	rgpulse(pw,oph,0.0,rof2);
	delay(taud2);

        rgradient('z',gzlvl1);
	delay(gt1+grise);
	rgradient('z',0.0);
        txphase(oph);
	delay(grise);
	delay(taud2);

     status(B);
	 rgpulse(pw,oph,rof1,rof2);
	delay(tau1);

        rgradient('z',gzlvl1*qlvl*(double)icosel);
	delay(gt1+grise);
	rgradient('z',0.0);
	delay(grise);
	delay(gstab);
     status(C);
}
Example #24
0
pulsesequence()
{
  char    pshape[MAXSTR], httype[MAXSTR];
  int     Hdim    = (int) (0.5 + getval("Hdim")); /* dimension for testing */
  double  rg1	  = 2.0e-6,
          compH   = getval("compH"),	/* compression factor for H-1 channel */
	  gt0     = getval("gt0"),	/* gradient pulse preceding d1 */
	  gt1     = getval("gt1"),	/* gradient pulse preceding mixing */
	  gt2     = getval("gt2"),	/* gradient pulse following mixing */
	  gzlvl0  = getval("gzlvl0"),	/* gradient level for gt1 */
	  gzlvl1  = getval("gzlvl1"),	/* gradient level for gt2 */
	  gzlvl2  = getval("gzlvl2"),	/* gradient level for gt3 */
	  gstab   = getval("gstab");	/* delay for gradient recovery */

  shape   hdx;

  getstr("pshape", pshape);
  getstr("httype", httype);
  add(one,oph,v1);
  
  /* MAKE PBOX SHAPES */

  if(Hdim == 0)
    hdx = pboxHT(pshape, pw*compH, tpwr, httype[0]); /* HADAMARD stuff */
  else /* if(Hdim == 1) */
    hdx = pboxHT_F1(pshape, pw*compH, tpwr, httype[0]);

/* Optional stuff to enable manual power calibration */

  if ((Hdim == 0) && (getval("htcal") > 0.5)) hdx.pwr = getval("htpwr");
  if ((Hdim == 1) && (getval("htcal1") > 0.5)) hdx.pwr = getval("htpwr1");

/* THE PULSE PROGRAMM STARTS HERE */

  status(A);
    delay(1.0e-4);
    zgradpulse(gzlvl0,gt0);

    pre_sat();
    if (getflag("wet"))
      wet4(zero,one);

    obspower(tpwr);
    delay(1.0e-5);

  status(B);

    if ((httype[0] == 'i') || (httype[0] == 's'))  /* inversion and sequential inversion */
    {
      pbox_pulse(&hdx, zero, rof1, rof1);
      zgradpulse(gzlvl2,gt2);
      obspower(tpwr);
      delay(gstab);
      rgpulse(pw,oph,rg1,rof2);
    }
    else if (httype[0] == 'r')              /* gradient echo */
    {
      obspower(tpwr);
      rgpulse(pw,oph,rg1,rg1);
      zgradpulse(gzlvl1,gt1);
      delay(gstab);
      pbox_pulse(&hdx, oph, rg1, rof2);
      zgradpulse(gzlvl1,gt1);
      delay(gstab);
    }
    else /* if (httype[0] == 'e') */        /* selective excitation */
      pbox_pulse(&hdx, oph, rof1, rof1);

  status(C);
}
pulsesequence()
{
 char   codec[MAXSTR], codecseq[MAXSTR];

 int	icosel,  t1_counter;

 double	d2_init = 0.0, 
        rf0 = 4095, rf200, pw200,
        copwr, codmf, cores, copwrf,

        tpwrs,   
        pwHs = getval("pwHs"), 
        compH = getval("compH"),
	pwClvl = getval("pwClvl"), 
        pwC = getval("pwC"), 
        compC = getval("compC"), 
        pwNlvl = getval("pwNlvl"), 
        pwN = getval("pwN"),

        sw1 = getval("sw1"), 
        swH = getval("swH"),
        swC = getval("swC"), 
        swN = getval("swN"), 
        swTilt,
        angle_H = getval("angle_H"), 
        angle_C = getval("angle_C"),
        angle_N, 
        cos_H, 
        cos_C,
        cos_N,

        mix = getval("mix"),
        tauCH = getval("tauCH"),                                                /* 1/4JCH  */
        tauNH = getval("tauNH"),                                                /* 1/4JNH  */
	tau1, tau2, tau3,
        tofali =getval("tofali"),                             /* aliphatic protons offset  */
        dofcaco =getval("dofcaco"),               /* offset for caco decoupling, ~120 ppm  */
        dof = getval("dof"),

        gstab = getval("gstab"),

        gt0 = getval("gt0"),  gzlvl0 = getval("gzlvl0"),
        gt1 = getval("gt1"),  gzlvl1 = getval("gzlvl1"),
                              gzlvl2 = getval("gzlvl2"),
        gt3 = getval("gt3"),  gzlvl3 = getval("gzlvl3"),
        gt4 = getval("gt4"),  gzlvl4 = getval("gzlvl4"),
        gt5 = getval("gt5"),  gzlvl5 = getval("gzlvl5"),
        gt6 = getval("gt6"),  gzlvl6 = getval("gzlvl6"),
        gt7 = getval("gt7"),  gzlvl7 = getval("gzlvl7"),
        gt8 = getval("gt8"),  gzlvl8 = getval("gzlvl8"),
        gt9 = getval("gt9"),  gzlvl9 = getval("gzlvl9");

/* LOAD VARIABLES */
   copwr = getval("copwr");        copwrf = getval("copwrf");
   codmf = getval("codmf");        cores = getval("cores");
   getstr("codecseq", codecseq);   getstr("codec", codec);

/* Load phase cycling variables */

   settable(t1, 4, phi1);   settable(t2, 2, phi2);   settable(t3, 1, phi3);
   settable(t4, 8, phi4);   settable(t5, 1, phi5);   settable(t14, 2, phi14);
   settable(t11, 8, rec);

   angle_N=0.0; cos_N=0.0;

/* activate auto-calibration flags */
setautocal();
  if (autocal[0] == 'n')
  {
    /* 180 degree adiabatic C13 pulse from 0 to 200 ppm */
    pw200 = getval("pw200");
    rf200 = (compC*4095.0*pwC*4000.0*sqrt((30.0*sfrq/600.0+7.0)/0.35));
    rf200 = (int) (rf200 + 0.5);
                             
    if (1.0/(4000.0*sqrt((30.0*sfrq/600.0+7.0)/0.35)) < pwC )
    { text_error( " Not enough C13 RF. pwC must be %f usec or less.\n",
                    (1.0e6/(4000.0*sqrt((30.0*sfrq/600.0+7.0)/0.35))) );
      psg_abort(1); }
  }
  else        /* if autocal = 'y'(yes), 'q'(quiet), r(read), or 's'(semi) */
  {
    strcpy(codecseq,"Pdec_154p");
    if(FIRST_FID)                                            /* call Pbox */
    {
      ppm = getval("dfrq");
      bw = 200.0*ppm; pws = 0.001; ofs = 0.0; nst = 1000; 
                                 /* 1 ms long pulse, nst: number of steps */
      stC200 = pbox_makeA("stC200", "sech", bw, pws, ofs, compC*pwC, pwClvl, nst);

      bw=20.0*ppm; ofs=154*ppm;
      Pdec_154p = pbox_Dsh("Pdec_154p", "WURST2", bw, ofs, compC*pwC, pwClvl);
    }
    rf200 = stC200.pwrf;  pw200 = stC200.pw;
  }
/* selective H20 one-lobe sinc pulse */
   tpwrs = tpwr - 20.0*log10(pwHs/(compH*pw*1.69));
   tpwrs = (int)(tpwrs+0.5);

/* check validity of parameter range */

   if((dm[A] == 'y'  || dm[B] == 'y' || dm[C] == 'y'))
   { printf("incorrect Dec1 decoupler flags!  ");      psg_abort(1);   }

   if((dm2[A] == 'y' || dm2[B] == 'y'))
   { printf("incorrect Dec2 decoupler flags!  ");      psg_abort(1);   }
  
   if ((dpwr > 48) || (dpwr2 > 48))
   { printf("don't fry the probe, dpwr too high!  ");  psg_abort(1);   }

/* set up angles for PR42 experiments */

   /* sw1 is used as symbolic index */
   if ( sw1 < 1000 ) { printf ("Please set sw1 to some value larger than 1000.\n"); psg_abort(1); }

   if (angle_H < 0 || angle_C < 0 || angle_H > 90 || angle_C > 90 )
   { printf("angles must be set between 0 and 90 degree.\n"); psg_abort(1); }

   cos_H = cos (PI*angle_H/180);  cos_C = cos (PI*angle_C/180);
   if ( (cos_H*cos_H + cos_C*cos_C) > 1.0) { printf ("Impossible angle combinations.\n"); psg_abort(1); }
   else { cos_N = sqrt(1 - (cos_H*cos_H + cos_C*cos_C) );  angle_N = acos(cos_N)*180/PI;  }

   if (ix == 1) d2_init = d2;
   t1_counter = (int)((d2-d2_init)*sw1 + 0.5);

   if(t1_counter % 2)   { tsadd(t3,2,4);  tsadd(t11,2,4);  }

   swTilt = swH*cos_H + swC*cos_C + swN*cos_N;


   if (phase1 == 1)  {;}                                                              /* CC */
   else if (phase1 == 2)  { tsadd(t1, 1, 4); }                                        /* SC */
   else if (phase1 == 3)  { tsadd(t2, 1, 4); tsadd(t14,1,4); }                        /* CS */
   else if (phase1 == 4)  { tsadd(t1, 1, 4); tsadd(t2,1,4); tsadd(t14,1,4); }         /* SS */

   if ( phase2 == 1 )    { tsadd(t5,2,4);   icosel = 1; }
   else                    icosel = -1; 

   tau1 = 1.0 * t1_counter * cos_H / swTilt;
   tau2 = 1.0 * t1_counter * cos_C / swTilt;
   tau3 = 1.0 * t1_counter * cos_N / swTilt;

   tau1 = tau1/2.0;  tau2 = tau2/2.0;  tau3 =tau3/2.0;


   if (ix ==1 )
   {
      printf ("Current Spectral Width:\t\t%5.2f\n", swTilt);
      printf ("Angle_H: %5.2f \n", angle_H);
      printf ("Angle_C: %5.2f \n", angle_C);
      printf ("Angle_N: %5.2f \n", angle_N);
      printf ("\n\n\n\n\n");
   }


/* BEGIN ACTUAL PULSE SEQUENCE */

status(A);

      delay(d1);

      rcvroff();
      obsoffset(tofali);  obspower(tpwr);     obspwrf(4095.0);
      decoffset(dof);     decpower(pwClvl);   decpwrf(rf0);
      dec2offset(dof2);   dec2power(pwNlvl);  dec2pwrf(4095.0);

      if (gt0 > 0.2e-6)
      {
         decrgpulse(pwC,zero,10.0e-6,0.0);
         dec2rgpulse(pwN,zero,2.0e-6,2.0e-6);
         zgradpulse(gzlvl0,gt0); 
         delay(gstab);
      }

      txphase(t1);   decphase(t2);   dec2phase(zero);

status(B);

   rgpulse(pw,t1,4.0e-6,2.0e-6);                     

      zgradpulse(gzlvl3,gt3);
      delay(2.0*tauCH - gt3 - 2.0*GRADIENT_DELAY -4.0e-6);

   decrgpulse(pwC,t2,2.0e-6,2.0e-6);	                        
      decphase(zero);   

   /*=======  Start of c13 evolution ==========*/

      if ( ((tau2 -PRG_START_DELAY - POWER_DELAY -pwN - 2.0*pwC/PI -2.0e-6)> 0) 
           && ((tau2 -PRG_STOP_DELAY - POWER_DELAY - pwN - 2.0*pwC/PI -2.0e-6)>0)
           && (codec[A] == 'y') )
      {
         decpower(copwr);  decpwrf(copwrf);
         decprgon(codecseq,1/codmf,cores);
         decon();

         delay(tau2 -PRG_START_DELAY - POWER_DELAY -pwN - 2.0*pwC/PI -2.0e-6);
   sim3pulse(2.0*pw, 0.0, 2.0*pwN, t1, zero, zero, 0.0, 0.0);
         delay(tau2 -PRG_STOP_DELAY - POWER_DELAY - pwN - 2.0*pwC/PI -2.0e-6);

         decoff();
         decprgoff();
      }
      else if ( (tau2 -pwN - 2.0*pwC/PI -2.0e-6) > 0)
      {
         delay(tau2 -pwN - 2.0*pwC/PI -2.0e-6);
   sim3pulse(2.0*pw, 0.0, 2.0*pwN, t1, zero, zero, 0.0, 0.0);
         delay(tau2 -pwN - 2.0*pwC/PI -2.0e-6);
      }
      else
      {
         delay(2.0*tau2);
         decphase(t14);  
         delay(4.0e-6);
   sim3pulse(2.0*pw, 2.0*pwC, 2.0*pwN, t1, t14, zero, 0.0, 0.0);
         delay(4.0e-6);
      }

      decpower(pwClvl);
      decpwrf(rf0);
      decphase(zero);
   /*======= End of  c13 evolution ==========*/
   decrgpulse(pwC,zero, 2.0e-6,2.0e-6);                       

      txphase(zero);
      delay(2.0*tauCH + tau1 - gt3 - 4.0*pwC
                    - gstab -4.0e-6 - 2.0*GRADIENT_DELAY);	
      zgradpulse(gzlvl3,gt3);
      delay(gstab);

   decrgpulse(pwC,zero,0.0, 0.0);
      decphase(one);
   decrgpulse(2.0*pwC, one, 0.2e-6, 0.0);
      decphase(zero);
   decrgpulse(pwC, zero, 0.2e-6, 0.0);

      delay(tau1);

   rgpulse(pw,zero,2.0e-6,0.0);                             

  /* ===========Beginning of NOE transfer ======= */

      delay(mix - gt4 - gt5 - pwN -pwC - 2.0*gstab);		
      obsoffset(tof);

      zgradpulse(gzlvl4,gt4);
      delay(gstab);

   decrgpulse(pwC, zero, 2.0e-6, 2.0e-6);
   dec2rgpulse(pwN, zero, 2.0e-6, 2.0e-6);

      zgradpulse(gzlvl5,gt5);
      delay(gstab);	
                                            /* H2O relaxes back to +z */

  /* ===========   End of NOE transfer ======= */

   rgpulse(pw, zero, 2.0e-6, 2.0e-6);                           

      zgradpulse(gzlvl6,gt6);
      delay(tauNH - gt6 - 4.0e-6 - 2.0*GRADIENT_DELAY);

   sim3pulse(2.0*pw, 0.0, 2*pwN, zero, zero, zero, 2.0e-6, 2.0e-6);

      delay(tauNH - gt6 - gstab -4.0e-6 - 2.0*GRADIENT_DELAY);
      zgradpulse(gzlvl6,gt6);
      txphase(one);
      delay(gstab);

   rgpulse(pw,one,2.0e-6,2.0e-6);	                    

      txphase(two);
      obspower(tpwrs);

      shaped_pulse("H2Osinc", pwHs, two, 2.0e-6, 2.0e-6);

      obspower(tpwr);
      zgradpulse(gzlvl7,gt7);
      dec2phase(t3);
      decoffset(dofcaco);          /* offset on 120ppm for CaCO decoupling */
      decpwrf(rf200);                             /* fine power for stC200 */
      delay(gstab);			

   dec2rgpulse(pwN,t3,2.0e-6,2.0e-6);

      dec2phase(t4);
      delay(tau3); 

   rgpulse(2.0*pw, zero, 2.0e-6, 2.0e-6);
   decshaped_pulse("stC200", 1.0e-3, zero, 2.0e-6, 2.0e-6);

      delay(tau3);
      delay(gt1 +gstab +8.0e-6 - 1.0e-3 - 2.0*pw);

   dec2rgpulse(2.0*pwN, t4, 2.0e-6, 2.0e-6);

      dec2phase(t5);
      zgradpulse(gzlvl1, gt1);       
      delay(gstab + WFG_START_DELAY + WFG_STOP_DELAY - 2.0*GRADIENT_DELAY);

   sim3pulse(pw, 0.0, pwN, zero, zero, t5, 2.0e-6, 2.0e-6);

      dec2phase(zero);
      zgradpulse(gzlvl8, gt8);
      delay(tauNH - gt8 - 2.0*GRADIENT_DELAY -4.0e-6);

   sim3pulse(2.0*pw, 0.0, 2.0*pwN, zero, zero, zero, 2.0e-6, 2.0e-6);

      delay(tauNH  - gt8 - gstab -4.0e-6 - 2.0*GRADIENT_DELAY);
      zgradpulse(gzlvl8, gt8);
      txphase(one);    dec2phase(one);
      delay(gstab);

   sim3pulse(pw, 0.0, pwN, one, zero, one, 2.0e-6, 2.0e-6);

      txphase(zero);   dec2phase(zero);
      zgradpulse(gzlvl9, gt9);
      delay(tauNH - gt9 - 2.0*GRADIENT_DELAY -4.0e-6);

   sim3pulse(2.0*pw, 0.0, 2.0*pwN, zero, zero, zero, 2.0e-6, 2.0e-6);

      delay(tauNH - gt9 - 2.0*GRADIENT_DELAY -gstab -4.0e-6);
      zgradpulse(gzlvl9, gt9);
      delay(gstab);

   rgpulse(pw, zero, 2.0e-6, 2.0e-6);

      delay((gt1/10.0) +gstab -2.0e-6 - 0.5*pw + 2.0*GRADIENT_DELAY + POWER_DELAY);

   rgpulse(2.0*pw, zero, 2.0e-6, 2.0e-6);

      zgradpulse(icosel*gzlvl2, gt1/10.0);    

      dec2power(dpwr2);	
      delay(gstab);

status(C);
      setreceiver(t11);
} 
Example #26
0
pulsesequence()

{

/* DECLARE VARIABLES */

 char       autocal[MAXSTR],  /* auto-calibration flag */
            fsat[MAXSTR],
	    fscuba[MAXSTR],
            f1180[MAXSTR],    /* Flag to start t1 @ halfdwell             */
            f2180[MAXSTR],    /* Flag to start t2 @ halfdwell             */
            ddseq[MAXSTR],    /* deuterium decoupling sequence */
            shp_sl[MAXSTR],

            shcreb[MAXSTR],  /* reburp shape for center of t1 period */
            shcgcob[MAXSTR], /* g3 inversion at 154 ppm (350 us) */
            shcgcoib[MAXSTR],  /* g3 time inversion at 154 ppm (350 us) */
            shca180[MAXSTR],   /* Ca 180 [D/sq(3)] during 15N CT */
            shco180[MAXSTR],   /* Co 180 [D/sq(15)] during 15N CT */
            sel_flg[MAXSTR],   /* active/passive purging of undesired 
                                  component  */ 
            fCT[MAXSTR],	       /* Flag for constant time C13 evolution */
            fc180[MAXSTR],
            cal_sphase[MAXSTR],
            shared_CT[MAXSTR],
            nietl_flg[MAXSTR];

 int         phase, phase2, ni2, icosel, 
             t1_counter,   /* used for states tppi in t1           */ 
             t2_counter;   /* used for states tppi in t2           */ 

 double      tau1,         /*  t1 delay */
             tau2,         /*  t2 delay */
             taua,         /*  ~ 1/4JNH =  2.25 ms */
             del1,       /* time for C'-N to refocus set to 0.5*24.0 ms */
             bigTN,        /* nitrogen T period */
             bigTC,        /* carbon T period */
             zeta,         /* delay for transfer from ca to cb = 3.5 ms */
             tsatpwr,      /* low level 1H trans.power for presat  */
             sw1,          /* sweep width in f1                    */             
             sw2,          /* sweep width in f2                    */             
             tauf,         /* 1/2J NH value                     */
             pw_sl,        /* selective pulse on water      */
             phase_sl,     /* phase on water      */
             tpwrsl,       /* power for pw_sl               */
             at,

             d_cgcob,     /* power level for g3 pulses at 154 ppm */
             d_creb,      /* power level for reburp 180 at center of t1 */
             pwcgcob,     /* g3 ~ 35o us 180 pulse */
             pwcreb,      /* reburp ~ 400us 180 pulse */ 
 
             pwD,        /* 2H 90 pulse, about 125 us */
             pwDlvl,        /* 2H 90 pulse, about 125 us */

             pwca180,     /* Ca 180 during N CT at d_ca180 */
             pwco180,     /* Co 180 during N CT at d_co180 */

             d_ca180,
             d_co180,

             compC = getval("compC"),	/* C-13 RF calibration parameters */
             pwC = getval("pwC"),
             pwClvl = getval("pwClvl"),

             pwN,
             pwNlvl,

             sphase,

             pw_sl1,
             tpwrsl1,

             gstab,

             gt1,
             gt2,
             gt3,
             gt4,
             gt5,
             gt6,
             gt7,
             gt8,
             gt9,
             gt11,
             gt13,
             gt14,

             gzlvl1,
             gzlvl2,
             gzlvl3,
             gzlvl4,
             gzlvl5,
             gzlvl6,
             gzlvl7,
             gzlvl8,
             gzlvl9,
             gzlvl11,
             gzlvl13,
             gzlvl14;
            
/*  variables commented out are already defined by the system      */


/* LOAD VARIABLES */


  getstr("autocal",autocal);
  getstr("fsat",fsat);
  getstr("f1180",f1180);
  getstr("f2180",f2180);
  getstr("fscuba",fscuba);
  getstr("ddseq",ddseq);
  getstr("shp_sl",shp_sl);

  getstr("sel_flg",sel_flg);
  
  getstr("fCT",fCT);
  getstr("fc180",fc180);
  getstr("cal_sphase",cal_sphase);

  getstr("shared_CT",shared_CT);

  getstr("nietl_flg",nietl_flg);

  taua   = getval("taua"); 
  del1  = getval("del1");
  bigTN = getval("bigTN");
  bigTC = getval("bigTC");
  zeta = getval("zeta");
  pwN = getval("pwN");
  tpwr = getval("tpwr");
  tsatpwr = getval("tsatpwr");
  dpwr = getval("dpwr");
  pwNlvl = getval("pwNlvl");
  pwD = getval("pwD");
  pwDlvl = getval("pwDlvl");
  phase = (int) ( getval("phase") + 0.5);
  phase2 = (int) ( getval("phase2") + 0.5);
  sw1 = getval("sw1");
  sw2 = getval("sw2");
  ni2 = getval("ni2");
  tauf = getval("tauf");
  pw_sl = getval("pw_sl");
  phase_sl = getval("phase_sl");
  tpwrsl = getval("tpwrsl");
  at = getval("at");

  sphase = getval("sphase");

  pw_sl1 = getval("pw_sl1");
  tpwrsl1 = getval("tpwrsl1");

  gstab = getval("gstab");

  gt1 = getval("gt1");
  if (getval("gt2") > 0) gt2=getval("gt2");
    else gt2=gt1*0.1;
  gt3 = getval("gt3");
  gt4 = getval("gt4");
  gt5 = getval("gt5");
  gt6 = getval("gt6");
  gt7 = getval("gt7");
  gt8 = getval("gt8");
  gt9 = getval("gt9");
  gt11 = getval("gt11");
  gt13 = getval("gt13");
  gt14 = getval("gt14");

  gzlvl1 = getval("gzlvl1");
  gzlvl2 = getval("gzlvl2");
  gzlvl3 = getval("gzlvl3");
  gzlvl4 = getval("gzlvl4");
  gzlvl5 = getval("gzlvl5");
  gzlvl6 = getval("gzlvl6");
  gzlvl7 = getval("gzlvl7");
  gzlvl8 = getval("gzlvl8");
  gzlvl9 = getval("gzlvl9");
  gzlvl11 = getval("gzlvl11");
  gzlvl13 = getval("gzlvl13");
  gzlvl14 = getval("gzlvl14");

  if(autocal[0]=='n')
  {     
    getstr("shcgcob",shcgcob);
    getstr("shcgcoib",shcgcoib);
    getstr("shcreb",shcreb);
    getstr("shca180",shca180);
    getstr("shco180",shco180);
    
    d_ca180 = getval("d_ca180");
    d_co180 = getval("d_co180");
    d_cgcob = getval("d_cgcob");
    d_creb = getval("d_creb");
    pwca180 = getval("pwca180");
    pwco180 = getval("pwco180");
    pwcgcob = getval("pwcgcob");
    pwcreb = getval("pwcreb");
  }
  else
  {        
    strcpy(shcgcob,"Pg3_107p");    
    strcpy(shcgcoib,"Pg3i_107p");    
    strcpy(shcreb,"Preb_on");    
    strcpy(shca180,"Phard_15p");    
    strcpy(shco180,"Phard_133p");    
    if (FIRST_FID)  
    {
      cgcob = pbox(shcgcob, G3CGCOB, CAB180ps, dfrq, compC*pwC, pwClvl);
      cgcoib = pbox(shcgcoib, G3CGCOBi, CAB180ps, dfrq, compC*pwC, pwClvl);  
      creb = pbox(shcreb, CREB180, CAB180ps, dfrq, compC*pwC, pwClvl);      
      ca180 = pbox(shca180, CA180, CA180ps, dfrq, compC*pwC, pwClvl);        
      co180 = pbox(shco180, CO180, CA180ps, dfrq, compC*pwC, pwClvl);  
    }   
    d_ca180 = ca180.pwr;
    d_co180 = co180.pwr;
    d_cgcob = cgcob.pwr;
    d_creb = creb.pwr;
    pwca180 = ca180.pw;
    pwco180 = co180.pw;
    pwcgcob = cgcob.pw;
    pwcreb = creb.pw;
  }   

/* LOAD PHASE TABLE */

  settable(t1,2,phi1);
  settable(t2,4,phi2);
  settable(t3,8,phi3);
  settable(t4,1,phi4);
  settable(t5,16,phi5);
  settable(t6,8,phi6);
  settable(t7,1,phi7);
  settable(t8,16,rec); 

/* CHECK VALIDITY OF PARAMETER RANGES */

   if(shared_CT[A] == 'n')
    if(bigTN - 0.5*(ni2 -1)/sw2 - POWER_DELAY < 0.2e-6)
    {
        text_error(" ni2 is too big\n");
        text_error(" please set ni2 smaller or equal to %d\n",
    			(int) ((bigTN -POWER_DELAY)*sw2*2.0) +1 );
        psg_abort(1);
    }

   if(fCT[A] == 'y')
    if(bigTC - 0.5*(ni-1)/sw1 - WFG_STOP_DELAY - gt14 - 102.0e-6
        - POWER_DELAY - 4.0e-6 - pwD - POWER_DELAY - PRG_START_DELAY
        - POWER_DELAY - WFG_START_DELAY - 4.0e-6 - pwcgcob - WFG_STOP_DELAY
        - POWER_DELAY - 4.0e-6 < 0.2e-6) {

          text_error("ni is too big\n");
          text_error(" please set ni smaller or equal to %d\n",
    			(int) ((bigTC - WFG_STOP_DELAY - gt14 - 102.0e-6
        			- POWER_DELAY - 4.0e-6 - pwD - POWER_DELAY - PRG_START_DELAY
        			- POWER_DELAY - WFG_START_DELAY - 4.0e-6 - pwcgcob - WFG_STOP_DELAY
        			- POWER_DELAY - 4.0e-6)*sw1*2.0) +1 );
          psg_abort(1);
    }

    if((dm[A] == 'y' || dm[B] == 'y' || dm[C] == 'y'))
    {
        text_error("incorrect dec1 decoupler flags!  ");
        psg_abort(1);
    }

    if((dm2[A] == 'y' || dm2[B] == 'y' || dm2[C] == 'y'))
    {
        text_error("incorrect dec2 decoupler flags! Should be 'nnn' ");
        psg_abort(1);
    }

    if( tsatpwr > 6 )
    {
        text_error("TSATPWR too large !!!  ");
        psg_abort(1);
    }

    if( dpwr > 46 )
    {
        text_error("don't fry the probe, DPWR too large!  ");
        psg_abort(1);
    }

    if( dpwr2 > 47 )
    {
        text_error("don't fry the probe, DPWR2 too large!  ");
        psg_abort(1);
    }

    if( pwClvl > 63 )
    {
        text_error("don't fry the probe, pwClvl too large!  ");
        psg_abort(1);
    }

    if( pwNlvl > 63 )
    {
        text_error("don't fry the probe, pwNlvl too large!  ");
        psg_abort(1);
    }

    if( pw > 200.0e-6 )
    {
        text_error("dont fry the probe, pw too high ! ");
        psg_abort(1);
    } 
    if( pwN > 200.0e-6 )
    {
        text_error("dont fry the probe, pwN too high ! ");
        psg_abort(1);
    } 
    if( pwC > 200.0e-6 )
    {
        text_error("dont fry the probe, pwC too high ! ");
        psg_abort(1);
    } 

    if( f1180[A] != 'n' && f2180[A] != 'n' ) {
        text_error("flags may be set wrong: set f1180=n and f2180=n for 3d\n");
        psg_abort(1);
    }

    if(d_ca180 > 58) 
    {
        text_error("dont fry the probe, d_ca180 too high ! ");
        psg_abort(1);
    }

    if(d_co180 > 58) 
    {
        text_error("dont fry the probe, d_ca180 too high ! ");
        psg_abort(1);
    }

    if( gt1 > 15e-3 || gt2 > 15e-3 || gt3 > 15e-3 
        || gt4 > 15e-3 || gt5 > 15e-3 || gt6 > 15e-3 
        || gt7 > 15e-3 || gt8 > 15e-3 || gt9 > 15e-3 
        || gt11 > 15e-3 || gt13 > 15e-3  
        || gt14 > 15e-3)
    {
       text_error("gti values must be < 15e-3\n");
       psg_abort(1);
    } 

    if(tpwrsl > 25) {
       text_error("tpwrsl must be less than 25\n");
       psg_abort(1);
    }

    if(tpwrsl1 > 25) {
       text_error("tpwrsl1 must be less than 25\n");
       psg_abort(1);
    }

    if( dpwr3 > 50) {
       text_error("dpwr3 too high\n");
       psg_abort(1);
    }
    if( del1 > 0.1 ) {
       text_error("too long del1\n");
       psg_abort(1);
    }
    if( zeta > 0.1 ) {
       text_error("too long zeta\n");
       psg_abort(1);
    }
    if( bigTN > 0.1) {
       text_error("too long bigTN\n");
       psg_abort(1);
    }
    if( bigTC > 0.1) {
       text_error("too long bigTC\n");
       psg_abort(1);
    }
    if( pw_sl > 10e-3) {
       text_error("too long pw_sl\n");
       psg_abort(1);
    }
    if( pw_sl1 > 10e-3) {
       text_error("too long pw_sl1\n");
       psg_abort(1);
    }
    if( at > 0.1 && dm2[D] == 'y') {
       text_error("too long at with dec2\n");
       psg_abort(1);
    }

    if(pwDlvl > 59) {
        text_error("pwDlvl is too high; <= 59\n");
        psg_abort(1);
    }

    if(d_creb > 62) {
        text_error("d_creb is too high; <= 62\n");
        psg_abort(1);
    }

    if(d_cgcob > 60) {
        text_error("d_cgcob is too high; <=60\n");
        psg_abort(1);
    }

    if(cal_sphase[A] == 'y') {
      text_error("Use only to calibrate sphase\n");
      text_error("Set zeta to 600 us, gt11=gt13=0, fCT=y, fc180=n\n");
    }

    if(nietl_flg[A] == 'y' && sel_flg[A] == 'y') {
       text_error("Both nietl_flg and sel_flg cannot by y\n");
       psg_abort(1);
    }

    if (fCT[A] == 'n' && fc180[A] =='y' && ni > 1.0) {
       text_error("must set fc180='n' to allow Calfa/Cbeta evolution (ni>1)\n");
       psg_abort(1);
   }


/*  Phase incrementation for hypercomplex 2D data */

    /* changed from 1 to 3; spect. rev. not needed */
    if (phase == 2) { tsadd(t2,3,4); tsadd(t3,3,4); }

    if (shared_CT[A] == 'n') 
      {
       if (phase2 == 2) { tsadd(t7,2,4); icosel = 1; }
         else icosel = -1;
      }
     else 
      {
       if (phase2 == 2) { tsadd(t7,2,4); icosel = -1; }
         else icosel = 1;
      }

    if (nietl_flg[A] == 'y') icosel = -1*icosel;

/* Calculate modifications to phases for States-TPPI acquisition          */

   if( ix == 1) d2_init = d2 ;
   t1_counter = (int) ( (d2-d2_init)*sw1 + 0.5 );
   if(t1_counter % 2) {
      tsadd(t2,2,4);     
      tsadd(t8,2,4);    
    }

   if( ix == 1) d3_init = d3 ;
   t2_counter = (int) ( (d3-d3_init)*sw2 + 0.5 );
   if(t2_counter % 2) {
      tsadd(t5,2,4);  
      tsadd(t8,2,4);    
    }

/*  Set up f1180  tau1 = t1         */

      tau1 = d2;
      if(f1180[A] == 'y' && fCT[A] == 'y') 
          tau1 += ( 1.0 / (2.0*sw1) );

      if(f1180[A] == 'y' && fCT[A] == 'n') 
          tau1 += (1.0 / (2.0*sw1) - 4.0/PI*pwC - POWER_DELAY
                    - 4.0e-6);

      if(f1180[A] == 'n' && fCT[A] == 'n') 
          tau1 = (tau1 - 4.0/PI*pwC - POWER_DELAY
                    - 4.0e-6);

      if(tau1 < 0.2e-6) tau1 = 4.0e-7; 
      tau1 = tau1/2.0;

/*  Set up f2180  tau2 = t2         */

    tau2 = d3;
    if(f2180[A] == 'y') {
        tau2 += ( 1.0 / (2.0*sw2) ); 
        if(tau2 < 0.2e-6) tau2 = 0.2e-6;
    }
        tau2 = tau2/2.0;

/* BEGIN ACTUAL PULSE SEQUENCE */

status(A);
   obspower(tsatpwr);     /* Set transmitter power for 1H presaturation */
   decpower(pwClvl);      /* Set Dec1 power to high power          */
   dec2power(pwNlvl);     /* Set Dec2 power for 15N hard pulses         */
   dec3power(pwDlvl);     /* Set Dec3 for 2H hard pulses */

/* Presaturation Period */

   if (fsat[0] == 'y')
     {
      delay(2.0e-5);
      rgpulse(d1,zero,0.0,2.0e-6);
      obspower(tpwr);      /* Set transmitter power for hard 1H pulses */
      delay(2.0e-5);
      if (fscuba[0] == 'y')
	{
	 delay(2.2e-2);
	 rgpulse(pw,zero,2.0e-6,0.0);
	 rgpulse(2*pw,one,2.0e-6,0.0);
	 rgpulse(pw,zero,2.0e-6,0.0);
	 delay(2.2e-2);
        }
     }
    else
     {
      delay(d1);
     }
   obspower(tpwr);           /* Set transmitter power for hard 1H pulses */
   txphase(zero);
   dec2phase(zero);
   delay(1.0e-5);

/* Begin Pulses */

status(B);

   rcvroff();
   lk_hold();
   delay(20.0e-6);

   rgpulse(pw,zero,0.0,0.0);                    /* 90 deg 1H pulse */

   delay(0.2e-6);
   zgradpulse(gzlvl5,gt5);
   delay(2.0e-6);

   delay(taua - gt5 - 2.2e-6);   /* taua <= 1/4JNH */ 

   sim3pulse(2*pw,0.0,2*pwN,zero,zero,zero,0.0,0.0);

   dec2phase(t1); decphase(zero); 

   delay(taua - gt5 - 200.2e-6); 

   delay(0.2e-6);
   zgradpulse(gzlvl5,gt5);
   delay(200.0e-6);

   if (sel_flg[A] == 'y') 
     {
      rgpulse(pw,one,4.0e-6,0.0);

      initval(1.0,v2);
      obsstepsize(phase_sl);
      xmtrphase(v2);

      /* shaped pulse */
      obspower(tpwrsl);
      shaped_pulse(shp_sl,pw_sl,two,2.0e-6,0.0);
      xmtrphase(zero);
      delay(2.0e-6);
      obspower(tpwr);
      /* shaped pulse */

      initval(1.0,v6);
      dec2stepsize(45.0);
      dcplr2phase(v6);

      delay(0.2e-6);
      zgradpulse(gzlvl3,gt3);
      delay(200.0e-6);

      dec2rgpulse(pwN,t1,0.0,0.0);
      dcplr2phase(zero);

      delay(1.34e-3 - SAPS_DELAY);
   
      rgpulse(pw,zero,0.0,0.0);
      rgpulse(2.0*pw,one,2.0e-6,0.0);
      rgpulse(pw,zero,2.0e-6,0.0);

      decpower(d_ca180);

        dec2phase(zero);
   
        delay(del1 - 1.34e-3 - 4.0*pw - 4.0e-6 
              - POWER_DELAY + WFG_START_DELAY + pwca180 + WFG_STOP_DELAY);
     }
    else  
     {
      rgpulse(pw,three,4.0e-6,0.0);

      initval(1.0,v2);
      obsstepsize(phase_sl);
      xmtrphase(v2);
   
      /* shaped pulse */
      obspower(tpwrsl);
      shaped_pulse(shp_sl,pw_sl,zero,2.0e-6,0.0);
      xmtrphase(zero);
      delay(2.0e-6);
      obspower(tpwr);
      /* shaped pulse */
   
      delay(0.2e-6);
      zgradpulse(gzlvl3,gt3);
      delay(200.0e-6);

      dec2rgpulse(pwN,t1,0.0,0.0);
      dec2phase(zero);

      decpower(d_ca180);

      delay(del1 - POWER_DELAY + WFG_START_DELAY
      		+ pwca180 + WFG_STOP_DELAY);
     }

   decphase(zero);
   dec2rgpulse(2*pwN,zero,0.0,0.0);
   decshaped_pulse(shca180,pwca180,zero,0.0,0.0);

   dec2phase(one);

   delay(del1);

   dec2rgpulse(pwN,one,0.0,0.0);

   decpower(pwClvl);

   decphase(t2); 

   delay(0.2e-6);
   zgradpulse(gzlvl4,gt4);
   delay(200.0e-6);

   dec2phase(t5); 

   /* Turn on D decoupling using the third decoupler */
   dec3phase(one);
   dec3power(pwDlvl);
   dec3rgpulse(pwD,one,4.0e-6,0.0);
   dec3phase(zero);
   dec3power(dpwr3);
   dec3unblank();
   setstatus(DEC3ch, TRUE, 'w', FALSE, dmf3);
   /* Turn on D decoupling */

   decrgpulse(pwC,t2,0.0,0.0);

   delay(zeta
	- PRG_STOP_DELAY - DELAY_BLANK - POWER_DELAY - 4.0e-6
        - pwD
        - gt11 - 102.0e-6 - POWER_DELAY - WFG_START_DELAY); 
      
   /* Turn off D decoupling */
   setstatus(DEC3ch, FALSE, 'c', FALSE, dmf3);
   dec3blank(); 
   dec3phase(three);
   dec3power(pwDlvl);
   dec3rgpulse(pwD,three,4.0e-6,0.0);
   /* Turn off D decoupling */

    decphase(zero);

   delay(2.0e-6);
   zgradpulse(gzlvl11,gt11);
   delay(100.0e-6);

   if (cal_sphase[A] == 'y') 
     {
      decpower(pwClvl);
      decshaped_pulse("hard",2.0*pwC,zero,4.0e-6,4.0e-6);
     }
    else 
     {
      initval(1.0,v3);
      decstepsize(sphase);
      dcplrphase(v3);
      decpower(d_creb);
      decshaped_pulse(shcreb,pwcreb,zero,4.0e-6,4.0e-6);
      dcplrphase(zero);
     }

   delay(2.0e-6);
   zgradpulse(gzlvl11,gt11);
   delay(100.0e-6);

   /* Turn on D decoupling using the third decoupler */
   dec3phase(one);
   dec3power(pwDlvl);
   dec3rgpulse(pwD,one,4.0e-6,0.0);
   dec3phase(zero);
   dec3power(dpwr3);
   dec3unblank();
   setstatus(DEC3ch, TRUE, 'w', FALSE, dmf3);
   /* Turn on D decoupling */

   delay(zeta - WFG_STOP_DELAY - gt11 - 102.0e-6 
	- POWER_DELAY - 4.0e-6 - pwD - POWER_DELAY - PRG_START_DELAY
        - DELAY_BLANK - POWER_DELAY - 4.0e-6);

   decpower(pwClvl);
   decrgpulse(pwC,t3,4.0e-6,0.0);

   if (fCT[A] == 'y') 
     {
      delay(tau1);

      decpower(d_cgcob);
      decshaped_pulse(shcgcob,pwcgcob,zero,4.0e-6,0.0);

      delay(bigTC - POWER_DELAY - WFG_START_DELAY - 4.0e-6
            - pwcgcob - WFG_STOP_DELAY 
            - 102.0e-6 - gt14 
            - PRG_STOP_DELAY - DELAY_BLANK
            - POWER_DELAY - 4.0e-6 - pwD - POWER_DELAY - WFG_START_DELAY);
 
      /* Turn off D decoupling */
      setstatus(DEC3ch, FALSE, 'c', FALSE, dmf3);
      dec3blank();
      dec3phase(three);
      dec3power(pwDlvl);
      dec3rgpulse(pwD,three,4.0e-6,0.0);
      /* Turn off D decoupling */

      delay(2.0e-6);
      zgradpulse(gzlvl14,gt14);
      delay(100.0e-6);

      initval(1.0,v4);
      decstepsize(sphase);
      dcplrphase(v4);
      decpower(d_creb);
      decshaped_pulse(shcreb,pwcreb,zero,4.0e-6,4.0e-6);
      dcplrphase(zero);
    
      delay(2.0e-6);
      zgradpulse(gzlvl14,gt14);
      delay(100.0e-6);

      /* Turn on D decoupling using the third decoupler */
      dec3phase(one);
      dec3power(pwDlvl);
      dec3rgpulse(pwD,one,4.0e-6,0.0);
      dec3phase(zero);
      dec3power(dpwr3);
      dec3unblank(); 
      setstatus(DEC3ch, TRUE, 'w', FALSE, dmf3);
      /* Turn on D decoupling */


      delay(bigTC - tau1 - WFG_STOP_DELAY - gt14
            - 102.0e-6 - POWER_DELAY - 4.0e-6 - pwD - POWER_DELAY
            - PRG_START_DELAY - POWER_DELAY - WFG_START_DELAY
            - 4.0e-6 - pwcgcob - WFG_STOP_DELAY - POWER_DELAY 
            - 4.0e-6);

      decpower(d_cgcob);
      decshaped_pulse(shcgcoib,pwcgcob,zero,4.0e-6,0.0);
      decphase(t4);
     }
    else if(fCT[A] == 'n' && fc180[A] == 'n') 
     {
      delay(tau1);
      delay(tau1);
     }
    else if(fCT[A] == 'n' && fc180[A] == 'y') 
     {
      initval(1.0,v4);
      decstepsize(sphase);
      dcplrphase(v4);

      decpower(d_creb);
      decshaped_pulse(shcreb,pwcreb,zero,4.0e-6,0.0);

      dcplrphase(zero);
     }

   decpower(pwClvl);
   decrgpulse(pwC,t4,4.0e-6,0.0);

   delay(zeta - POWER_DELAY - 4.0e-6
          - pwD - PRG_STOP_DELAY - DELAY_BLANK
          - gt13
          - 102.0e-6 - POWER_DELAY - WFG_START_DELAY); 

   /* Turn off D decoupling */
   setstatus(DEC3ch, FALSE, 'c', FALSE, dmf3);
   dec3blank(); 
   dec3power(pwDlvl);
   dec3rgpulse(pwD,three,4.0e-6,0.0);
   /* Turn off D decoupling */

   delay(2.0e-6);
   zgradpulse(gzlvl13,gt13);
   delay(100.0e-6);

   if (cal_sphase[A] == 'y') 
     {
      decpower(pwClvl);
      decshaped_pulse("hard",2.0*pwC,zero,4.0e-6,4.0e-6);
     }
    else 
     {
      initval(1.0,v5);
      decstepsize(sphase);
      dcplrphase(v5);
      decpower(d_creb);
      decshaped_pulse(shcreb,pwcreb,zero,4.0e-6,4.0e-6);
      dcplrphase(zero);
     }

   delay(2.0e-6);
   zgradpulse(gzlvl13,gt13);
   delay(100.0e-6);

   /* Turn on D decoupling using the third decoupler */
   dec3phase(one);
   dec3power(pwDlvl);
   dec3rgpulse(pwD,one,4.0e-6,0.0);
   dec3phase(zero);
   dec3power(dpwr3);
   dec3unblank();
   setstatus(DEC3ch, TRUE, 'w', FALSE, dmf3);
   /* Turn on D decoupling */


   delay(zeta - WFG_STOP_DELAY - gt13 - 102.0e-6  
        - POWER_DELAY - 4.0e-6 - pwD - POWER_DELAY
        - PRG_START_DELAY - DELAY_BLANK
        - POWER_DELAY - 4.0e-6);

   decpower(pwClvl);
   decrgpulse(pwC,zero,4.0e-6,0.0);

   /* Turn off D decoupling */
   setstatus(DEC3ch, FALSE, 'c', FALSE, dmf3);
   dec3blank();
   dec3phase(three);
   dec3power(pwDlvl);
   dec3rgpulse(pwD,three,4.0e-6,0.0);
   /* Turn off D decoupling */

   delay(0.2e-6);
   zgradpulse(gzlvl9,gt9);
   delay(200.0e-6);

   if (shared_CT[A] == 'n') 
     {
      dec2rgpulse(pwN,t5,2.0e-6,0.0);

      decpower(d_ca180);

      dec2phase(t6); 

      delay(bigTN - tau2 - POWER_DELAY);

      dec2rgpulse(2*pwN,t6,0.0,0.0);
      decshaped_pulse(shca180,pwca180,zero,0.0,0.0);
      dec2phase(t7);

      delay(bigTN - WFG_START_DELAY - pwca180 - WFG_STOP_DELAY
            - gt1 - 2.0*GRADIENT_DELAY - 500.2e-6 
            - POWER_DELAY - 4.0e-6 - WFG_START_DELAY
            - pwco180 - WFG_STOP_DELAY);

      delay(0.2e-6);
      zgradpulse(gzlvl1,gt1);
      delay(500.0e-6);

      decpower(d_co180);
      decshaped_pulse(shco180,pwco180,zero,4.0e-6,0.0);

      delay(tau2);
   
      sim3pulse(pw,0.0,pwN,zero,zero,t7,0.0,0.0);
     }
    else if (shared_CT[A] == 'y') 
     {
      dec2rgpulse(pwN,t5,2.0e-6,0.0);

      decpower(d_co180);
      dec2phase(t6); 

      if (bigTN - tau2 >= 0.2e-6) 
        {
         delay(tau2);

         decshaped_pulse(shco180,pwco180,zero,4.0e-6,0.0);
         decpower(d_ca180);

         delay(0.2e-6);
         zgradpulse(gzlvl1,gt1);
         delay(500.0e-6);

         delay(bigTN - 4.0e-6 - WFG_START_DELAY - pwco180 - WFG_STOP_DELAY
               - POWER_DELAY - gt1 - 500.2e-6 - 2.0*GRADIENT_DELAY
               - WFG_START_DELAY - pwca180 - WFG_STOP_DELAY);

         decshaped_pulse(shca180,pwca180,zero,0.0,0.0);
         dec2rgpulse(2*pwN,t6,0.0,0.0);

         delay(bigTN - tau2);
        }
       else 
        {
         delay(tau2);
         decshaped_pulse(shco180,pwco180,zero,4.0e-6,0.0);

         delay(0.2e-6);
         zgradpulse(gzlvl1,gt1);
         delay(500.0e-6);
     
         decpower(d_ca180);
         delay(bigTN - 4.0e-6 - WFG_START_DELAY - pwco180
               - WFG_STOP_DELAY - gt1 - 500.2e-6 - 2.0*GRADIENT_DELAY
               - POWER_DELAY - WFG_START_DELAY - pwca180 - WFG_STOP_DELAY); 
   
         decshaped_pulse(shca180,pwca180,zero,0.0,0.0);
    
         delay(tau2 - bigTN);
         dec2rgpulse(2.0*pwN,t6,0.0,0.0);
        }
      sim3pulse(pw,0.0,pwN,zero,zero,t7,0.0,0.0);
     }
/* end of shared_CT */

   if (nietl_flg[A] == 'n') 
     {
      decpower(pwClvl);
      decrgpulse(pwC,zero,4.0e-6,0.0);

      delay(0.2e-6);
      zgradpulse(gzlvl6,gt6);
      delay(2.0e-6);

      dec2phase(zero);
      delay(tauf - POWER_DELAY - 4.0e-6 
                 - pwC - gt6 - 2.2e-6);

      sim3pulse(2*pw,0.0,2*pwN,zero,zero,zero,0.0,0.0);

      txphase(one);
      dec2phase(one);
   
      delay(tauf - gt6 - 200.2e-6);

      delay(0.2e-6);
      zgradpulse(gzlvl6,gt6);
      delay(200.0e-6);

      sim3pulse(pw,0.0,pwN,one,zero,one,0.0,0.0);
      
      delay(0.2e-6);
      zgradpulse(gzlvl7,gt7);
      delay(2.0e-6);
 
      txphase(zero);
      dec2phase(zero);
      delay(tauf - gt7 - 2.2e-6);

      sim3pulse(2*pw,0.0,2*pwN,zero,zero,zero,0.0,0.0);

      delay(tauf - gt7 - 200.2e-6);

      delay(0.2e-6);
      zgradpulse(gzlvl7,gt7);
      delay(200.0e-6);
   
      sim3pulse(pw,0.0e-6,pwN,zero,zero,zero,0.0,0.0);
     }
    else  
     {   /* nietl_flg == y */
      /* shaped pulse */
      obspower(tpwrsl1);
      shaped_pulse(shp_sl,pw_sl1,zero,2.0e-6,0.0);
      delay(2.0e-6);
      obspower(tpwr);
      /* shaped pulse */

      decpower(pwClvl);
      decrgpulse(pwC,zero,4.0e-6,0.0);

      delay(0.2e-6);
      zgradpulse(gzlvl6,gt6);
      delay(2.0e-6);
   
      dec2phase(zero);
      delay(tauf 
                 - POWER_DELAY - 2.0e-6 - WFG_START_DELAY
                 - pw_sl1 - WFG_STOP_DELAY - 2.0e-6 - POWER_DELAY
                 - POWER_DELAY - 4.0e-6 
                 - pwC - gt6 - 2.2e-6);

      sim3pulse(2*pw,0.0,2*pwN,zero,zero,zero,0.0,0.0);

      txphase(one);
      dec2phase(zero);

      delay(tauf - gt6 - 200.2e-6);

      delay(0.2e-6);
      zgradpulse(gzlvl6,gt6);
      delay(200.0e-6);

      sim3pulse(pw,0.0,pwN,one,zero,zero,0.0,0.0);
   
      delay(0.2e-6);
      zgradpulse(gzlvl7,gt7);
      delay(2.0e-6);
 
      txphase(zero);
      dec2phase(zero);
      delay(tauf - gt7 - 2.2e-6);

      sim3pulse(2*pw,0.0,2*pwN,zero,zero,zero,0.0,0.0);
      txphase(one);
      dec2phase(one);
   
      delay(tauf - gt7 - 200.2e-6);

      delay(0.2e-6);
      zgradpulse(gzlvl7,gt7);
      delay(200.0e-6);
   
      sim3pulse(pw,0.0e-6,pwN,one,zero,one,0.0,0.0);
      txphase(zero);
     }  /* end of nietl_flg == y  */

   delay(gt2 +gstab -0.5*(pwN-pw) -2.0*pw/PI);

   rgpulse(2*pw,zero,0.0,0.0);

   delay(2.0e-6);
   zgradpulse(icosel*gzlvl2,gt2);
   decpower(dpwr);    /* NO  13C decoupling */
   dec2power(dpwr2);  /* NO  15N decoupling */
   delay(gstab -2.0e-6 -2.0*GRADIENT_DELAY -2.0*POWER_DELAY);

   lk_sample();
/* BEGIN ACQUISITION */
status(C);
   setreceiver(t8);

}
Example #27
0
void pulsesequence()
{
double  gzlvlE = getval("gzlvlE"),
        gtE = getval("gtE"),
        EDratio = getval("EDratio"),
        gstab = getval("gstab"),
        mult = getval("mult"),
	pwx180 = getval("pwx180"),
	pwxlvl180 = getval("pwxlvl180"),
	pwx180r = getval("pwx180r"),
	pwxlvl180r = getval("pwxlvl180r"),
        hsglvl = getval("hsglvl"),
        hsgt = getval("hsgt"),
        tauA=getval("tauA"),        //compensation for tauB and tauD
        tauB=getval("tauB"),        //effect of rof2
        tauD=getval("tauD"),        //effect of alfa
        tBal=getval("tBal"),        //supports inova console if ~1/(fb*1.3)
        pwr_XBIP = getval("pwr_XBIP"),
        pw_XBIP = getval("pw_XBIP"),
        pwr_HBIP = getval("pwr_HBIP"),
        pw_HBIP = getval("pw_HBIP"),
        gzlvlcr = getval("gzlvlcr"),
        gtcr = getval("gtcr"),        //crusher gradient in BIRD
        npoints = getval("npoints"),  // npoints should be an integer multiple of np
        tau, evolcorr, taug,cycles;
int     prgcycle = (int)(getval("prgcycle")+0.5),
	phase1 = (int)(getval("phase")+0.5),
	icosel, ZZgsign;
char	pwx180ad[MAXSTR], pwx180adR[MAXSTR], pwx180ref[MAXSTR],
        shp_XBIP[MAXSTR], shp_HBIP[MAXSTR], BIRD[MAXSTR], BIRDmode[MAXSTR];

//synchronize gradients to srate for probetype='nano'
//   Preserve gradient "area"
        gtE = syncGradTime("gtE","gzlvlE",0.5);
        gzlvlE = syncGradLvl("gtE","gzlvlE",0.5);

  getstr("pwx180ad", pwx180ad);
  getstr("pwx180adR", pwx180adR);
  getstr("pwx180ref", pwx180ref);
  getstr("shp_XBIP",shp_XBIP);
  getstr("shp_HBIP",shp_HBIP);
  getstr("BIRD",BIRD);
  getstr("BIRDmode",BIRDmode);

  tau = 1 / (4*(getval("j1xh")));
  evolcorr = (4*pwx/PI)+2*pw+8.0e-6;
  cycles=np/npoints;
  cycles = (double)((int)((cycles)));
  initval(cycles,v20);

  if (mult > 0.5)
    taug = 2*tau + getval("tauC");
  else
    taug = gtE + gstab + 2 * GRADIENT_DELAY;
  ZZgsign=-1; 
  if (mult == 2) ZZgsign=1;
  icosel = 1;
 
  assign(ct,v17);
  assign(zero,v18);
  assign(zero,v19);

  if (getflag("prgflg") && (satmode[0] == 'y') && (prgcycle > 1.5))
    {
        hlv(ct,v17);
        mod2(ct,v18); dbl(v18,v18);
        if (prgcycle > 2.5)
           {
                hlv(v17,v17);
                hlv(ct,v19); mod2(v19,v19); dbl(v19,v19);
           }
     }
 
     if (BIRD[0]=='n')          //gHSQC phases
        {
                settable(t1,4,ph1);
                settable(t2,2,ph2);
                settable(t3,8,ph3);
                settable(t4,16,ph4);
                settable(t5,16,ph5);
        }
     else                      //rtgHSQC-BIRD phases
        {
                settable(t1,8,ph11);
                settable(t2,2,ph12);
                settable(t3,16,ph13);
                settable(t4,32,ph14);
                settable(t5,32,ph15);
                settable(t7,4,ph17);
                settable(t8,4,ph18);
                settable(t9,4,ph19);
                getelem(t7, v17, v7);
                getelem(t8, v17, v8);
                getelem(t9, v17, v9);
        }

     getelem(t1, v17, v1);
     getelem(t3, v17, v3);
     getelem(t4, v17, v4);
     getelem(t2, v17, v2);
     getelem(t5, v17, oph);

  assign(zero,v6);
  add(oph,v18,oph);
  add(oph,v19,oph);

  if ((phase1 == 2) || (phase1 == 5))
    icosel = -1;

  initval(2.0*(double)(((int)(d2*getval("sw1")+0.5)%2)),v14);
  add(v2, v14, v2);
  add(oph, v14, oph);

status(A);
   obspower(tpwr); decpower(pwxlvl);
   delay(5.0e-5);
   if (getflag("sspul"))
        steadystate();

   if (satmode[0] == 'y')
     {
        if ((d1-satdly) > 0.02)
                delay(d1-satdly);
        else
                delay(0.02);
        if (getflag("slpsat"))
           {
                shaped_satpulse("relaxD",satdly,zero);
                if (getflag("prgflg"))
                   shaped_purge(v6,zero,v18,v19);
           }
        else
           {
                satpulse(satdly,zero,rof1,rof1);
                if (getflag("prgflg"))
                   purge(v6,zero,v18,v19);
           }
     }
   else
        delay(d1);

   if (getflag("wet"))
     wet4(zero,one);

  status(B);
              /****** null flag starts here *****/
    if (getflag("nullflg"))
    {
      rgpulse(0.5 * pw, zero, rof1, rof1);
      delay(2 * tau);
      decpower(pwxlvl180);
      decshaped_pulse(pwx180ad, pwx180, zero, rof1, rof1);
      rgpulse(2.0 * pw, zero, rof1, rof1);
      delay(2 * tau + 2 * POWER_DELAY);
      decshaped_pulse(pwx180adR, pwx180, zero, rof1, rof1);
      decpower(pwxlvl);
      rgpulse(1.5 * pw, two, rof1, rof1);
      zgradpulse(hsglvl, hsgt);
      delay(1e-3);
    }

/*********gHSQC or gHSQC part of pure shift starts here *****/

    if (getflag("cpmgflg"))
    {
      rgpulse(pw, v6, rof1, 0.0);
      cpmg(v6, v15);
    }
    else
      rgpulse(pw, v6, rof1, rof1);
    delay(tau);
    decpower(pwxlvl180);
    decshaped_pulse(pwx180ad, pwx180, zero, rof1, rof1);
    rgpulse(2.0 * pw, zero, rof1, rof1);
    delay(tau + 2 * POWER_DELAY);
    decshaped_pulse(pwx180adR, pwx180, zero, rof1, rof1);
    decpower(pwxlvl);
    rgpulse(pw, v1, rof1, rof1);
    zgradpulse(hsglvl, 2 * hsgt);
    delay(1e-3);
    decrgpulse(pwx, v2, rof1, 2.0e-6);

      delay(d2 / 2);
    rgpulse(2 * pw, zero, 2.0e-6, 2.0e-6);
      delay(d2 / 2);

    delay(taug - POWER_DELAY);
    if (mult > 0.5)
    {
    decpower(pwxlvl180r);
    decshaped_pulse(pwx180ref, pwx180r, zero, rof1, rof1);
    rgpulse(mult * pw, zero, rof1, rof1);
    delay(taug - mult * pw - 2 * rof1 + POWER_DELAY - gtE - gstab - 2 * GRADIENT_DELAY+evolcorr);
    zgradpulse(gzlvlE, gtE);
    delay(gstab);
    decshaped_pulse(pwx180ref, pwx180r, zero, rof1, rof1);
    }
    else
    {
    decpower(pwxlvl180);
    decshaped_pulse(pwx180ad, pwx180, zero, rof1, rof1);
    delay(taug + POWER_DELAY - gtE - gstab - 2 * GRADIENT_DELAY+evolcorr);
    zgradpulse(gzlvlE, gtE);
    delay(gstab);
    decshaped_pulse(pwx180ad, pwx180, zero, rof1, rof1);
    }

    decpower(pwxlvl);

    decrgpulse(pwx, v4, 2.0e-6, rof1);
    zgradpulse(ZZgsign*0.6 * hsglvl, 1.2 * hsgt);
    delay(1e-3);
    rgpulse(pw, v3, rof1, rof1);
    decpower(pwxlvl180);
    decshaped_pulse(pwx180adR, pwx180, zero, rof1, rof1);
    decpower(dpwr);
    delay(tau - (2 * pw / PI) - 2*rof1);
    rgpulse(2 * pw, zero, rof1, rof2);
    decpower(pwxlvl180);
    decshaped_pulse(pwx180ad, pwx180, zero, rof1, rof1);
    decpower(dpwr);
    zgradpulse(icosel * 2.0*gzlvlE/EDratio, gtE/2.0);
    delay(tau - gtE/2.0 - 2 * GRADIENT_DELAY);

/********gHSQC part stops and BIRD Acquisition starts here*************/
    // delay(tBal);
        //filter delay (Hoult) for inova; adjust tBal manually for the same effect
        //delay(1.0/(getval("fb")*1.3))

        if (BIRD[0]=='y')
        {
#ifdef NVPSG
                setacqmode(WACQ|NZ);    //use this line only for vnmrs console; comment this out in inova
#endif
                obsblank();
//                delay(rof2);
                startacq(alfa);
        }

/*----------------------------------------------------------------------------
         Observe the 1st half chunk
-----------------------------------------------------------------------------*/

        if (BIRD[0]=='y')
        {
                status(C);
                acquire(npoints/2.0,1.0/sw);
                rcvroff();                                            
                status(B);
                obspower(tpwr);

/*------------------------------------------------------------------------
         Using hard 13C inversion pulse in BIRD
--------------------------------------------------------------------------*/

                if (BIRDmode[0]== 'h')
                {
                        rgpulse(pw,v7,rof1,rof1);
                        decpower(pwxlvl);
                        delay(tau);        
                        zgradpulse(gzlvlcr,gtcr);
                        delay(tau-gtcr);
                        simpulse(2.0*pw,2.0*pwx,v8,v8,rof1,rof1);
                        decpower(dpwr);
                        delay(tau);
                        zgradpulse(gzlvlcr,gtcr);
                        delay(tau-gtcr);
                        rgpulse(pw,v9,rof1,rof1);
                }

/*---------------------------------------------------------------------------
        Using BIP 13C inversion pulse in BIRD
----------------------------------------------------------------------------*/

                if (BIRDmode[0]== 'b')
                {
                  rgpulse(pw,v7,rof1,rof1);                     
                  if (pwr_XBIP!=pwxlvl) decpower(pwr_XBIP); else decpower(pwxlvl);
                  if (pwr_HBIP!=tpwr)  obspower(pwr_HBIP);
                  delay(tau); 
                  zgradpulse(gzlvlcr,gtcr);
                  delay(tau-gtcr);                              
                  simshaped_pulse(shp_HBIP,shp_XBIP,2.0*pw,pw_XBIP,v8,v8,rof1,rof1);
                  if (pwr_HBIP!=tpwr) obspower(tpwr);
                  decpower(dpwr);
                  delay(tau);
                  zgradpulse(gzlvlcr,gtcr);
                  delay(tau-gtcr);
                  rgpulse(pw,v9,rof1,rof1);
                }
                
                delay(tauA);
                rgpulse(pw*2.0,v7,rof1,rof1);  // hard 180 degree refocusing pulse
                obsblank();
                delay(tauB);
                rcvron();       //this includes rof3
                delay(tauD);
                decr(v20);

/*------------------------------------------------------------------------------
                Loops for more chunks
------------------------------------------------------------------------------*/

                starthardloop(v20);
                status(C);
                        acquire(npoints,1.0/sw);
                        rcvroff();                                    
                status(B);
                        obspower(tpwr);                               

/*------------------------------------------------------------------------                                              
Using hard 13C inversion pulse in BIRD
--------------------------------------------------------------------------*/
                if (BIRDmode[0]== 'h')
                {
                        rgpulse(pw,v7,rof1,rof1);
                        decpower(pwxlvl);                             
                        delay(tau);         
                        zgradpulse(gzlvlcr,gtcr);
                        delay(tau-gtcr);                      
                        simpulse(2.0*pw,2.0*pwx,v8,v8,rof1,rof1);
                        decpower(dpwr);
                        delay(tau);
                        zgradpulse(gzlvlcr,gtcr);
                        delay(tau-gtcr);
                        rgpulse(pw,v9,rof1,rof1);
                }
/*---------------------------------------------------------------------------
Using BIP 13C inversion pulse in BIRD
----------------------------------------------------------------------------*/
//                if (BIRDmode[0]== 'b')
                if (BIRDmode[0]== 'b')
                {
                        rgpulse(pw,v7,rof1,rof1);                     
                        if (pwr_XBIP!=pwxlvl) decpower(pwr_XBIP); else decpower(pwxlvl);
                        delay(tau);      
                        zgradpulse(gzlvlcr,gtcr);
                        delay(tau-gtcr);                         
                        simshaped_pulse(shp_HBIP,shp_XBIP,2*pw,pw_XBIP,v8,v8,rof1,rof1);
                        decpower(dpwr);
                        delay(tau);
                        zgradpulse(gzlvlcr,gtcr);
                        delay(tau-gtcr);
                rgpulse(pw,v9,rof1,rof1);
                }

                delay(tauA);
                rgpulse(pw*2.0,v7,rof1,rof1);            // hard 180 degree refocusing pulse
                obsblank();
                delay(tauB);
                rcvron();       //this includes rof3
                delay(tauD);

                endhardloop();

/*----------------------------------------------------------------
                Acquisition of last half chunk
----------------------------------------------------------------*/
                status(C);
                        acquire(npoints/2.0,1.0/sw);
                        rcvroff();                                    
                        endacq();
                        incr(v20);
        }
                 /****** BIRD ends here for all *****/
/***************** ACQ for conventional gHSQC ******************************/
        else
        status(C);
}
Example #28
0
pulsesequence()
{
/* DECLARE VARIABLES */

 char        fscuba[MAXSTR],f1180[MAXSTR],f2180[MAXSTR],fsat[MAXSTR],
             shape[MAXSTR],sh_ad[MAXSTR],f3180[MAXSTR],
             N_flg[MAXSTR],diag_supp[MAXSTR];

 int	     phase,
             phase2,
             phase3,
             t1_counter,
             t2_counter,
             t3_counter, icosel;

 double      hscuba,                /* length of 1/2 scuba delay */
             pwx2,                  /* PW90 for X-nuc            */
             tsatpwr,               /* low power level for presat*/
             dhpwr2,                /* power level for X hard pulses */
             jxh,                   /* coupling for XH           */
             tauxh,                 /* delay = 1/(2jxh)          */
	     tau1,	      	    /* t1/2  H */
	     tau2,	      	    /* t2/2 N */
	     tau3,	      	    /* t3/2 N */
	     sw1,                  /* spectral width in 1H dimension */
             sw2,                  /* spectral width in 15N dimension */
             sw3,                  /* spectral width in 15N dimension */
             MIX,                  /* Total Mixing time for noesy portion */
             pw_sl,                /* selective 2ms pulse on water */
             tpwrsl,               /* power level for pw_sl   */ 
             ppm,nst,pws,bw,ofs,   /* used by Pbox */
             pwN,pwNlvl,compH,compC,pwC,pwClvl,
             d_ad,                 /* C high power for adiabatic pulses */
             pwc_ad,               /* C 90 pulse width   */

             zeta,                /* Bax-Logan trick */
             zeta1,               /* Bax-Logan trick */

             BigT,
             BigT1,

             gzlvl0,
             gzlvl1,
             gzlvl2,
             gzlvl3,
             gzlvl4,
             gzlvl5,
             gzlvl6,
             gzlvl7,
             gzlvl8,
             gzlvl9,
             gzlvl10,
             gzlvl11,
             gzlvl12,

             gstab,
             gt1,
             gt2,
             gt3,
             gt4,
             gt5,
             gt6,
             gt7,
             gt8,
             gt9,
             gt10,
             gt11,
             gt12;

/* LOAD VARIABLES */
          pwNlvl=getval("pwNlvl");
          pwN=getval("pwN");
          compC=getval("compC");
          pwC=getval("pwC");
          pwClvl=getval("pwClvl");
          compH=getval("compH");

  jxh = getval("jxh");
  dhpwr2 = getval("dhpwr2"); 
  pwx2 = getval("pwx2");
  tsatpwr = getval("tsatpwr");
  hscuba = getval("hscuba");
  phase = (int) (getval("phase") + 0.5);
  phase2 = (int) (getval("phase2") + 0.5);
  phase3 = (int) (getval("phase3") + 0.5);
  sw1 = getval("sw1");
  sw2 = getval("sw2");
  sw3 = getval("sw3");
  MIX  = getval("MIX");
  pw_sl = getval("pw_sl");
  tpwrsl = getval("tpwrsl");

  pwc_ad = getval("pwc_ad");
  d_ad = getval("d_ad");

  ni = getval("ni"); 

  BigT = getval("BigT");
  BigT1 = getval("BigT1");

  gstab  = getval("gstab");
  gzlvl0 = getval("gzlvl0");
  gzlvl1 = getval("gzlvl1");
  gzlvl2 = getval("gzlvl2");
  gzlvl3 = getval("gzlvl3");
  gzlvl4 = getval("gzlvl4");
  gzlvl5 = getval("gzlvl5");
  gzlvl6 = getval("gzlvl6");
  gzlvl7 = getval("gzlvl7");
  gzlvl8 = getval("gzlvl8");
  gzlvl9 = getval("gzlvl9");
  gzlvl10 = getval("gzlvl10");
  gzlvl11 = getval("gzlvl11");
  gzlvl12 = getval("gzlvl12");

  gt1 = getval("gt1");
  gt2 = getval("gt2");
  gt3 = getval("gt3");
  gt4 = getval("gt4");
  gt5 = getval("gt5");
  gt6 = getval("gt6");
  gt7 = getval("gt7");
  gt8 = getval("gt8");
  gt9 = getval("gt9");
  gt10 = getval("gt10");
  gt11 = getval("gt11");
  gt12 = getval("gt12");

  getstr("fscuba",fscuba); 
  getstr("fsat",fsat); 
  getstr("f1180",f1180); 
  getstr("f2180",f2180); 
  getstr("f3180",f3180); 

  getstr("N_flg",N_flg);

  getstr("diag_supp",diag_supp);
  getstr("sh_ad",sh_ad);
  getstr("shape",shape);
  if(d_ad > 62) {
   printf("chirp power is too high \n");
   psg_abort(1);
  }
  if(pwc_ad > 1.2e-3) {
    printf("adiabatic pulse is too long; set < 0.5 ms\n");
    psg_abort(1);
  } 

   setautocal();                        /* activate auto-calibration flags */ 
        
      if (autocal[0] != 'n') 
        /* if autocal = 'y'(yes), 'q'(quiet), r(read), or 's'(semi) */
      {
        strcpy(shape,"H2Osel");
        strcpy(sh_ad,"C13adiab");
        if(FIRST_FID)                                            /* call Pbox */
        {
          ppm = getval("dfrq"); ofs = 0.0;   pws = 0.0005; /*0.5 ms pulse */
          bw = 200.0*ppm;       nst = 1000;          /* nst - number of steps */
          C13adiab = pbox_makeA("C13adiab", "sech", bw, pws, ofs, compC*pwC, pwClvl, nst);
          H2Osel = pbox_Rsh("H2Osel", "sinc90", pw_sl, 0.0, compH*pw, tpwr);
          ofs_check(H1ofs, C13ofs, N15ofs, H2ofs);
        }
        pw_sl = H2Osel.pw; tpwrsl = H2Osel.pwr-1.0;  /* 1dB correction applied */
        d_ad = C13adiab.pwr; pwc_ad = C13adiab.pw;
        pwx2=pwN; dhpwr2=pwNlvl;
      }

/* check validity of parameter range */

    if((dm[A] == 'y' || dm[B] == 'y' || dm[C] == 'y'))
	{
	printf("incorrect Dec1 decoupler flags!  ");
	psg_abort(1);
    } 

    if((dm2[A] == 'y' || dm2[B] == 'y' || dm2[C] == 'y'))
	{
	printf("incorrect Dec2 decoupler flags!  ");
	psg_abort(1);
    } 

    if( tsatpwr > 8 )
    {
	printf("tsatpwr too large !!!  ");
	psg_abort(1);
    }

    if( dpwr > -16 )
    {
	printf("No C decoupling used in this expt. ");
	psg_abort(1);
    }

    if( dpwr2 > -16 )
    {
	printf("No N decoupling used in this expt. ");
	psg_abort(1);
    }

    if(gzlvl0 > 500) {
        printf("gzlvl0_max is 500\n");
        psg_abort(1);
    } 

    if( gt1 > 3e-3 || gt2 > 3e-3 || gt3 > 3e-3 || gt4 > 3e-3 
        || gt5 > 3e-3 || gt6 > 3e-3 || gt7 > 3e-3 
        || gt8 > 3e-3 || gt9 > 3e-3 || gt10 > 3e-3 || gt11 > 3e-3  
        || gt12 > 3e-3)
    {
        printf("gradients are on for too long !!! ");
        psg_abort(1);
    } 


    if(ix==1) {
    if(f1180[A] != 'n' || f2180[A] !='y' || f3180[A] != 'y') {
        printf("f1180 should be n, f2180 y, and f3180 should be y\n");
    }
   }


/* LOAD VARIABLES */

  settable(t1, 4,  phi1);
  settable(t2, 1,  phi2);
  settable(t3, 1,  phi3);
  settable(t4, 1,  phi4);
  settable(t5, 1,  phi5);
  settable(t6, 1,  phi6);
  settable(t7, 1,  phi7);
  settable(t8, 1,  phi8);
  settable(t9, 2,  phi9);
  settable(t10, 4,  rec);

/* INITIALIZE VARIABLES */

  tauxh = 1/(4*jxh);

/* Phase incrementation for hypercomplex data */

  if( phase == 2 ) {
        tsadd(t2, 1, 4);
        tsadd(t3, 1, 4);
   }

   if ( phase2 == 2 ) {    /* Hypercomplex in t2 */
        tsadd(t1, 1, 4);
   }

   if ( phase3 == 2 )     /* Hypercomplex in t3 */
   {
        tsadd(t6, 2, 4);
        tsadd(t7, 2, 4);
        tsadd(t8, 2, 4);
        tsadd(t10, 2, 4);
        icosel = -1;
   }
   else
       icosel = 1;

/* calculate modifications to phases based on current t2/t3 values
   to achieve States-TPPI acquisition */

   if(ix==1)
     d4_init = d4;
     t3_counter = (int) ( (d4-d4_init)*sw3 + 0.5);
     if(t3_counter %2) {
       tsadd(t4,2,4);
       tsadd(t5,2,4);
       tsadd(t10,2,4);
     }

   if(ix==1)
     d3_init = d3;
     t2_counter = (int) ( (d3-d3_init)*sw2 + 0.5);
     if(t2_counter %2) {
       tsadd(t1,2,4);
       tsadd(t10,2,4); 
     }

   if(ix==1)
     d2_init = d2;
     t1_counter = (int) ( (d2-d2_init)*sw1 + 0.5);
     if(t1_counter %2) {
       tsadd(t2,2,4);
       tsadd(t3,2,4);
       tsadd(t10,2,4); 
     }

/* set up so that get (-90,180) phase corrects in F1 if f1180 flag is y */

     tau1 = d2;
     if(f1180[A] == 'y') {
            tau1 += 1/(2.0*sw1);
     }

     tau1 = tau1/2.0;
     if(tau1 < 0.2e-6) tau1 = 0.2e-6;
     

/* set up so that get (-90,180) phase corrects in F2 if f2180 flag is y */

   tau2 = d3;
   if(f2180[A] == 'y')  
      tau2 += ( 1.0/(2.0*sw2) - (4.0/PI)*pwx2
                - 2.0*(2.0*GRADIENT_DELAY + 50.0e-6 + 5.0e-6) );
   if(f2180[A] == 'n')  
      tau2 = ( tau2 - (4.0/PI)*pwx2
                - 2.0*(2.0*GRADIENT_DELAY + 50.0e-6 + 5.0e-6) );

   tau2 = tau2/2.0;

   if(ix==1)
     if((tau2 + 5.0e-6 - 0.5*(WFG_START_DELAY + 4.0*pw + WFG_STOP_DELAY)
         < 5.0e-6) && N_flg[A] == 'n')
      printf("tau2 is negative; set f1180 to y\n");

/* set up so that get (-90,180) phase corrects in F3 if f3180 flag is y */

   tau3 = d4;
   if(f3180[A] == 'y')  tau3 += ( 1.0/(2.0*sw3) );

   tau3 = tau3/2.0;
   if( tau3 < 0.2e-6) tau3 = 2.0e-7; 

/* Now include Bax/Logan trick */

   if(ni != 1) {
     if(diag_supp[A] == 'n')
        zeta = (tauxh - gt5 - 102.0e-6 + 2.0*pwx2 - 2.0e-6);
     else 
        zeta = (1.0/(8.0*93.39) - gt5 - 102.0e-6 + 2.0*pwx2 - 2.0e-6);
     zeta = zeta / ( (double) (ni-1) );

     if(zeta < 0.0) {
        printf("problem with zeta\n");
        psg_abort(1);
     }

   }

   else
      zeta = 0.0;

   if( ix == 1) d2_init = d2;
   t1_counter = (int) ( (d2 - d2_init)*sw1 + 0.5 );

   zeta1 = zeta*( (double)t1_counter );
   tau1 = tau1 - zeta1; 



/* BEGIN ACTUAL PULSE SEQUENCE */

status(A);
   obspower(tsatpwr);            /* Set power for presaturation  */
   decpower(d_ad);               /* Set decoupler1 power to d_ad */
   dec2power(dhpwr2);            /* Set decoupler2 power to dhpwr2 */

/* Presaturation Period */


 if(fsat[0] == 'y')
{
  txphase(zero);
  rgpulse(d1,zero,2.0e-6,2.0e-6);  /* presat */
  obspower(tpwr);                /* Set power for hard pulses  */

    if (fscuba[0] == 'y')            /* Scuba pulse sequence */
    {  
      hsdelay(hscuba);

      rgpulse(pw,zero,1.0e-6,0.0);	/* 90x180y90x */
      rgpulse(2*pw,one,1.0e-6,0.0);
      rgpulse(pw,zero,1.0e-6,0.0);
 
      txphase(zero);
      delay(hscuba);        
    }
}

else  {
 obspower(tpwr);                /* Set power for hard pulses  */
 delay(d1);
}

status(B);

   obsoffset(tof);

   rcvroff();
   delay(20.0e-6);

  /* eliminate all magnetization originating from 15N */

  dec2rgpulse(pwx2,zero,0.0,0.0);

  delay(2.0e-6);
  zgradpulse(gzlvl1,gt1);
  delay(gstab);

  rgpulse(pw,zero,0.0,0.0);

  delay(2.0e-6);
  zgradpulse(gzlvl2,gt2);
  delay(2.0e-6);

  delay(tauxh - gt2 - 4.0e-6);               /* delay=1/4J(XH)   */

  sim3pulse(2*pw,0.0e-6,2*pwx2,zero,zero,zero,0.0,0.0);

  delay(tauxh - gt2 - 202.0e-6);             /* delay=1/4J(XH)   */

  txphase(one); dec2phase(t1);

  delay(2.0e-6);
  zgradpulse(gzlvl2,gt2);
  delay(gstab);

  rgpulse(pw,one,0.0,0.0);       

  /* shaped pulse */
  obspower(tpwrsl);
  shaped_pulse(shape,pw_sl,two,2.0e-6,0.0);
  delay(2.0e-6);
  obspower(tpwr);
  /* shaped pulse */

  delay(2.0e-6);
  zgradpulse(gzlvl3,gt3);
  delay(gstab);

  txphase(zero);

  dec2rgpulse(pwx2,t1,0.0,0.0);
  dec2phase(zero);

  if(N_flg[A] == 'n') 
  {
    if(tau2 + 5.0e-6 - 0.5*(WFG2_START_DELAY
                 + pwc_ad + WFG2_STOP_DELAY) < 0.2e-6)
     {
      rgradient('z',gzlvl0); /* use rgradient since shaping takes more time */
      delay(tau2 + 5.0e-6 - 0.5*(WFG_START_DELAY + 4.0*pw + WFG_STOP_DELAY));
      rgradient('z',0.0);
      delay(50.0e-6);

      shaped_pulse("composite",4.0*pw,zero,0.0,0.0);  /* 90x-180y-90x  */

      rgradient('z',-1.0*gzlvl0);
      delay(tau2 + 5.0e-6 - 0.5*(WFG_START_DELAY + 4.0*pw + WFG_STOP_DELAY));
      rgradient('z',0.0);
      delay(50.0e-6);

     }

     else

     {
      rgradient('z',gzlvl0); /* use rgradient since shaping takes more time */
      delay(tau2 + 5.0e-6 - 0.5*(WFG2_START_DELAY
              + pwc_ad + WFG2_STOP_DELAY));
      rgradient('z',0.0);
      delay(50.0e-6);

      simshaped_pulse("composite",sh_ad,4.0*pw,pwc_ad,zero,zero,0.0,0.0);

      rgradient('z',-1.0*gzlvl0); /* use rgradient since shaping takes more time */
      delay(tau2 + 5.0e-6 - 0.5*(WFG2_START_DELAY
              + pwc_ad + WFG2_STOP_DELAY));
      rgradient('z',0.0);
      delay(50.0e-6);

     }
  }   /* N_flg[A] == y */

  else
    sim3pulse(2.0*pw,0.0,2.0*pwx2,zero,zero,zero,4.0e-6,4.0e-6);

  dec2rgpulse(pwx2,zero,0.0,0.0);

  delay(2.0e-6);
  zgradpulse(gzlvl4,gt4);
  delay(gstab);

  if(diag_supp[A] == 'n') {

  /* shaped pulse */
  obspower(tpwrsl);
  shaped_pulse(shape,pw_sl,t3,2.0e-6,0.0);
  delay(2.0e-6);
  obspower(tpwr);
  /* shaped pulse */

  rgpulse(pw,t2,2.0e-6,0.0);
  txphase(t9);

  delay(tau1 + tauxh + zeta1 - gt5 - 102.0e-6);

  delay(2.0e-6);
  zgradpulse(gzlvl5,gt5);
  delay(100.0e-6);

  dec2rgpulse(2.0*pwx2,zero,0.0,0.0);

  delay(tau1);

  rgpulse(2.0*pw,t9,0.0,0.0); txphase(one);

  delay(tauxh - zeta1 - gt5 - 102.0e-6 + 2.0*pwx2);

  delay(2.0e-6);
  zgradpulse(gzlvl5,gt5);
  delay(100.0e-6);

  rgpulse(pw,one,0.0,0.0);

  /* shaped pulse */
  obspower(tpwrsl);
  shaped_pulse(shape,pw_sl,one,2.0e-6,0.0);
  delay(2.0e-6);
  obspower(tpwr);
  /* shaped pulse */

  delay(MIX - gt6 - gstab -2.0e-6); 

    delay(2.0e-6);
    zgradpulse(gzlvl6,gt6);
    delay(gt6);
    delay(gstab);

  }

  else {

  initval(1.0,v4);
  obsstepsize(45.0);
  xmtrphase(v4);

  /* shaped pulse */
  obspower(tpwrsl);
  shaped_pulse(shape,pw_sl,t3,2.0e-6,0.0);
  delay(2.0e-6);
  obspower(tpwr);
  /* shaped pulse */
/*
  xmtrphase(zero);
  delay(2.0e-6);

  initval(1.0,v4);
  obsstepsize(45.0);
  xmtrphase(v4);
*/
  
  rgpulse(pw,t2,2.0e-6,0.0);

  xmtrphase(zero);
  txphase(t9);

  delay(tau1 + 1.0/(8.0*93.39) + zeta1 - gt5 - 102.0e-6 - SAPS_DELAY);

  delay(2.0e-6);
  zgradpulse(gzlvl5,gt5);
  delay(100.0e-6);

  dec2rgpulse(2.0*pwx2,zero,0.0,0.0);

  delay(tau1);

  rgpulse(2.0*pw,t9,0.0,0.0); txphase(one);

  delay(1.0/(8.0*93.39) - zeta1 - gt5 - 102.0e-6 + 2.0*pwx2);

  delay(2.0e-6);
  zgradpulse(gzlvl5,gt5);
  delay(100.0e-6);

  rgpulse(pw,one,0.0,0.0);

  /* shaped pulse */
  obspower(tpwrsl);
  shaped_pulse(shape,pw_sl,one,2.0e-6,0.0);
  delay(2.0e-6);
  obspower(tpwr);
  /* shaped pulse */

    delay(2.0e-6);
    zgradpulse(gzlvl6,gt6/2.0);
    delay(gstab);

    delay(MIX - 1.5*gt6 - 2.0*(gstab+2.0e-6) - 2.0*pwx2); 

    dec2rgpulse(2.0*pwx2,zero,0.0,0.0); 

    delay(2.0e-6);
    zgradpulse(gzlvl6,gt6);
    delay(gstab);

  }

   rgpulse(pw,two,2.0e-6,0.0);

  /* shaped pulse */
  obspower(tpwrsl);
  shaped_pulse(shape,pw_sl,zero,2.0e-6,0.0);
  delay(2.0e-6); txphase(zero);
  obspower(tpwr);
  /* shaped pulse */

  delay(2.0e-6);
  zgradpulse(gzlvl7,gt7);
  delay(2.0e-6);

  delay(tauxh  
      - POWER_DELAY - 2.0e-6 - WFG_START_DELAY
      - pw_sl - WFG_STOP_DELAY - 2.0e-6 - POWER_DELAY 
      - gt7 - 4.0e-6);               /* delay=1/4J(XH)   */

  sim3pulse(2*pw,0.0e-6,2*pwx2,zero,zero,zero,0.0,0.0);

  delay(tauxh 
      - gt7 - gstab -2.0e-6
      - POWER_DELAY - 2.0e-6 - WFG_START_DELAY
      - pw_sl - WFG_STOP_DELAY - 2.0e-6 - POWER_DELAY); 

  delay(2.0e-6);
  zgradpulse(gzlvl7,gt7);
  delay(gt7);
  delay(gstab);

  /* shaped pulse */
  obspower(tpwrsl);
  shaped_pulse(shape,pw_sl,one,2.0e-6,0.0);
  obspower(tpwr);
  delay(2.0e-6); txphase(zero);
  /* shaped pulse */

  rgpulse(pw,one,0.0,0.0);

  delay(2.0e-6);
  zgradpulse(gzlvl8,gt8);
  delay(gstab);

  txphase(t6);

  if(phase3 == 1)
    dec2rgpulse(pwx2,t4,4.0e-6,0.0);
  if(phase3 == 2)
    dec2rgpulse(pwx2,t5,4.0e-6,0.0);

  decphase(zero); 

  if(tau3 - 0.5*(WFG_START_DELAY
                 + pwc_ad + WFG_STOP_DELAY)
          < 0.2e-6) {

  delay(tau3);
  delay(tau3);

  }

  else {

  delay(tau3 - 0.5*(WFG_START_DELAY
               + pwc_ad + WFG_STOP_DELAY));

  decshaped_pulse(sh_ad,pwc_ad,zero,0.0,0.0); 

  delay(tau3 - 0.5*(WFG_START_DELAY
               + pwc_ad + WFG_STOP_DELAY));

  }

  delay(2.0e-6);
  zgradpulse(-1.0*gzlvl11,gt11);
  delay(100.0e-6);

  delay(BigT - 4.0/PI*pwx2 + pw - 2.0*GRADIENT_DELAY - gt11
        - 102.0e-6);

  dec2rgpulse(2.0*pwx2,zero,0.0,0.0);

  delay(2.0e-6);
  zgradpulse(gzlvl11,gt11);
  delay(100.0e-6);

  delay(BigT - 2.0*GRADIENT_DELAY - gt11
        - 102.0e-6);

  rgpulse(pw,t6,0.0,0.0);

  /* shaped pulse */
  obspower(tpwrsl);
  shaped_pulse(shape,pw_sl,t7,2.0e-6,0.0);
  delay(2.0e-6); txphase(zero);
  obspower(tpwr);
  /* shaped pulse */

  delay(2.0e-6);
  zgradpulse(gzlvl9,gt9);
  delay(100.0e-6);

  delay(tauxh 
      - POWER_DELAY - 2.0e-6 - WFG_START_DELAY
      - pw_sl - WFG_STOP_DELAY - 2.0e-6 - POWER_DELAY 
      - gt9 - 102.0e-6);

  sim3pulse(2.0*pw,0.0,2.0*pwx2,zero,zero,zero,0.0,0.0);
  dec2phase(t8);

  delay(2.0e-6);
  zgradpulse(gzlvl9,gt9);
  delay(100.0e-6);

  delay(tauxh 
      - gt9 - 102.0e-6
      - POWER_DELAY - 2.0e-6 - WFG_START_DELAY
      - pw_sl - WFG_STOP_DELAY - 2.0e-6 - POWER_DELAY); 

  /* shaped pulse */
  obspower(tpwrsl);
  shaped_pulse(shape,pw_sl,zero,2.0e-6,0.0);
  obspower(tpwr);
  delay(2.0e-6); txphase(zero);
  /* shaped pulse */

  sim3pulse(pw,0.0,pwx2,zero,zero,t8,0.0,0.0);

  dec2phase(zero);

  delay(2.0e-6);
  zgradpulse(gzlvl10,gt10);
  delay(2.0e-6);

  delay(tauxh - gt10 - 4.0e-6);

  sim3pulse(2*pw,0.0e-6,2*pwx2,zero,zero,zero,2.0e-6,2.0e-6);  

  delay(2.0e-6);
  zgradpulse(gzlvl10,gt10);
  delay(100.0e-6);

  delay(tauxh
        - gt10 - 102.0e-6
        + 2.0/PI*pw - pwx2 + 0.5*(pwx2-pw));

  dec2rgpulse(pwx2,zero,0.0,0.0);

  dec2power(dpwr2);  /* Very Important */
  decpower(dpwr);

  delay(BigT1 - 2.0*POWER_DELAY);

  rgpulse(2.0*pw,zero,0.0,0.0); 

  delay(2.0e-6);
  zgradpulse(-1.0*icosel*gzlvl12,gt12);
  delay(50.0e-6);

  delay(BigT1 - 2.0*GRADIENT_DELAY - 52.0e-6 - gt12);

/* acquire data */

status(C);
     setreceiver(t10);
}
Example #29
0
pulsesequence()
{
   double mix,SSpwr,pwSS,hsdly,pwa,pwd,gt1,gzlvl1,gzlvl2;
   char ptable[MAXSTR],SSshape[MAXSTR];
   getstr("ptable",ptable); getstr("SSshape",SSshape);
   mix=getval("mix"); hsdly=getval("hsdly"); 
   loadtable(ptable);
   pwa=getval("pwa"); pwd=getval("pwd");
   gt1=getval("gt1"); gzlvl1=getval("gzlvl1"); gzlvl2=getval("gzlvl2");
   SSpwr=getval("SSpwr"); pwSS=getval("pwSS");
     initval(7.0,v2);   /* set up 45 degree phase shift for first pulse    */
     obsstepsize(45.0);
   getelem(t1,ct,v1);     /* 1st pulse phase    */
   getelem(t3,ct,v3);     /* read pulse phase   */
   getelem(t4,ct,v4);     /* receiver phase     */
   if (phase1 > 1.5) incr(v1);     /* hypercomplex phase shift */
   assign(v4,oph);
   /*HYPERCOMPLEX MODE USES REDFIELD TRICK TO MOVE AXIAL PEAKS TO EDGE */
    initval(2.0*(double)(((int)(d2*getval("sw1")+0.5)%2)),v6);
  if ((phase1==1)||(phase1==2)) {add(v1,v6,v1); add(v4,v6,oph);}

    assign(v3,v7);       /* for steering pulses */
    add(v3,one,v8); 
    if (pwa<0.0) { pwa = -pwa; add(v7,two,v7); }
    if (pwd<0.0) { pwd = -pwd; add(v8,two,v8); }

/* CHECK VALIDITY OF PARAMETER RANGE */

  if (dm[A] == 'y' || dm[B] == 'y')
   {
        printf(" dm must be 'nny' or 'nnn' ");
        psg_abort(1);
   }

  if ((dm[C] == 'y' || dm2[C] == 'y') && at > 0.085)
   {
        printf(" check at time! Don't fry probe \n");
        psg_abort(1);
   }

  if (dm2[A] == 'y' || dm2[B] == 'y')
   {
        printf(" dm2 must be 'nny' or 'nnn' ");
        psg_abort(1);
   }

  if (dpwr > 50)
   {
        printf(" dpwr must be less than 49 \n");
        psg_abort(1);
   }

  if (dpwr2 > 50)
   {
        printf(" dpwr2 must be less than 46 \n");
        psg_abort(1);
   }

/* BEGIN PULSE SEQUENCE */

   status(A);
     xmtrphase(v2);
     txphase(v1);
     obspower(tpwr);
     hsdelay(d1);
   status(B);
      rgpulse(pw, v1, rof1, 1.0e-6);
      xmtrphase(zero);
      txphase(t2);
      if (d2 > 0.001)
       {
     zgradpulse(gzlvl2,0.4*d2-SAPS_DELAY/2.0-2.0*GRADIENT_DELAY-(2.0*pw/PI));
     delay(0.1*d2-rof1);
     zgradpulse(-gzlvl2,0.4*d2-SAPS_DELAY/2.0-2.0*GRADIENT_DELAY-(2.0*pw/PI));
     delay(0.1*d2-rof1);
       }
       else delay(d2);
      rgpulse(pw, t2, rof1, 1.0e-6);
   status(C);
      obspower(SSpwr);
      delay(hsdly);
      zgradpulse(gzlvl1,gt1);
      hsdelay(mix-hsdly-gt1);
      shaped_pulse(SSshape,pwSS,t3,rof1,0.0);
      obspower(SSpwr-12.0);
      rgpulse(pwa,v7,2.0e-6,0.0);    /* steering pulses */
      rgpulse(pwd,v8,0.0e-6,0.0);
      delay(rof2);
   status(D);
}
Example #30
0
void pulsesequence()
{
   double          ss,
                   arraydim,
                   p1lvl,
                   trim,
                   mix,
                   window,
                   cycles,
                   phase;
   int             iphase;
   char            sspul[MAXSTR];


/* LOAD AND INITIALIZE VARIABLES */
   ni = getval("ni");
   arraydim = getval("arraydim");
   mix = getval("mix");
   trim = getval("trim");
   phase = getval("phase");
   iphase = (int) (phase + 0.5);
   p1lvl = getval("p1lvl");
   ss = getval("ss");
   window=getval("window");
   getstr("sspul", sspul);

   if (iphase == 3)
   {
      initval((double)((int)((ix-1)/(arraydim/ni)+1.0e-6)), v14);
   }
   else
   {
      assign(zero, v14);
   }


/* CHECK CONDITIONS */
   if ((iphase != 3) && (arrayelements > 2))
   {
      fprintf(stdout, "PHASE=3 is required if MIX is arrayed!\n");
      psg_abort(1);
   }
   if (satdly > 9.999)
   {
      fprintf(stdout, "Presaturation period is too long.\n");
      psg_abort(1);
   }
   if (!newtransamp)
   {
      fprintf(stdout, "TOCSY requires linear amplifiers on transmitter.\n");
      fprintf(stdout, "Use DECTOCSY with the appropriate re-cabling,\n");
      psg_abort(1);
   }
   if ((p1 == 0.0) && (ix == 1))
      fprintf(stdout, "Warning:  P1 has a zero value.\n");
   if ((rof1 < 9.9e-6) && (ix == 1))
      fprintf(stdout,"Warning:  ROF1 is less than 10 us\n");

   if (satpwr > 40)
        {
         printf("satpwr too large  - acquisition aborted./n");
         psg_abort(1);
        }

/* DETERMINE STEADY-STATE MODE */
   if (ss < 0)
   {
      ss = (-1) * ss;
   }
   else
   {   
      if ((ss > 0) && (ix == 1))
      {
         ss = ss;
      }
      else
      {   
         ss = 0;
      }
   }
   initval(ss, ssctr);
   initval(ss, ssval);


/* STEADY-STATE PHASECYCLING */
/* This section determines if the phase calculations trigger off of (SS - SSCTR)
   or off of CT */

   ifzero(ssctr);
      hlv(ct, v13);
      mod2(ct, v1);
      hlv(ct, v2);
   elsenz(ssctr);
      sub(ssval, ssctr, v12);	/* v12 = 0,...,ss-1 */
      hlv(v12, v13);
      mod2(v12, v1);
      hlv(v12, v2);
   endif(ssctr);


/* CALCULATE PHASES */
/* A 2-step cycle is performed on the first pulse (90 degrees) to suppress
   axial peaks in the first instance.  Second, the 2-step F2 quadrature image
   suppression subcycle is added to all pulse phases and receiver phase.
   Finally, a 2-step cycle is performed on the spin-lock pulses. */

   mod2(v13, v13);
   dbl(v1, v1);
   incr(v1);
   hlv(v2, v2);
   mod2(v2, v2);
   dbl(v2, v2);
   incr(v2);
   add(v13, v2, v2);
   sub(v2, one, v3);
   add(two, v2, v4);
   add(two, v3, v5);
   add(v1, v13, v1);
   assign(v1, oph);
   if (iphase == 2)
      incr(v1);
   if (iphase == 3)
      add(v1, v14, v1);

 /*HYPERCOMPLEX MODE USES REDFIELD TRICK TO MOVE AXIAL PEAKS TO EDGE*/
   initval(2.0*(double)(((int)(d2*getval("sw1")+0.5)%2)),v6);
   if ((iphase==1)||(iphase==2)) {add(v1,v6,v1); add(oph,v6,oph);} 

/* CALCULATE AND INITIALIZE LOOP COUNTER */
      if (pw > 0.0)
      {
         cycles = (mix - trim) / (64.66*pw+32*window);
         cycles = 2.0*(double) (int) (cycles/2.0);
      }
      else
      {
         cycles = 0.0;
      }
      initval(cycles, v9);			/* V9 is the MIX loop count */

/* BEGIN ACTUAL PULSE SEQUENCE CODE */
   status(A);
      rlpower(p1lvl, TODEV);
      if (sspul[0] == 'y')
      {
         rgpulse(1000*1e-6, zero, rof1, 0.0e-6);
         rgpulse(1000*1e-6, one, 0.0e-6, rof1);
      }
      hsdelay(d1);
if (getflag("wet")) wet4(zero,one);
rlpower(p1lvl, TODEV);
     if (satmode[A] == 'y')
     { rlpower(satpwr,TODEV);
      rgpulse(satdly,zero,rof1,rof2);
      rlpower(p1lvl,TODEV);}
   status(B);
      rgpulse(p1, v1, rof1, 1.0e-6);
      if (satmode[B] =='y')
       {
        if (d2 > 0.0)
         {
           rlpower(satpwr,TODEV);
           rgpulse(d2 - (2*POWER_DELAY) - 1.0e-6 - (2*p1/3.1416),zero,0.0,0.0);
         }
       }
      else
       {
        if (d2 > 0.0)
          delay(d2 - POWER_DELAY - 1.0e-6  - (2*p1/3.1416));
       } 
      rcvroff();
      rlpower(tpwr,TODEV); 
      txphase(v13);
      xmtron();
      delay(trim);
      if (cycles > 1.0)
      {
         starthardloop(v9);
            mleva(window); mleva(window); mlevb(window); mlevb(window);
            mlevb(window); mleva(window); mleva(window); mlevb(window);
            mlevb(window); mlevb(window); mleva(window); mleva(window);
            mleva(window); mlevb(window); mlevb(window); mleva(window);
            rgpulse(.66*pw,v3,rof1,rof2);
         endhardloop();
      }
      txphase(v13);
      xmtroff();

/* detection */
      delay(rof2);
      rcvron();
   status(C);
}