pulsesequence() { // Define Variables and Objects and Get Parameter Values MPSEQ dec = getblew("blewH",0,0.0,0.0,0,1); strncpy(dec.ch,"dec",3); putCmd("chHblew='dec'\n"); CP hx = getcp("HX",0.0,0.0,0,1); strncpy(hx.fr,"dec",3); strncpy(hx.to,"obs",3); putCmd("frHX='dec'\n"); putCmd("toHX='obs'\n"); //-------------------------------------- // Copy Current Parameters to Processed //------------------------------------- putCmd("groupcopy('current','processed','acquisition')"); // Dutycycle Protection DUTY d = init_dutycycle(); d.dutyon = getval("pwH90") + getval("tHX") + getval("rd") + getval("ad") + at; d.dutyoff = d1 + 4.0e-6; d = update_dutycycle(d); abort_dutycycle(d,10.0); // Set Phase Tables settable(phH90,4,table1); settable(phXhx,4,table2); settable(phHhx,4,table3); settable(phRec,4,table4); setreceiver(phRec); // Begin Sequence txphase(phXhx); decphase(phH90); obspwrf(getval("aXhx")); decpwrf(getval("aH90")); obsunblank(); decunblank(); _unblank34(); delay(d1); sp1on(); delay(2.0e-6); sp1off(); delay(2.0e-6); // H to X Cross Polarization decrgpulse(getval("pwH90"),phH90,0.0,0.0); decphase(phHhx); _cp_(hx,phHhx,phXhx); // Begin Acquisition _mpseqon(dec, phHhx); obsblank(); _blank34(); delay(getval("rd")); startacq(getval("ad")); acquire(np, 1/sw); endacq(); _mpseqoff(dec); obsunblank(); decunblank(); _unblank34(); }
void pulsesequence() { // Define Variables and Objects and Get Parameter Values DSEQ dec = getdseq("H"); strncpy(dec.t.ch,"dec",3); putCmd("chHtppm='dec'\n"); strncpy(dec.s.ch,"dec",3); putCmd("chHspinal='dec'\n"); //-------------------------------------- // Copy Current Parameters to Processed //------------------------------------- putCmd("groupcopy('current','processed','acquisition')"); // Dutycycle Protection DUTY d = init_dutycycle(); d.dutyon = getval("pwX90"); d.dutyoff = d1 + 4.0e-6; d.c1 = d.c1 + (!strcmp(dec.seq,"tppm")); d.c1 = d.c1 + ((!strcmp(dec.seq,"tppm")) && (dec.t.a > 0.0)); d.t1 = getval("rd") + getval("ad") + at; d.c2 = d.c2 + (!strcmp(dec.seq,"spinal")); d.c2 = d.c2 + ((!strcmp(dec.seq,"spinal")) && (dec.s.a > 0.0)); d.t2 = getval("rd") + getval("ad") + at; d = update_dutycycle(d); abort_dutycycle(d,10.0); // Set Phase Tables settable(phX90,4,table1); settable(phRec,4,table2); setreceiver(phRec); // Begin Sequence txphase(phX90); decphase(zero); obspwrf(getval("aX90")); obsunblank(); decunblank(); _unblank34(); delay(d1); sp1on(); delay(2.0e-6); sp1off(); delay(2.0e-6); // X Direct Polarization rgpulse(getval("pwX90"),phX90,0.0,0.0); // Begin Acquisition _dseqon(dec); obsblank(); _blank34(); delay(getval("rd")); startacq(getval("ad")); acquire(np, 1/sw); endacq(); _dseqoff(dec); obsunblank(); decunblank(); _unblank34(); }
pulsesequence() { // Define Variables and Objects and Get Parameter Values initval(getval("periods"),v2); //-------------------------------------- // Copy Current Parameters to Processed //------------------------------------- putCmd("groupcopy('current','processed','acquisition')"); // Set Phase Tables settable(phX90,4,table1); settable(phRec,4,table2); setreceiver(phRec); // Begin Sequence txphase(phX90); decphase(zero); obspwrf(getval("aX90")); obsunblank(); decunblank(); _unblank34(); delay(d1); xgate(1.0); sp1on(); delay(2.0e-6); sp1off(); delay(2.0e-6); // Apply a Rotorsync Delay rgpulse(getval("pwX90"),phX90,0.0,0.0); rotorsync(v2); rgpulse(getval("pwX90"),phX90,0.0,0.0); xgate(getval("xperiods")); rgpulse(getval("pwX90"),phX90,0.0,0.0); delay(10.0e-6); // X Direct Polarization rgpulse(getval("pwX90"),phX90,0.0,0.0); // Begin Acquisition obsblank(); _blank34(); delay(getval("rd")); startacq(getval("ad")); acquire(np, 1/sw); endacq(); obsunblank(); decunblank(); _unblank34(); }
void pulsesequence(){ //Define Variables and Get Parameter Values double pwTune = getval("pwTune"); pwTune = pwTune*6.0; at = pwTune*2.0; char atval[MAXSTR]; sprintf(atval,"at = %f\n", at); putCmd(atval); int chTune = (int) getval("chTune"); if ((chTune < 1) || (chTune > 4)) { abort_message("chTune(%d) must be between 1 and 4\n", chTune); } //-------------------------------------- // Copy Current Parameters to Processed //------------------------------------- putCmd("groupcopy('current','processed','acquisition')"); // Set Phase Tables settable(phTune,4,table1); settable(phRec,4,table2); setreceiver(t2); //Begin Sequence obspwrf(getval("aTune")); obsunblank(); decunblank(); _unblank34(); delay(d1); sp1on(); delay(2e-6); sp1off(); delay(2.0e-6); //Begin Phase Detected Pulse set4Tune(chTune,getval("gain")); delay(1.0e-4); ShapedXmtNAcquire("phtran",pwTune,phTune,6.0e-6,chTune); obsunblank(); decunblank(); _unblank34(); }
pulsesequence() { // Define Variables and Objects and Get Parameter Values double aXecho = getval("aXecho"); double t1Xechoinit = getval("t1Xecho"); double pwXecho = getval("pwXecho"); double t2Xechoinit = getval("t2Xecho"); double t1Xecho = t1Xechoinit - pwXecho/2.0; if (t1Xecho < 0.0) t1Xecho = 0.0; double t2Xecho = t2Xechoinit - pwXecho/2.0 - getval("rd"); if (t2Xecho < 0.0) t2Xecho = 0.0; CP hx = getcp("HX",0.0,0.0,0,1); strncpy(hx.fr,"dec",3); strncpy(hx.to,"obs",3); putCmd("frHX='dec'\n"); putCmd("toHX='obs'\n"); DSEQ dec = getdseq("H"); strncpy(dec.t.ch,"dec",3); putCmd("chHtppm='dec'\n"); strncpy(dec.s.ch,"dec",3); putCmd("chHspinal='dec'\n"); //-------------------------------------- // Copy Current Parameters to Processed //------------------------------------- putCmd("groupcopy('current','processed','acquisition')"); // Dutycycle Protection DUTY d = init_dutycycle(); d.dutyon = getval("pwH90") + getval("tHX") + pwXecho; d.dutyoff = d1 + 4.0e-6; d.c1 = d.c1 + (!strcmp(dec.seq,"tppm")); d.c1 = d.c1 + ((!strcmp(dec.seq,"tppm")) && (dec.t.a > 0.0)); d.t1 = getval("rd") + getval("ad") + at; d.c2 = d.c2 + (!strcmp(dec.seq,"spinal")); d.c2 = d.c2 + ((!strcmp(dec.seq,"spinal")) && (dec.s.a > 0.0)); d.t2 = getval("rd") + getval("ad") + at; d = update_dutycycle(d); abort_dutycycle(d,10.0); // Set Phase Tables settable(phH90,4,table1); settable(phXhx,4,table2); settable(phHhx,4,table3); settable(phXecho,16,table4); settable(phRec,8,table5); setreceiver(phRec); // Begin Sequence txphase(phXhx); decphase(phH90); obspwrf(getval("aXhx")); decpwrf(getval("aH90")); obsunblank(); decunblank(); _unblank34(); delay(d1); // sp1on(); delay(2.0e-6); sp1off(); delay(2.0e-6); // H to X Cross Polarization decrgpulse(getval("pwH90"),phH90,0.0,0.0); decphase(phHhx); sp1on(); _cp_(hx,phHhx,phXhx); sp1off(); // Begin Decoupling _dseqon(dec); // X Hahn Echo txphase(phXecho); obspwrf(aXecho); delay(t1Xecho); rgpulse(pwXecho,phXecho,0.0,0.0); delay(t2Xecho); // Begin Acquisition obsblank(); _blank34(); delay(getval("rd")); startacq(getval("ad")); acquire(np, 1/sw); endacq(); _dseqoff(dec); obsunblank(); decunblank(); _unblank34(); }
pulsesequence() { // Define Variables and Objects and Get Parameter Values CP hx = getcp("HX",0.0,0.0,0,1); strncpy(hx.fr,"dec",3); strncpy(hx.to,"obs",3); putCmd("frHX='dec'\n"); putCmd("toHX='obs'\n"); DSEQ dec = getdseq("H"); strncpy(dec.t.ch,"dec",3); putCmd("chHtppm='dec'\n"); strncpy(dec.s.ch,"dec",3); putCmd("chHspinal='dec'\n"); DSEQ xdec = getdseq("X"); strncpy(xdec.t.ch,"obs",3); // These four statements assure strncpy(xdec.s.ch,"obs",3); // that the X decoupling will putCmd("chXtppm='obs'\n"); // be on X for either TPPM or putCmd("chXspinal='obs'\n"); // SPINAL. // Set Constant-time Period for d2. if (d2_index == 0) d2_init = getval("d2"); double d2_ = (ni - 1)/sw1 + d2_init; putCmd("d2acqret = %f\n",roundoff(d2_,12.5e-9)); putCmd("d2dwret = %f\n",roundoff(1.0/sw1,12.5e-9)); //-------------------------------------- // Copy Current Parameters to Processed //------------------------------------- putCmd("groupcopy('current','processed','acquisition')"); // Dutycycle Protection DUTY d = init_dutycycle(); d.dutyon = 3.0*getval("pwH90") + getval("pwHtilt") + getval("tHX"); d.dutyoff = d1 + 4.0e-6 + getval("tHmix"); d.c1 = d.c1 + (!strcmp(dec.seq,"tppm")); d.c1 = d.c1 + ((!strcmp(dec.seq,"tppm")) && (dec.t.a > 0.0)); d.t1 = getval("rd") + getval("ad") + at; d.c2 = d.c2 + (!strcmp(dec.seq,"spinal")); d.c2 = d.c2 + ((!strcmp(dec.seq,"spinal")) && (dec.s.a > 0.0)); d.t2 = getval("rd") + getval("ad") + at; d.c3 = d.c3 + (!strcmp(xdec.seq,"tppm")); d.c3 = d.c3 + ((!strcmp(xdec.seq,"tppm")) && (xdec.t.a > 0.0)); d.t3 = d2_; d.c4 = d.c4 + (!strcmp(xdec.seq,"spinal")); d.c4 = d.c4 + ((!strcmp(xdec.seq,"spinal")) && (xdec.s.a > 0.0)); d.t4 = d2_; d = update_dutycycle(d); abort_dutycycle(d,10.0); // Set Phase Tables settable(phH90,16,table1); settable(phHmix1,16,table2); settable(phHmix2,4,table3); settable(phHtilt,4,table4); settable(phXhx,4,table5); settable(phHhx,4,table6); settable(phRec,4,table7); if (phase1 == 2) tsadd(phH90,1,4); setreceiver(phRec); // Begin Sequence txphase(phXhx); decphase(phH90); obspwrf(getval("aXhx")); decpwrf(getval("aH90")); obsunblank(); decunblank(); _unblank34(); delay(d1); sp1on(); delay(2.0e-6); sp1off(); delay(2.0e-6); // H Preparation and tilt decrgpulse(getval("pwH90"),phH90,0.0,0.0); decunblank(); // Delay for 1H Wideline T2 _dseqon(xdec); delay(d2); _dseqoff(xdec); // Mix period for Spin Diffison decrgpulse(getval("pwH90"),phHmix1,0.0,0.0); delay(getval("tHmix")); decrgpulse(getval("pwH90"),phHmix2,0.0,0.0); // Tilt Pulse and Ramped H to X Cross Polarization with LG Offset decrgpulse(getval("pwHtilt"),phHtilt,0.0,0.0); decphase(phHhx); _cp_(hx,phHhx,phXhx); // Begin Acquisition obsblank(); _blank34(); _dseqon(dec); delay(getval("rd")); startacq(getval("ad")); acquire(np, 1/sw); endacq(); _dseqoff(dec); obsunblank(); decunblank(); _unblank34(); }
pulsesequence() { //Define Variables and Objects and Get Parameter Values double tHX3 = (getval("tHX"))/3.0; //Define MOIST CP in the Sequence MPSEQ sd = getsammyd("smydH",0,0.0,0.0,0,1); strncpy(sd.ch,"dec",3); putCmd("chHsmyd='dec'\n"); MPSEQ so = getsammyo("smyoX",0,0.0,0.0,0,1); strncpy(so.ch,"obs",3); putCmd("chXsmyo='obs'\n"); DSEQ dec = getdseq("H"); strncpy(dec.t.ch,"dec",3); putCmd("chHtppm='dec'\n"); strncpy(dec.s.ch,"dec",3); putCmd("chHspinal='dec'\n"); d2 = sd.nelem*sd.telem; // Set Constant-time Period for d2. if (d2_index == 0) d2_init = getval("d2"); double d2_ = (ni - 1)/sw1 + d2_init; putCmd("d2acqret = %f\n",roundoff(d2_,12.5e-9)); putCmd("d2dwret = %f\n",roundoff(1.0/sw1,12.5e-9)); //-------------------------------------- // Copy Current Parameters to Processed //------------------------------------- putCmd("groupcopy('current','processed','acquisition')"); // Dutycycle Protection DUTY d = init_dutycycle(); d.dutyon = getval("pwH90") + getval("pwHlock")+ getval("tHX") + d2_; d.dutyoff = d1 + 4.0e-6; d.c1 = d.c1 + (!strcmp(dec.seq,"tppm")); d.c1 = d.c1 + ((!strcmp(dec.seq,"tppm")) && (dec.t.a > 0.0)); d.t1 = getval("rd") + getval("ad") + at; d.c2 = d.c2 + (!strcmp(dec.seq,"spinal")); d.c2 = d.c2 + ((!strcmp(dec.seq,"spinal")) && (dec.s.a > 0.0)); d.t2 = getval("rd") + getval("ad") + at; d = update_dutycycle(d); abort_dutycycle(d,10.0); // Set Phase Tables settable(phH90,4,table1); settable(phHlock,4,table2); settable(phHcomp,4,table3); settable(ph1Xhx,4,table4); settable(ph2Xhx,4,table5); settable(ph1Hhx,4,table6); settable(ph2Hhx,4,table7); settable(phHsmyd,4,table8); settable(phXsmyo,4,table9); settable(phHdec,4,table10); settable(phRec,4,table11); setreceiver(phRec); // Begin Sequence txphase(ph1Xhx); decphase(phH90); obspwrf(getval("aXhx")); decpwrf(getval("aH90")); obsunblank(); decunblank(); _unblank34(); delay(d1); sp1on(); delay(2.0e-6); sp1off(); delay(2.0e-6); // H 90-degree Pulse decrgpulse(getval("pwH90"),phH90,0.0,0.0); // Prelock with Compensation Pulse decunblank(); decon(); if (getval("onHlock") > 0) { decphase(phHlock); delay(getval("pwHlock")); decphase(phHcomp); decpwrf(getval("aHcomp")); delay(getval("pwHcomp")); } // H to X MOIST Cross Polarization xmtron(); decphase(ph1Hhx); decpwrf(getval("aHhx")); delay(tHX3); txphase(ph1Xhx); decphase(ph1Hhx); delay(tHX3); txphase(ph2Xhx); decphase(ph2Hhx); delay(tHX3); xmtroff(); decoff(); // SAMMY Spinlocks on X and H _mpseqon(sd,phHsmyd); _mpseqon(so,phXsmyo); delay(d2); _mpseqoff(sd); _mpseqoff(so); decphase(phHdec); // Begin Acquisition obsblank(); _blank34(); _dseqon(dec); _decdoffset(getval("rd"),getval("ofHdec")); startacq(getval("ad")); acquire(np, 1/sw); endacq(); _dseqoff(dec); decoffset(dof); obsunblank(); decunblank(); _unblank34(); }
pulsesequence() { // Define Variables and Objects and Get Parameter Values double aXecho = getval("aXecho"); // define the echoX group in the sequence double t1Xechoinit = getval("t1Xecho"); double pwXecho = getval("pwXecho"); double t2Xechoinit = getval("t2Xecho"); double t1Xecho = t1Xechoinit - pwXecho/2.0; if (t1Xecho < 0.0) t1Xecho = 0.0; double t2Xecho = t2Xechoinit - pwXecho/2.0 - getval("rd"); if (t2Xecho < 0.0) t2Xecho = 0.0; DSEQ dec = getdseq("H"); strncpy(dec.t.ch,"dec",3); putCmd("chHtppm='dec'\n"); strncpy(dec.s.ch,"dec",3); putCmd("chHspinal='dec'\n"); //-------------------------------------- // Copy Current Parameters to Processed //------------------------------------- putCmd("groupcopy('current','processed','acquisition')"); // Dutycycle Protection DUTY d = init_dutycycle(); d.dutyon = getval("pwX90") + pwXecho; d.dutyoff = d1 + 4.0e-6; d.c1 = d.c1 + (!strcmp(dec.seq,"tppm")); d.c1 = d.c1 + ((!strcmp(dec.seq,"tppm")) && (dec.t.a > 0.0)); d.t1 = t1Xecho + t2Xecho + getval("rd") + getval("ad") + at; d.c2 = d.c2 + (!strcmp(dec.seq,"spinal")); d.c2 = d.c2 + ((!strcmp(dec.seq,"spinal")) && (dec.s.a > 0.0)); d.t2 = t1Xecho + t2Xecho + getval("rd") + getval("ad") + at; d = update_dutycycle(d); abort_dutycycle(d,10.0); // Set Phase Tables settable(phX90,4,table1); settable(phXecho,16,table2); settable(phRec,8,table3); setreceiver(phRec); // Begin Sequence txphase(phX90); decphase(zero); obspwrf(getval("aX90")); obsunblank(); decunblank(); _unblank34(); delay(d1); sp1on(); delay(2.0e-6); sp1off(); delay(2.0e-6); // H Decoupler on Before Echo _dseqon(dec); // X Direct Polarization rgpulse(getval("pwX90"),phX90,0.0,0.0); // X Solid-State Echo txphase(phXecho); obspwrf(aXecho); delay(t1Xecho); rgpulse(pwXecho,phXecho,0.0,0.0); delay(t2Xecho); // Begin Acquisition obsblank(); _blank34(); delay(getval("rd")); startacq(getval("ad")); acquire(np, 1/sw); endacq(); _dseqoff(dec); obsunblank(); decunblank(); _unblank34(); }
void pulsesequence() { //====================================================== // Define Variables and Objects and Get Parameter Values //====================================================== // -------------------------------- // Acquisition Decoupling // ------------------------------- char Xseq[MAXSTR]; getstr("Xseq",Xseq); DSEQ dec = getdseq("X"); strncpy(dec.t.ch,"dec",3); putCmd("chXtppm='dec'\n"); strncpy(dec.s.ch,"dec",3); putCmd("chXspinal='dec'\n"); //------------------------------------- // Homonuclear Decoupling During Echo //------------------------------------- MPDEC homo1 = getmpdec("hdec1H",0,0.0,0.0,0,1); strncpy(homo1.mps.ch,"obs",3); putCmd("chHhdec1='obs'\n"); // -------------------- // H echo calculation // -------------------- double t1Hecho = getval("t1Hecho") - getval("pwHecho")/2.0 - ((!strcmp(homo1.dm,"y"))?getval("pwHshort1")*2.:0.0); if (t1Hecho < 0.0) t1Hecho = 0.0; double t2Hecho = getval("t2Hecho") - getval("pwHecho")/2.0 - ((!strcmp(homo1.dm,"y"))?getval("pwHshort1")*2.:0.0) - getval("rd")- getval("ad"); if (t2Hecho < 0.0) t2Hecho = 0.0; double t1H_echo = 0.0; double t2H_echo = 0.0; double t1H_left = 0.0; double t2H_left = 0.0; if (!strcmp(homo1.dm,"y")) { t2H_echo = homo1.mps.t*((int)(t2Hecho/homo1.mps.t)); t2H_left = t2Hecho - t2H_echo; t1H_echo = t2H_echo; t1H_left = t1Hecho - t1H_echo; } //-------------------------------------- // Copy Current Parameters to Processed //------------------------------------- putCmd("groupcopy('current','processed','acquisition')"); //---------------------- // Dutycycle Protection //---------------------- DUTY d = init_dutycycle(); d.dutyon = getval("pwH90"); d.dutyoff = d1 + 4.0e-6; if (!strcmp(homo1.dm,"y")) d.dutyon += t1H_echo + t2H_echo; else d.dutyoff += t1H_echo + t2H_echo; d.c1 = d.c1 + (!strcmp(Xseq,"tppm")); d.c1 = d.c1 + ((!strcmp(Xseq,"tppm")) && (dec.t.a > 0.0)); d.t1 = getval("rd") + getval("ad") + at; d.c2 = d.c2 + (!strcmp(Xseq,"spinal")); d.c2 = d.c2 + ((!strcmp(Xseq,"spinal")) && (dec.s.a > 0.0)); d.t2 = getval("rd") + getval("ad") + at; d = update_dutycycle(d); abort_dutycycle(d,10.0); //------------------------ // Set Phase Tables //----------------------- settable(phH90,4,table1); settable(phHecho,8,table2); settable(phRec,4,table3); setreceiver(phRec); //======================= // Begin Sequence //======================= txphase(phH90); decphase(zero); obspwrf(getval("aH90")); obsunblank(); decunblank(); _unblank34(); delay(d1); sp1on(); delay(2.0e-6); sp1off(); delay(2.0e-6); //------------------------ // H Direct Polarization //------------------------ rgpulse(getval("pwH90"),phH90,0.0,0.0); obsunblank(); decunblank(); _unblank34(); // ----------------------------- // H Hahn Echo // ----------------------------- if (!strcmp(homo1.dm,"y")) { delay (t1H_left); if (getval("pwHshort1") > 0.0 ) { obspwrf(getval("aHhdec1")); rgpulse(getval("pwHshort1"),three,0.0,0.0); obsunblank(); } if (!strcmp(homo1.dm,"y")) _mpseqon(homo1.mps,zero); delay(t1H_echo); if (!strcmp(homo1.dm,"y")) _mpseqoff(homo1.mps); if (getval("pwHshort1") > 0.0 ) { obspwrf(getval("aHhdec1")); txphase(one); rgpulse(getval("pwHshort1"),one,0.0,0.0); obsunblank(); } } else delay(t1Hecho); txphase(phHecho); obspwrf(getval("aHecho")); rgpulse(getval("pwHecho"),phHecho,0.0,0.0); obsunblank(); if (!strcmp(homo1.dm,"y")) { if (getval("pwHshort1") > 0.0 ) { obspwrf(getval("aHhdec1")); rgpulse(getval("pwHshort1"),three,0.0,0.0); obsunblank(); } if (!strcmp(homo1.dm,"y")) _mpseqon(homo1.mps,zero); delay(t2H_echo); if (!strcmp(homo1.dm,"y")) _mpseqoff(homo1.mps); if(getval("pwHshort1")>0 ) { obspwrf(getval("aHhdec1")); rgpulse(getval("pwHshort1"),one,0.0,0.0); obsunblank(); } delay(t2H_left); } else delay(t2Hecho); //==================== // Begin Acquisition //==================== _dseqon(dec); obsblank(); decblank(); _blank34(); delay(getval("rd")); startacq(getval("ad")); acquire(np, 1/sw); endacq(); _dseqoff(dec); obsunblank(); decunblank(); _unblank34(); }
pulsesequence() { // Define Variables and Objects and Get Parameter Values CP hx = getcp("HX",0.0,0.0,0,1); strncpy(hx.fr,"dec",3); strncpy(hx.to,"obs",3); putCmd("frHX='dec'\n"); putCmd("toHX='obs'\n"); DSEQ dec = getdseq("H"); strncpy(dec.t.ch,"dec",3); putCmd("chHtppm='dec'\n"); strncpy(dec.s.ch,"dec",3); putCmd("chHspinal='dec'\n"); //-------------------------------------- // Copy Current Parameters to Processed //------------------------------------- putCmd("groupcopy('current','processed','acquisition')"); // Dutycycle Protection DUTY d = init_dutycycle(); d.dutyon = getval("pw1Hhytrap") + getval("pw2Hhytrap") + getval("tHX"); d.dutyoff = d1 + 4.0e-6 + getval("t1HYtrap") + getval("t2HYtrap"); d.c1 = d.c1 + (!strcmp(dec.seq,"tppm")); d.c1 = d.c1 + ((!strcmp(dec.seq,"tppm")) && (dec.t.a > 0.0)); d.t1 = getval("rd") + getval("ad") + at; d.c2 = d.c2 + (!strcmp(dec.seq,"spinal")); d.c2 = d.c2 + ((!strcmp(dec.seq,"spinal")) && (dec.s.a > 0.0)); d.t2 = getval("rd") + getval("ad") + at; d = update_dutycycle(d); abort_dutycycle(d,10.0); // Set Phase Tables settable(ph1Hhytrap,4,table1); settable(phYhytrap,4,table2); settable(ph2Hhytrap,4,table3); settable(phXhx,4,table4); settable(phHhx,4,table5); settable(phRec,4,table6); setreceiver(phRec); // Begin Sequence txphase(phXhx); decphase(ph1Hhytrap); dec2phase(phYhytrap); obspwrf(getval("aXhx")); decpwrf(getval("aHhytrap")); dec2pwrf(getval("aYhytrap")); obsunblank(); decunblank(); _unblank34(); delay(d1); sp1on(); delay(2.0e-6); sp1off(); delay(2.0e-6); // TRAPDOR on H with Y Modulation decrgpulse(getval("pw1Hhytrap"),ph1Hhytrap,0.0,0.0); decphase(ph2Hhytrap); decunblank(); dec2on(); delay(getval("t1HYtrap")); dec2off(); decrgpulse(getval("pw2Hhytrap"),ph2Hhytrap,0.0,0.0); decphase(phHhx); decunblank(); decphase(phHhx); decpwrf(getval("aHhx")); delay(getval("t2HYtrap")); // H to X Cross Polarization _cp_(hx,phHhx,phXhx); // Begin Acquisition _dseqon(dec); obsblank(); _blank34(); delay(getval("rd")); startacq(getval("ad")); acquire(np, 1/sw); endacq(); _dseqoff(dec); obsunblank(); decunblank(); _unblank34(); }
void pulsesequence() { // Set the Maximum Dynamic Table and v-var Numbers settablenumber(20); setvvarnumber(30); // Define Variables and Objects and Get Parameter Values MPSEQ dumbo = getdumbogen("dumboX","dcf1X",0,0.0,0.0,0,1); strncpy(dumbo.ch,"obs",3); putCmd("chXdumbo='obs'\n"); MPSEQ c7 = getpostc7("c7X",0,0.0,0.0,0,1); MPSEQ c7ref = getpostc7("c7X",c7.iSuper,c7.phAccum,c7.phInt,1,1); strncpy(c7.ch,"obs",3); putCmd("chXc7='obs'\n"); WMPA wdumbo = getwdumbogen("wdumboX","dcfX"); strncpy(wdumbo.ch,"obs",3); putCmd("chXwdumbo='obs'\n"); double tXzfinit = getval("tXzf"); //Define the Z-filter delay in the sequence double tXzf = tXzfinit - 5.0e-6 - wdumbo.r1; // Set Constant-time Period for d2. if (d2_index == 0) d2_init = getval("d2"); double d2_ = (ni - 1)/sw1 + d2_init; putCmd("d2acqret = %f\n",roundoff(d2_,12.5e-9)); putCmd("d2dwret = %f\n",roundoff(1.0/sw1,12.5e-9)); //-------------------------------------- // Copy Current Parameters to Processed //------------------------------------- putCmd("groupcopy('current','processed','acquisition')"); // Dutycycle Protection DUTY d = init_dutycycle(); d.dutyon = c7.t + getval("pwXtilt") + d2_ + getval("pwXtilt") + c7ref.t + getval("pwX90") + + wdumbo.q*wdumbo.cycles*wdumbo.pw; d.dutyoff = 4.0e-6 + d1 + tXzfinit + wdumbo.r2 + at - wdumbo.q*wdumbo.cycles*wdumbo.pw; d = update_dutycycle(d); abort_dutycycle(d,10.0); // Set Phase Tables settable(ph1Xc7,4,table1); settable(phXdumbo,4,table2); settable(ph2Xc7,4,table3); settable(phX90,16,table4); settable(phXwdumbo,4,table5); settable(phRec,16,table6); settable(ph1Xtilt,4,table7); settable(ph2Xtilt,4,table8); // Set the Small-Angle Prep Phase double obsstep = 360.0/(PSD*8192); obsstepsize(obsstep); int phfX90 = initphase(0.0, obsstep); //Add STATES Quadrature Phase if (phase1 == 2) initval((45.0/obsstep),v1); else initval(0.0,v1); initval((d2*c7.of[0]*360.0/obsstep),v2); initval(0.0,v3); obsstepsize(obsstep); setreceiver(phRec); // Begin Sequence xmtrphase(v1); txphase(ph1Xc7); obspwrf(getval("aXc7")); obsunblank(); decunblank(); _unblank34(); delay(d1); sp1on(); delay(2.0e-6); sp1off(); delay(2.0e-6); // C7 Recoupling of 2Q coherence _mpseq(c7, ph1Xc7); // F1 Evolution With DUMBO xmtrphase(v3); if (!getval("scXdcf1")){ obspwrf(getval("aX90")); rgpulse(getval("pwXtilt"),ph1Xtilt,0.0,0.0); } obspwrf(getval("aXdumbo")); obsunblank(); _mpseqon(dumbo,phXdumbo); delay(d2); _mpseqoff(dumbo); if (!getval("scXdcf1")){ obspwrf(getval("aX90")); rgpulse(getval("pwXtilt"),ph2Xtilt,0.0,0.0); } obspwrf(getval("aX90")); obsunblank(); // C7 Transfer to 1Q Coherence xmtrphase(v2); _mpseq(c7ref, ph2Xc7); // Z-filter Delay delay(tXzf); // Detection Pulse txphase(phX90); obspwrf(getval("aX90")); startacq(5.0e-6); rcvroff(); delay(wdumbo.r1); rgpulse(getval("pwX90"), phX90, 0.0, 0.0); obsunblank(); xmtrphase(v3); delay(wdumbo.r2); // Apply WPMLG Cycles During Acqusition decblank(); _blank34(); _wdumbo(wdumbo,phXwdumbo); endacq(); obsunblank(); decunblank(); _unblank34(); }
pulsesequence() { // Set the Maximum Dynamic Table and v-var Numbers settablenumber(10); setvvarnumber(30); // Define Variables and Objects and Get Parameter Values double aXprep = getval("aXprep"); double pwXprep = getval("pwXprep"); double phvXprep = getval("phXprep"); WMPA wsam = getwsamn("wsamX"); strncpy(wsam.ch,"obs",3); putCmd("chXwsam='obs'\n"); //-------------------------------------- // Copy Current Parameters to Processed //------------------------------------- putCmd("groupcopy('current','processed','acquisition')"); // Dutycycle Protection DUTY d = init_dutycycle(); d.dutyon = getval("pwXprep") + wsam.cycles1*wsam.cycles*wsam.pw; d.dutyoff = d1 + 4.0e-6 + 5.0e-6 + wsam.r1 + wsam.r2 + at - wsam.cycles1*wsam.cycles*wsam.pw; d = update_dutycycle(d); abort_dutycycle(d,10.0); // Set Phase Tables settable(phXprep,4,table1); settable(phXwsam,4,table2); settable(phRec,4,table3); setreceiver(phRec); // Set the Small-Angle Step double obsstep = 360.0/(PSD*8192); obsstepsize(obsstep); int phfXprep = initphase(phvXprep,obsstep); int phXzero = initphase(0.0,obsstep); // Begin Sequence xmtrphase(phfXprep); txphase(phXprep); obspwrf(aXprep); obsunblank(); decunblank(); _unblank34(); delay(d1); sp1on(); delay(2.0e-6); sp1off(); delay(2.0e-6); // Standard 90-degree prepX pulse for SAM startacq(5.0e-6); rcvroff(); delay(wsam.r1); rgpulse(pwXprep, phXprep, 0.0, 0.0); xmtrphase(phXzero); delay(wsam.r2); // Apply WSAM Cycles decblank(); _blank34(); _wsamn(wsam, phXwsam); endacq(); obsunblank(); decunblank(); _unblank34(); }
void pulsesequence() { // Define Variables and Objects and Get Parameter Values CP hy = getcp("HY",0.0,0.0,0,1); strncpy(hy.fr,"dec",3); strncpy(hy.to,"dec2",4); putCmd("frHY='dec'\n"); putCmd("toHY='dec2'\n"); CP yx = getcp("YX",0.0,0.0,0,1); strncpy(yx.fr,"dec2",4); strncpy(yx.to,"obs",3); putCmd("frYX='dec2'\n"); putCmd("toYX='obs'\n"); DSEQ dec = getdseq("H"); strncpy(dec.t.ch,"dec",3); putCmd("chHtppm='dec'\n"); strncpy(dec.s.ch,"dec",3); putCmd("chHspinal='dec'\n"); //-------------------------------------- // Copy Current Parameters to Processed //------------------------------------- putCmd("groupcopy('current','processed','acquisition')"); // Dutycycle Protection DUTY d = init_dutycycle(); d.dutyon = getval("pwY90") + getval("pwH90") + getval("tHY") + getval("tYX") + 2.0*getval("pwX90"); d.dutyoff = d1 + 4.0e-6; d.c1 = d.c1 + (!strcmp(dec.seq,"tppm")); d.c1 = d.c1 + ((!strcmp(dec.seq,"tppm")) && (dec.t.a > 0.0)); d.t1 = getval("rd") + getval("ad") + at; d.c2 = d.c2 + (!strcmp(dec.seq,"spinal")); d.c2 = d.c2 + ((!strcmp(dec.seq,"spinal")) && (dec.s.a > 0.0)); d.t2 = getval("rd") + getval("ad") + at; d = update_dutycycle(d); abort_dutycycle(d,10.0); // Create Phasetables settable(phH90,4,table1); settable(phHhy,4,table2); settable(phY90,4,table3); settable(phYhy,4,table4); settable(phHyx,4,table5); settable(phYyx,4,table6); settable(phXyx,8,table7); settable(phRec,8,table8); // Begin Sequence setreceiver(phRec); txphase(phXyx); decphase(phH90); dec2phase(phY90); obspwrf(getval("aXyx")); decpwrf(getval("aH90")); dec2pwrf(getval("aY90")); obsunblank(); decunblank(); _unblank34(); delay(d1); sp1on(); delay(2.0e-6); sp1off(); delay(2.0e-6); // H to Y Cross Polarization with a Y Prepulse dec2rgpulse(getval("pwY90"),phY90,0.0,0.0); dec2phase(phYhy); dec2pwrf(getval("aYyx")); decrgpulse(getval("pwH90"),phH90,0.0,0.0); decphase(phHhy); _cp_(hy,phHhy,phYhy); // Y to X Cross Polarization decphase(phHyx); dec2phase(phYyx); decpwrf(getval("aHyx")); decunblank(); decon(); _cp_(yx,phYyx,phXyx); decphase(phHhy); dec2blank(); decoff(); // Begin Acquisition _dseqon(dec); obsblank(); _blank34(); delay(getval("rd")); startacq(getval("ad")); acquire(np, 1/sw); endacq(); _dseqoff(dec); obsunblank(); decunblank(); _unblank34(); }
pulsesequence() { // Define Variables and Objects and Get Parameter Values CP hy = getcp("HY",0.0,0.0,0,1); strncpy(hy.fr,"dec",3); strncpy(hy.to,"dec2",4); putCmd("frHY='dec'\n"); putCmd("toHY='dec2'\n"); CP yx = getcp("YX",0.0,0.0,0,1); strncpy(yx.fr,"dec2",4); strncpy(yx.to,"obs",3); putCmd("frYX='dec2'\n"); putCmd("toYX='obs'\n"); DSEQ dec = getdseq("H"); strncpy(dec.t.ch,"dec",3); putCmd("chHtppm='dec'\n"); strncpy(dec.s.ch,"dec",3); putCmd("chHspinal='dec'\n"); // Set Constant-time Period for d2. if (d2_index == 0) d2_init = getval("d2"); double d2_ = (ni - 1)/sw1 + d2_init; putCmd("d2acqret = %f\n",roundoff(d2_,12.5e-9)); putCmd("d2dwret = %f\n",roundoff(1.0/sw1,12.5e-9)); // Set Constant-time Period for d3. if (d3_index == 0) d3_init = getval("d3"); double d3_ = (ni - 1)/sw1 + d3_init; putCmd("d3acqret = %f\n",roundoff(d3_,12.5e-9)); putCmd("d3dwret = %f\n",roundoff(1.0/sw2,12.5e-9)); // Set Mixing Period to N Rotor Cycles double taur,mix,srate; mix = getval("tXmix"); srate = getval("srate"); taur = 0.0; if (srate >= 500.0) taur = roundoff((1.0/srate), 0.125e-6); else { printf("ABORT: Spin Rate (srate) must be greater than 500\n"); psg_abort(1); } mix = roundoff(mix,taur); mix = mix - getval("pwX90"); if (mix < 0.0) mix = 0.0; //-------------------------------------- // Copy Current Parameters to Processed //------------------------------------- putCmd("groupcopy('current','processed','acquisition')"); // Dutycycle Protection DUTY d = init_dutycycle(); d.dutyon = getval("pwY90") + getval("pwH90") + getval("tHY") + getval("tYX") + 2.0*getval("pwX90") + mix; d.dutyoff = d1 + 4.0e-6; d.c1 = d.c1 + (!strcmp(dec.seq,"tppm")); d.c1 = d.c1 + ((!strcmp(dec.seq,"tppm")) && (dec.t.a > 0.0)); d.t1 = d2 + d3 + getval("rd") + getval("ad") + at; d.c2 = d.c2 + (!strcmp(dec.seq,"spinal")); d.c2 = d.c2 + ((!strcmp(dec.seq,"spinal")) && (dec.s.a > 0.0)); d.t2 = d2 + d3 + getval("rd") + getval("ad") + at; d = update_dutycycle(d); abort_dutycycle(d,10.0); // Create Phasetables settable(phH90,4,table1); settable(phHhy,4,table2); settable(phY90,4,table3); settable(phYhy,4,table4); settable(phHyx,4,table5); settable(phYyx,4,table6); settable(phXyx,8,table7); settable(phXmix1,8,table8); settable(phXmix2,8,table9); settable(phRec,8,table10); if (phase2 == 2) tsadd(phXyx,1,4); if (phase1 == 2) tsadd(phYhy,1,4); // Begin Sequence setreceiver(phRec); txphase(phXyx); decphase(phH90); dec2phase(phY90); obspwrf(getval("aXyx")); decpwrf(getval("aH90")); dec2pwrf(getval("aY90")); obsunblank(); decunblank(); _unblank34(); delay(d1); sp1on(); delay(2.0e-6); sp1off(); delay(2.0e-6); // H to Y Cross Polarization with a Y Prepulse dec2rgpulse(getval("pwY90"),phY90,0.0,0.0); dec2phase(phYhy); dec2pwrf(getval("aYyx")); decrgpulse(getval("pwH90"),phH90,0.0,0.0); decphase(phHhy); _cp_(hy,phHhy,phYhy); // F1 Indirect Period For Y _dseqon(dec); delay(d2); _dseqoff(dec); // Y to X Cross Polarization decphase(phHyx); dec2phase(phYyx); decpwrf(getval("aHyx")); decunblank(); decon(); _cp_(yx,phYyx,phXyx); decphase(phHhy); decoff(); // F2 Indirect Period for X txphase(phXmix1); obspwrf(getval("aX90")); _dseqon(dec); delay(d3); _dseqoff(dec); // RAD(DARR) Mixing For X decpwrf(getval("aHmix")); decunblank(); decon(); rgpulse(getval("pwX90"),phXmix1,0.0,0.0); txphase(phXmix2); obsunblank(); delay(mix); rgpulse(getval("pwX90"),phXmix2,0.0,0.0); decoff(); // Begin Acquisition _dseqon(dec); obsblank(); _blank34(); delay(getval("rd")); startacq(getval("ad")); acquire(np, 1/sw); endacq(); _dseqoff(dec); obsunblank(); decunblank(); _unblank34(); }
pulsesequence() { // Define Variables and Objects and Get Parameter Values double pwX90 = getval("pwX90"); double d22 = d2/2.0 - pwX90; if (d22 < 0.0) d22 = 0.0; MPSEQ fh = getfslg("fslgH",0,0.0,0.0,0,1); strncpy(fh.ch,"dec",3); putCmd("chHfslg='dec'\n"); CP hx = getcp("HX",0.0,0.0,0,1); strncpy(hx.fr,"dec",3); strncpy(hx.to,"obs",3); putCmd("frHX='dec'\n"); putCmd("toHX='obs'\n"); DSEQ dec = getdseq("H"); strncpy(dec.t.ch,"dec",3); putCmd("chHtppm='dec'\n"); strncpy(dec.s.ch,"dec",3); putCmd("chHspinal='dec'\n"); // Set Constant-time Period for d2. if (d2_index == 0) d2_init = getval("d2"); double d2_ = (ni - 1)/sw1 + d2_init; putCmd("d2acqret = %f\n",roundoff(d2_,12.5e-9)); putCmd("d2dwret = %f\n",roundoff(1.0/sw1,12.5e-9)); //-------------------------------------- // Copy Current Parameters to Processed //------------------------------------- putCmd("groupcopy('current','processed','acquisition')"); // Dutycycle Protection DUTY d = init_dutycycle(); d.dutyon = 3.0*getval("pwHtilt") + d2_ + getval("pwH90") + getval("tHX"); d.dutyoff = d1 + 4.0e-6; d.c1 = d.c1 + (!strcmp(dec.seq,"tppm")); d.c1 = d.c1 + ((!strcmp(dec.seq,"tppm")) && (dec.t.a > 0.0)); d.t1 = getval("rd") + getval("ad") + at; d.c2 = d.c2 + (!strcmp(dec.seq,"spinal")); d.c2 = d.c2 + ((!strcmp(dec.seq,"spinal")) && (dec.s.a > 0.0)); d.t2 = getval("rd") + getval("ad") + at; d = update_dutycycle(d); abort_dutycycle(d,10.0); // Set Phase Tables settable(phHtilt,4,table1); settable(phHfslg,4,table2); settable(phHtilt2,4,table3); settable(phH90,4,table4); settable(phHtilt3,4,table5); settable(phXhx,4,table6); settable(phHhx,4,table7); settable(phRec,4,table8); //Add STATES TPPI ("States with "FAD") tsadd(phRec,2*d2_index,4); if (phase1 == 2) { tsadd(phHtilt3,2*d2_index+3,4); tsadd(phHhx,2*d2_index+3,4); } else { tsadd(phHtilt3,2*d2_index,4); tsadd(phHhx,2*d2_index,4); } setreceiver(phRec); // Begin Sequence txphase(phXhx); decphase(phHtilt); obspwrf(getval("aXhx")); decpwrf(getval("aH90")); obsunblank();decunblank();_unblank34(); delay(d1); sp1on(); delay(2.0e-6); sp1off(); delay(2.0e-6); // H Preparation with a Tilt Pulse decrgpulse(getval("pwHtilt"),phHtilt,0.0,0.0); // FSLG spinlock on H and Reverse Tilt to Zed _mpseqon(fh,phHfslg); delay(d22); rgpulse(2.0*pwX90,zero,0.0,0.0); txphase(phXhx); delay(d22); _mpseqoff(fh); decpwrf(getval("aH90")); decrgpulse(getval("pwHtilt"),phHtilt2,0.0,0.0); // H 90 and Ramped H to X Cross Polarization with LG Offset decrgpulse(getval("pwH90"),phH90,0.0,0.0); decrgpulse(getval("pwHtilt"),phHtilt3,0.0,0.0); decphase(phHhx); _cp_(hx,phHhx,phXhx); // Begin Acquisition obsblank(); _blank34(); _dseqon(dec); delay(getval("rd")); startacq(getval("ad")); acquire(np, 1/sw); endacq(); _dseqoff(dec); obsunblank(); decunblank(); _unblank34(); }
void pulsesequence() { // Define Variables and Objects and Get Parameter Values CP hx = getcp("HX",0.0,0.0,0,1); strncpy(hx.fr,"dec",3); strncpy(hx.to,"obs",3); putCmd("frHX='dec'\n"); putCmd("toHX='obs'\n"); PBOXPULSE shca = getpboxpulse("shcaX",0,1); strncpy(shca.ch,"obs",3); putCmd("chXshca ='obs'\n"); PBOXPULSE shco = getpboxpulse("shcoX",0,1); strncpy(shco.ch,"obs",3); putCmd("chXshco ='obs'\n"); PBOXPULSE shcaco = combine_PBOXPULSE(shca,shco,0,1); DSEQ dec = getdseq("H"); strncpy(dec.t.ch,"dec",3); putCmd("chHtppm='dec'\n"); strncpy(dec.s.ch,"dec",3); putCmd("chHspinal='dec'\n"); DSEQ mix = getdseq("Hmix"); strncpy(mix.t.ch,"dec",3); putCmd("chHmixtppm='dec'\n"); strncpy(mix.s.ch,"dec",3); putCmd("chHmixspinal='dec'\n"); double shcacolen = (shcaco.pw + 2.0*shcaco.t2)/2.0; double d22 = d2/2.0; // Set Constant-time Period for d2. if (d2_index == 0) d2_init = getval("d2"); double d2_ = (ni - 1)/sw1 + d2_init; putCmd("d2acqret = %f\n",roundoff(d2_,12.5e-9)); putCmd("d2dwret = %f\n",roundoff(1.0/sw1,12.5e-9)); //-------------------------------------- // Copy Current Parameters to Processed //------------------------------------- putCmd("groupcopy('current','processed','acquisition')"); // Dutycycle Protection DUTY d = init_dutycycle(); d.dutyon = getval("pwH90") + getval("tHX") + 2.0*shcaco.pw + 4.0*getval("pwX90"); d.dutyoff = d1 + 4.0e-6; d.c1 = d.c1 + (!strcmp(dec.seq,"tppm")); d.c1 = d.c1 + ((!strcmp(dec.seq,"tppm")) && (dec.t.a > 0.0)); d.t1 = d2_ + getval("tZF") - getval("pwX90") + getval("rd") + getval("ad") + at; d.c2 = d.c2 + (!strcmp(dec.seq,"spinal")); d.c2 = d.c2 + ((!strcmp(dec.seq,"spinal")) && (dec.s.a > 0.0)); d.t2 = d2_ + getval("tZF") - getval("pwX90") + getval("rd") + getval("ad") + at; d.c3 = d.c3 + (!strcmp(mix.seq,"tppm")); d.c3 = d.c3 + ((!strcmp(mix.seq,"tppm")) && (mix.t.a > 0.0)); d.t3 = 2.0*getval("taua") + 2.0*getval("taub") + 2.0*shcaco.t1 + 2.0*shcaco.t2 - 4.0*shcacolen - 2.5*getval("pwX90") - 6.0e-6; d.c4 = d.c4 + (!strcmp(mix.seq,"spinal")); d.c4 = d.c4 + ((!strcmp(mix.seq,"spinal")) && (mix.s.a > 0.0)); d.t4 = 2.0*getval("taua") + 2.0*getval("taub") + 2.0*shcaco.t1 + 2.0*shcaco.t2 - 4.0*shcacolen - 2.5*getval("pwX90") - 6.0e-6; d = update_dutycycle(d); abort_dutycycle(d,10.0); // Set Up 2D int errval = (int) ((getval("taua") - shcacolen)*2.0*sw1); if ((getval("taua") - ni/(2.0*sw1) - shcacolen) < 0.0) { text_error("Error:ni is too large. Make ni equal to %d or less.\n",errval); psg_abort(1); } // Set Phase Tables settable(phH90,4,table1); settable(phXhx,4,table2); settable(phHhx,4,table3); settable(ph1Xshcaco,4,table4); settable(ph1X90,4,table5); settable(ph2X90,4,table6); settable(ph2Xshcaco,4,table7); settable(ph3X90,4,table8); settable(ph4X90,4,table9); settable(phRec,4,table10); setreceiver(phRec); // States Acquisition if (phase1 == 2) tsadd(phXhx,3,4); // Begin Sequence txphase(phXhx); decphase(phH90); obspwrf(getval("aXhx")); decpwrf(getval("aH90")); obsunblank(); decunblank(); _unblank34(); delay(d1); sp1on(); delay(2.0e-6); sp1off(); delay(2.0e-6); // H to X Cross Polarization decrgpulse(getval("pwH90"),phH90,0.0,0.0); decphase(phHhx); _cp_(hx,phHhx,phXhx); decphase(zero); // Begin F1 Refocused INEPT _dseqon(mix); txphase(ph1Xshcaco); obspwrf(shcaco.a); delay(getval("taua") - d22 - shcacolen); _pboxpulse(shcaco,ph1Xshcaco); obsblank(); obspower(getval("tpwr")); delay(3.0e-6); obsunblank(); obsunblank(); txphase(ph1X90); obspwrf(getval("aX90")); delay(getval("taua") + d22 - shcacolen - getval("pwX90") - 3.0e-6); rgpulse(getval("pwX90"),ph1X90,0.0,0.0); rgpulse(getval("pwX90"),ph2X90,0.0,0.0); txphase(ph2Xshcaco); obspwrf(shcaco.a); obsunblank(); delay(getval("taub") - shcacolen - getval("pwX90")); _pboxpulse(shcaco,ph2Xshcaco); obsblank(); obspower(getval("tpwr")); delay(3.0e-6); obsunblank(); txphase(ph3X90); obspwrf(getval("aX90")); obsunblank(); delay(getval("taub") - shcacolen - getval("pwX90")/2.0 - 3.0e-6); rgpulse(getval("pwX90"),ph3X90,0.0,0.0); txphase(ph4X90); obsunblank(); _dseqoff(mix); _dseqon(dec); delay(getval("tZF") - getval("pwX90")); rgpulse(getval("pwX90"),ph4X90,0.0,0.0); // Begin Acquisition obsblank(); _blank34(); delay(getval("rd")); startacq(getval("ad")); acquire(np, 1/sw); endacq(); _dseqoff(dec); obsunblank(); decunblank(); _unblank34(); }
pulsesequence() { // Define Variables and Objects and Get Parameter Values CP hx = getcp("HX",0.0,0.0,0,1); strncpy(hx.fr,"dec",3); strncpy(hx.to,"obs",3); putCmd("frHX='dec'\n"); putCmd("toHX='obs'\n"); MPSEQ fh = getfslg("fslgH",0,0.0,0.0,0,1); strncpy(fh.ch,"dec",3); putCmd("chHfslg='dec'\n"); MPSEQ fx = getfslg("fslgX",0,0.0,0.0,0,1); strncpy(fx.ch,"obs",3); putCmd("chXfslg='obs'\n"); DSEQ dec = getdseq("H"); strncpy(dec.t.ch,"dec",3); putCmd("chHtppm='dec'\n"); strncpy(dec.s.ch,"dec",3); putCmd("chHspinal='dec'\n"); // Set Constant-time Period for d2. if (d2_index == 0) d2_init = getval("d2"); double d2_ = (ni - 1)/sw1 + d2_init; putCmd("d2acqret = %f\n",roundoff(d2_,12.5e-9)); putCmd("d2dwret = %f\n",roundoff(1.0/sw1,12.5e-9)); //-------------------------------------- // Copy Current Parameters to Processed //------------------------------------- putCmd("groupcopy('current','processed','acquisition')"); // Dutycycle Protection DUTY d = init_dutycycle(); d.dutyon = getval("pwH90") + getval("tHX") + d2_; d.dutyoff = d1 + 4.0e-6; d.c1 = d.c1 + (!strcmp(dec.seq,"tppm")); d.c1 = d.c1 + ((!strcmp(dec.seq,"tppm")) && (dec.t.a > 0.0)); d.t1 = getval("rd") + getval("ad") + at; d.c2 = d.c2 + (!strcmp(dec.seq,"spinal")); d.c2 = d.c2 + ((!strcmp(dec.seq,"spinal")) && (dec.s.a > 0.0)); d.t2 = getval("rd") + getval("ad") + at; d = update_dutycycle(d); abort_dutycycle(d,10.0); // Set Phase Tables settable(phH90,4,table1); settable(phXhx,4,table2); settable(phHhx,4,table3); settable(phHtilt,4,table4); settable(phHfslg,4,table5); settable(phXlock,4,table6); settable(phRec,4,table7); setreceiver(phRec); // Begin Sequence txphase(phXhx); decphase(phH90); obspwrf(getval("aXhx")); decpwrf(getval("aH90")); obsunblank(); decunblank(); _unblank34(); delay(d1); sp1on(); delay(2.0e-6); sp1off(); delay(2.0e-6); // H to X Cross Polarization decrgpulse(getval("pwH90"),phH90,0.0,0.0); decphase(phHhx); _cp_(hx,phHhx,phXhx); // Tilt Pulse on H with Continued X Spinlock xmtron(); decon(); decpwrf(getval("aH90")); obspwrf(getval("aXhx")); decrgpulse(getval("pwHtilt"),phHtilt,0.0,0.0); // FSLG Spinlocks on X and H xmtron(); decon(); _mpseqon(fh,phHfslg); _mpseqon(fx,phXlock); delay(d2); _mpseqoff(fh); _mpseqoff(fx); // Begin Acquisition obsblank(); _blank34(); _dseqon(dec); delay(getval("rd")); startacq(getval("ad")); acquire(np, 1/sw); endacq(); _dseqoff(dec); obsunblank(); decunblank(); _unblank34(); }
pulsesequence() { // Define Variables and Objects and Get Parameter Values SHAPE p1 = getpulse("90H",0.0,0.0,1,0); strncpy(p1.pars.ch,"dec",3); putCmd("chH90='dec'\n"); p1.pars.array = disarry("xx", p1.pars.array); p1 = update_shape(p1,0.0,0.0,1); MPSEQ ph = getpmlgxmx("pmlgH",0,0.0,0.0,1,0); strncpy(ph.ch,"dec",3); putCmd("chHpmlg='dec'\n"); double pwHpmlg = getval("pwHpmlg"); ph.nelem = (int) (d2/(2.0*pwHpmlg) + 0.1); ph.array = disarry("xx", ph.array); ph = update_mpseq(ph,0,p1.pars.phAccum,p1.pars.phInt,1); SHAPE p2 = getpulse("90H",0.0,0.0,2,0); strncpy(p2.pars.ch,"dec",3); putCmd("chH90='dec'\n"); p2.pars.array = disarry("xx", p2.pars.array); p2 = update_shape(p2,ph.phAccum,ph.phInt,2); double pwX180 = getval("pwX180"); double d22 = ph.t/2.0 - pwX180/2.0; if (d22 < 0.0) d22 = 0.0; // CP hx and DSEQ dec Return to the Reference Phase CP hx = getcp("HX",0.0,0.0,0,1); strncpy(hx.fr,"dec",3); strncpy(hx.to,"obs",3); putCmd("frHX='dec'\n"); putCmd("toHX='obs'\n"); DSEQ dec = getdseq("H"); strncpy(dec.t.ch,"dec",3); putCmd("chHtppm='dec'\n"); strncpy(dec.s.ch,"dec",3); putCmd("chHspinal='dec'\n"); // Set Constant-time Period for d2. if (d2_index == 0) d2_init = getval("d2"); double d2_ = (ni - 1)/sw1 + d2_init; putCmd("d2acqret = %f\n",roundoff(d2_,12.5e-9)); putCmd("d2dwret = %f\n",roundoff(1.0/sw1,12.5e-9)); //-------------------------------------- // Copy Current Parameters to Processed //------------------------------------- putCmd("groupcopy('current','processed','acquisition')"); // Dutycycle Protection DUTY d = init_dutycycle(); d.dutyon = p1.pars.t + d2_ + p2.pars.t + getval("pwH90") + getval("pwHtilt") + getval("tHX"); d.dutyoff = d1 + 4.0e-6 + getval("tHmix"); d.c1 = d.c1 + (!strcmp(dec.seq,"tppm")); d.c1 = d.c1 + ((!strcmp(dec.seq,"tppm")) && (dec.t.a > 0.0)); d.t1 = getval("rd") + getval("ad") + at; d.c2 = d.c2 + (!strcmp(dec.seq,"spinal")); d.c2 = d.c2 + ((!strcmp(dec.seq,"spinal")) && (dec.s.a > 0.0)); d.t2 = getval("rd") + getval("ad") + at; d = update_dutycycle(d); abort_dutycycle(d,10.0); // Set Phase Tables settable(ph1H90,4,table1); settable(phHpmlg,4,table2); settable(ph2H90,4,table3); settable(ph3H90,4,table4); settable(phHtilt,4,table5); settable(phXhx,4,table6); settable(phHhx,4,table7); settable(phRec,4,table8); //Add STATES TPPI ("States with "FAD") tsadd(phRec,2*d2_index,4); if (phase1 == 2) { tsadd(ph2H90,2*d2_index+3,4); } else { tsadd(ph2H90,2*d2_index,4); } setreceiver(phRec); // Begin Sequence txphase(phXhx); decphase(ph1H90); obspwrf(getval("aX180")); decpwrf(getval("aH90")); obsunblank();decunblank(); _unblank34(); delay(d1); sp1on(); delay(2.0e-6); sp1off(); delay(2.0e-6); // Offset H Preparation with a Tilt Pulse _shape(p1,ph1H90); // Offset SAMn Spinlock on H During F1 with Optional pwX180 _mpseqon(ph,phHpmlg); delay(d22); rgpulse(pwX180,zero,0.0,0.0); obspwrf(getval("aX90")); txphase(phXhx); delay(d22); _mpseqoff(ph); // Offset 90-degree Pulse to Zed and Spin-Diffusion Mix _shape(p2,ph2H90); decpwrf(getval("aH90")); delay(getval("tHmix")); // H90, 35-degree Tilt and H-to-X Cross Polarization with LG Offset decrgpulse(getval("pwH90"),ph3H90,0.0,0.0); decunblank(); decrgpulse(getval("pwHtilt"),phHtilt,0.0,0.0); decphase(phHhx); _cp_(hx,phHhx,phXhx); // Begin Acquisition obsblank(); _blank34(); _dseqon(dec); delay(getval("rd")); startacq(getval("ad")); acquire(np, 1/sw); endacq(); _dseqoff(dec); obsunblank(); decunblank(); _unblank34(); }
void pulsesequence() { // Define Variables and Objects and Get Parameter Values CP hx = getcp("HX",0.0,0.0,0,1); strncpy(hx.fr,"dec",3); strncpy(hx.to,"obs",3); putCmd("frHX='dec'\n"); putCmd("toHX='obs'\n"); MPSEQ spc5 = getspc5("spc5X",0,0.0,0.0,0,1); MPSEQ spc5ref = getspc5("spc5X",spc5.iSuper,spc5.phAccum,spc5.phInt,1,1); strncpy(spc5.ch,"obs",3); putCmd("chXspc5='obs'\n"); DSEQ dec = getdseq("H"); strncpy(dec.t.ch,"dec",3); putCmd("chHtppm='dec'\n"); strncpy(dec.s.ch,"dec",3); putCmd("chHspinal='dec'\n"); // Set Constant-time Period for d2. if (d2_index == 0) d2_init = getval("d2"); double d2_ = (ni - 1)/sw1 + d2_init; putCmd("d2acqret = %f\n",roundoff(d2_,12.5e-9)); putCmd("d2dwret = %f\n",roundoff(1.0/sw1,12.5e-9)); //-------------------------------------- // Copy Current Parameters to Processed //------------------------------------- putCmd("groupcopy('current','processed','acquisition')"); // Dutycycle Protection DUTY d = init_dutycycle(); d.dutyon = getval("pwH90") + getval("tHX") + getval("pwX90") + spc5.t + spc5ref.t; d.dutyoff = d1 + 4.0e-6 + 2.0*getval("tZF"); d.c1 = d.c1 + (!strcmp(dec.seq,"tppm")); d.c1 = d.c1 + ((!strcmp(dec.seq,"tppm")) && (dec.t.a > 0.0)); d.t1 = d2_ + getval("rd") + getval("ad") + at; d.c2 = d.c2 + (!strcmp(dec.seq,"spinal")); d.c2 = d.c2 + ((!strcmp(dec.seq,"spinal")) && (dec.s.a > 0.0)); d.t2 = d2_ + getval("rd") + getval("ad") + at; d = update_dutycycle(d); abort_dutycycle(d,10.0); // Create Phasetables settable(phH90,4,table1); settable(phHhx,4,table2); settable(phXhx,4,table3); settable(phXmix1,4,table4); settable(phXmix2,4,table5); settable(phRec,4,table6); setreceiver(phRec); if (phase1 == 2) tsadd(phXhx,1,4); // Begin Sequence txphase(phXhx); decphase(phH90); obspwrf(getval("aXhx")); decpwrf(getval("aH90")); obsunblank(); decunblank(); _unblank34(); delay(d1); sp1on(); delay(2.0e-6); sp1off(); delay(2.0e-6); // H to X Cross Polarization decrgpulse(getval("pwH90"),phH90,0.0,0.0); decphase(phHhx); _cp_(hx,phHhx,phXhx); // F2 Indirect Period for X obspwrf(getval("aX90")); _dseqon(dec); delay(d2); _dseqoff(dec); // Mixing with SPC5 Recoupling rgpulse(getval("pwX90"),phXmix1,0.0,0.0); obspwrf(getval("aXspc5")); xmtrphase(v1); txphase(phXmix1); delay(getval("tZF")); decpwrf(getval("aHmix")); decon(); _mpseq(spc5, phXmix1); xmtrphase(v2); txphase(phXmix2); _mpseq(spc5ref, phXmix2); decoff(); obspwrf(getval("aX90")); xmtrphase(zero); txphase(phXmix2); delay(getval("tZF")); rgpulse(getval("pwX90"),phXmix2,0.0,0.0); // Begin Acquisition _dseqon(dec); obsblank(); _blank34(); delay(getval("rd")); startacq(getval("ad")); acquire(np, 1/sw); endacq(); _dseqoff(dec); obsunblank(); decunblank(); _unblank34(); }
void pulsesequence() { // Define Variables and Objects and Get Parameter Values MPSEQ fh = getfslg("fslgH",0,0.0,0.0,0,1); strncpy(fh.ch,"dec",3); putCmd("chHfslg='dec'\n"); double tHXhmqc = getval("tHXhmqc"); //parameters for hmqcHX implemented double pwHhxhmqc = getval("pwHhxhmqc"); //directly in the pulse sequence double pmHhxhmqc = getval("pmHhxhmqc"); double pwXhxhmqc = getval("pwXhxhmqc"); double aXhxhmqc = getval("aXhxhmqc"); double aHhxhmqc = getval("aHhxhmqc"); double d2init = getval("d2"); d2init = d2init - pwXhxhmqc; if (d2init < 0.0) d2init = 0.0; double d22 = d2init/2.0; CP hx = getcp("HX",0.0,0.0,0,1); strncpy(hx.fr,"dec",3); strncpy(hx.to,"obs",3); putCmd("frHX='dec'\n"); putCmd("toHX='obs'\n"); DSEQ dec = getdseq("H"); strncpy(dec.t.ch,"dec",3); putCmd("chHtppm='dec'\n"); strncpy(dec.s.ch,"dec",3); putCmd("chHspinal='dec'\n"); // Set Constant-time Period for d2. if (d2_index == 0) d2_init = getval("d2"); double d2_ = (ni - 1)/sw1 + d2_init; putCmd("d2acqret = %f\n",roundoff(d2_,12.5e-9)); putCmd("d2dwret = %f\n",roundoff(1.0/sw1,12.5e-9)); //-------------------------------------- // Copy Current Parameters to Processed //------------------------------------- putCmd("groupcopy('current','processed','acquisition')"); // Dutycycle Protection DUTY d = init_dutycycle(); d.dutyon = getval("pwH90") + getval("tHX")+ 2.0*tHXhmqc + d2_ + 4.0*pmHhxhmqc + 2.0*pwHhxhmqc; d.dutyoff = d1 + 4.0e-6; d.c1 = d.c1 + (!strcmp(dec.seq,"tppm")); d.c1 = d.c1 + ((!strcmp(dec.seq,"tppm")) && (dec.t.a > 0.0)); d.t1 = getval("rd") + getval("ad") + at; d.c2 = d.c2 + (!strcmp(dec.seq,"spinal")); d.c2 = d.c2 + ((!strcmp(dec.seq,"spinal")) && (dec.s.a > 0.0)); d.t2 = getval("rd") + getval("ad") + at; d = update_dutycycle(d); abort_dutycycle(d,10.0); // Set Phase Tables settable(phH90,4,table1); settable(phXhx,4,table2); settable(phHhx,4,table3); settable(ph1Hhxhmqc,4,table4); settable(ph2Hhxhmqc,4,table5); settable(ph3Hhxhmqc,4,table6); settable(ph4Hhxhmqc,4,table7); settable(ph5Hhxhmqc,4,table8); settable(phXhxhmqc,32,table9); settable(ph6Hhxhmqc,4,table10); settable(ph7Hhxhmqc,8,table11); settable(ph8Hhxhmqc,4,table12); settable(ph9Hhxhmqc,4,table13); settable(phRec,16,table14); // Add STATES TPPI (States with FAD) tsadd(ph3Hhxhmqc,2*d2_index,4); tsadd(ph4Hhxhmqc,2*d2_index,4); tsadd(ph5Hhxhmqc,2*d2_index,4); tsadd(ph6Hhxhmqc,2*d2_index,4); tsadd(phRec,2*d2_index,4); if (phase1 == 2) { tsadd(ph3Hhxhmqc,1,4); tsadd(ph4Hhxhmqc,1,4); tsadd(ph5Hhxhmqc,1,4); tsadd(ph6Hhxhmqc,1,4); } setreceiver(phRec); // Begin Sequence txphase(phXhx); decphase(phH90); obspwrf(getval("aXhx")); decpwrf(getval("aH90")); obsunblank(); decunblank(); _unblank34(); delay(d1); sp1on(); delay(2.0e-6); sp1off(); delay(2.0e-6); // H to X Cross Polarization decrgpulse(getval("pwH90"),phH90,0.0,0.0); decphase(phHhx); _cp_(hx,phHhx,phXhx); // Begin hmqcHX with fh (FSLG) Between Pulses obspwrf(aXhxhmqc); _mpseqon(fh,ph1Hhxhmqc); // First "tau" period for J evolution delay(tHXhmqc); _mpseqoff(fh); decpwrf(aHhxhmqc); decrgpulse(pmHhxhmqc, ph2Hhxhmqc, 0.0, 0.0);// Create HX double-quantum coherence decrgpulse(pwHhxhmqc, ph3Hhxhmqc, 0.0, 0.0); decrgpulse(pmHhxhmqc, ph4Hhxhmqc, 0.0, 0.0); _mpseqon(fh,ph5Hhxhmqc); // Begin F1 evolution with FSLG delay(d22); rgpulse(pwXhxhmqc, phXhxhmqc, 0.0,0.0); delay(d22); _mpseqoff(fh); // End F1 evolution with FSLG decpwrf(aHhxhmqc); decrgpulse(pmHhxhmqc, ph6Hhxhmqc, 0.0, 0.0);// Refocus HX double quantum coherence decrgpulse(pwHhxhmqc, ph7Hhxhmqc, 0.0, 0.0); decrgpulse(pmHhxhmqc, ph8Hhxhmqc, 0.0, 0.0); _mpseqon(fh,ph9Hhxhmqc); // Second "tau" period for J evolution delay(tHXhmqc); _mpseqoff(fh); // Begin Acquisition decphase(phHhx); _dseqon(dec); obsblank(); _blank34(); delay(getval("rd")); startacq(getval("ad")); acquire(np, 1/sw); endacq(); _dseqoff(dec); obsunblank(); decunblank(); _unblank34(); }
pulsesequence() { // Define Variables and Objects and Get Parameter Values double aYxy8 = getval("aYxy8"); double pwYxy8 = getval("pwYxy8"); double nYxy8 = getval("nYxy8"); int cycles = (int) nYxy8/2.0; nYxy8 = 2.0*cycles; int counter = (int) (nYxy8 - 1.0); initval((nYxy8 - 1.0),v8); double onYxy8 = getval("onYxy8"); double srate = getval("srate"); DSEQ dec = getdseq("H"); strncpy(dec.t.ch,"dec",3); putCmd("chHtppm='dec'\n"); strncpy(dec.s.ch,"dec",3); putCmd("chHspinal='dec'\n"); DSEQ mix = getdseq("Hmix"); strncpy(mix.t.ch,"dec",3); putCmd("chHmixtppm='mix'\n"); strncpy(mix.s.ch,"dec",3); putCmd("chHmixspinal='mix'\n"); //-------------------------------------- // Copy Current Parameters to Processed //------------------------------------- putCmd("groupcopy('current','processed','acquisition')"); // Dutycycle Protection DUTY d = init_dutycycle(); d.dutyon = getval("pwX90") + 4.0*nYxy8*pwYxy8 + getval("pwX180"); d.dutyoff = d1 + 4.0e-6; d.c1 = d.c1 + (!strcmp(dec.seq,"tppm")); d.c1 = d.c1 + ((!strcmp(dec.seq,"tppm")) && (dec.t.a > 0.0)); d.t1 = getval("rd") + getval("ad") + at; d.c2 = d.c2 + (!strcmp(dec.seq,"spinal")); d.c2 = d.c2 + ((!strcmp(dec.seq,"spinal")) && (dec.s.a > 0.0)); d.t2 = getval("rd") + getval("ad") + at; d.c3 = d.c3 + (!strcmp(mix.seq,"tppm")); d.c3 = d.c3 + ((!strcmp(mix.seq,"tppm")) && (mix.t.a > 0.0)); d.t3 = 2.0*nYxy8*(1.0/srate - 2.0*pwYxy8) + 1.0/srate - getval("pwX180"); d.c4 = d.c4 + (!strcmp(mix.seq,"spinal")); d.c4 = d.c4 + ((!strcmp(mix.seq,"spinal")) && (mix.s.a > 0.0)); d.t4 = 2.0*nYxy8*(1.0/srate - 2.0*pwYxy8) + 1.0/srate - getval("pwX180"); d = update_dutycycle(d); abort_dutycycle(d,10.0); // Set Phase Tables settable(phX90,4,table1); settable(ph1Yxy8,8,table2); settable(ph2Yxy8,4,table3); settable(phX180,4,table4); settable(phRec,4,table5); if (counter < 0) tsadd(phRec,2,4); setreceiver(phRec); // Begin Sequence txphase(phX90); decphase(zero); obspwrf(getval("aX90")); obsunblank(); decunblank(); _unblank34(); delay(d1); sp1on(); delay(2.0e-6); sp1off(); delay(2.0e-6); // X Single Pulse rgpulse(getval("pwX90"),phX90,0.0,0.0); // xy8Y Period One obspwrf(getval("aX180")); txphase(phX180); if (counter >= 0) { _dseqon(mix); delay(pwYxy8/2.0); dec2pwrf(aYxy8); sub(v1,v1,v1); if (counter >= 1) { if (counter > 1) loop(v8,v9); getelem(ph1Yxy8,v1,v4); incr(v1); getelem(ph2Yxy8,ct,v2); add(v4,v2,v2); dec2phase(v2); delay(0.5/srate - pwYxy8); if (onYxy8 == 2) dec2rgpulse(pwYxy8,v2,0.0,0.0); else delay(pwYxy8); if (counter > 1) endloop(v9); } // X Refocussing Pulse delay(0.5/srate - pwYxy8/2.0 - getval("pwX180")/2.0); rgpulse(getval("pwX180"),phX180,0.0,0.0); dec2pwrf(aYxy8); delay(0.5/srate - pwYxy8/2.0 - getval("pwX180")/2.0); // xy8Y Period Two if (counter >= 1) { if (counter > 1) loop(v8,v9); if (onYxy8 == 2) dec2rgpulse(pwYxy8,v2,0.0,0.0); else delay(pwYxy8); getelem(ph1Yxy8,v1,v4); incr(v1); getelem(ph2Yxy8,ct,v2); add(v4,v2,v2); dec2phase(v2); delay(0.5/srate - pwYxy8); if (counter > 1) endloop(v9); } delay(pwYxy8/2.0); _dseqoff(mix); } // Begin Acquisition _dseqon(dec); obsblank(); _blank34(); delay(getval("rd")); startacq(getval("ad")); acquire(np, 1/sw); endacq(); _dseqoff(dec); obsunblank(); decunblank(); _unblank34(); }
void pulsesequence() { // Set the Maximum Dynamic Table Number settablenumber(10); setvvarnumber(30); // Define Variables and Objects and Get Parameter Values CP hx = getcp("HX",0.0,0.0,0,1); strncpy(hx.fr,"dec",3); strncpy(hx.to,"obs",3); putCmd("frHX='dec'\n"); putCmd("toHX='obs'\n"); WMPA toss = gettoss5("tossX"); strncpy(toss.ch,"obs",3); putCmd("chXtoss='obs'\n"); DSEQ dec = getdseq("H"); strncpy(dec.t.ch,"dec",3); putCmd("chHtppm='dec'\n"); strncpy(dec.s.ch,"dec",3); putCmd("chHspinal='dec'\n"); //-------------------------------------- // Copy Current Parameters to Processed //------------------------------------- putCmd("groupcopy('current','processed','acquisition')"); // Dutycycle Protection DUTY d = init_dutycycle(); d.dutyon = getval("pwH90") + getval("tHX") + 5.0*toss.pw; d.dutyoff = d1 + 4.0e-6; d.c1 = d.c1 + (!strcmp(dec.seq,"tppm")); d.c1 = d.c1 + ((!strcmp(dec.seq,"tppm")) && (dec.t.a > 0.0)); d.t1 = toss.rtau - 5.0*toss.pw + getval("rd") + getval("ad") + at; d.c2 = d.c2 + (!strcmp(dec.seq,"spinal")); d.c2 = d.c2 + ((!strcmp(dec.seq,"spinal")) && (dec.s.a > 0.0)); d.t2 = toss.rtau - 5.0*toss.pw + getval("rd") + getval("ad") + at; d = update_dutycycle(d); abort_dutycycle(d,10.0); // Set Phase Tables settable(phH90,22,table1); settable(phfXhx,11,table2); settable(phXhx,44,table3); settable(phHhx,4,table4); settable(phHdec,4,table5); settable(phXtoss,44,table6); settable(phRec,44,table7); setreceiver(phRec); obsstepsize(360.0/(PSD*8192)); // Begin Sequence xmtrphase(phfXhx); txphase(phXhx); decphase(phH90); obspwrf(getval("aXhx")); decpwrf(getval("aH90")); obsunblank(); decunblank(); _unblank34(); delay(d1); sp1on(); delay(2.0e-6); sp1off(); delay(2.0e-6); // H to X Cross Polarization - Shifted by -6COG11 decrgpulse(getval("pwH90"),phH90,0.0,0.0); decphase(phHhx); _cp_(hx,phHhx,phXhx); decphase(phHdec); // TOSS5 Sideband Suppression with included // (-6,-5,-6,-5,-6)COG11 Cycle _dseqon(dec); _toss5(toss, phXtoss); // Begin Acquisition with Quadrature Phase obsblank(); _blank34(); delay(getval("rd")); startacq(getval("ad")); acquire(np, 1/sw); endacq(); _dseqoff(dec); obsunblank(); decunblank(); _unblank34(); }
void pulsesequence() { // // Set the Maximum Dynamic Table Number // settablenumber(10); setvvarnumber(30); //Define Variables and Objects and Get Parameter Values CP hx = getcp("HX",0.0,0.0,0,1); strncpy(hx.fr,"dec",3); strncpy(hx.to,"obs",3); putCmd("frHX='dec'\n"); putCmd("toHX='obs'\n"); WMPA cpmg = getcpmg("cpmgX"); strncpy(cpmg.ch,"obs",3); putCmd("chXcpmg='obs'\n"); double aXecho = getval("aXecho"); // define the echoX group in the sequence double t1Xechoinit = getval("t1Xecho"); double pwXecho = getval("pwXecho"); double t2Xechoinit = getval("t2Xecho"); double t1Xecho = t1Xechoinit - pwXecho/2.0 - getval("pwX90")/2.0; if (t1Xecho < 0.0) t1Xecho = 0.0; double t2Xecho = t2Xechoinit - pwXecho/2.0 - cpmg.r1 - cpmg.t2 - getval("ad"); if (t2Xecho < 0.0) t2Xecho = 0.0; DSEQ dec = getdseq("H"); strncpy(dec.t.ch,"dec",3); putCmd("chHtppm='dec'\n"); strncpy(dec.s.ch,"dec",3); putCmd("chHspinal='dec'\n"); //-------------------------------------- // Copy Current Parameters to Processed //------------------------------------- putCmd("groupcopy('current','processed','acquisition')"); // Dutycycle Protection DUTY d = init_dutycycle(); d.dutyon = getval("pwH90") + getval("tHX") + pwXecho + (cpmg.cycles - 1)*cpmg.pw; d.dutyoff = d1 + 4.0e-6; d.c1 = d.c1 + (!strcmp(dec.seq,"tppm")); d.c1 = d.c1 + ((!strcmp(dec.seq,"tppm")) && (dec.t.a > 0.0)); d.t1 = t1Xecho + t2Xecho + getval("rd") + getval("ad") + at - (cpmg.cycles - 1)*cpmg.pw; d.c2 = d.c2 + (!strcmp(dec.seq,"spinal")); d.c2 = d.c2 + ((!strcmp(dec.seq,"spinal")) && (dec.s.a > 0.0)); d.t2 = t1Xecho + t2Xecho + getval("rd") + getval("ad") + at - (cpmg.cycles - 1)*cpmg.pw; d = update_dutycycle(d); abort_dutycycle(d,10.0); // Set Phase Tables settable(phH90,64,table1); settable(phXhx,64,table2); settable(phHhx,64,table3); settable(phXecho,64,table4); settable(phXcpmg,64,table5); settable(phRec,64,table6); setreceiver(phRec); // Begin Sequence txphase(phXhx); decphase(phH90); obspwrf(getval("aXhx")); decpwrf(getval("aH90")); obsunblank(); decunblank(); _unblank34(); delay(d1); sp1on(); delay(2.0e-6); sp1off(); delay(2.0e-6); // H to X Cross Polarization decrgpulse(getval("pwH90"),phH90,0.0,0.0); decphase(phHhx); _cp_(hx,phHhx,phXhx); // H Decoupling On decphase(zero); _dseqon(dec); // X Hahn Echo txphase(phXecho); obspwrf(aXecho); delay(t1Xecho); rgpulse(pwXecho,phXecho,0.0,0.0); delay(t2Xecho); // Apply CPMG Cycles obsblank(); _blank34(); delay(cpmg.r1); startacq(getval("ad")); _cpmg(cpmg,phXcpmg); endacq(); _dseqoff(dec); obsunblank(); decunblank(); _unblank34(); }
pulsesequence() { // Set the Maximum Dynamic Table and v-var Numbers settablenumber(10); setvvarnumber(30); // Define Variables and Objects and Get Parameter Values double aXprep1 = getval("aXprep1"); // Define Tilted Pulses using "prep1X". double pw1Xprep1 = getval("pw1Xprep1"); double pw2Xprep1 = getval("pw2Xprep1"); double phXprep1 = getval("phXprep1"); WMPA wpmlg = getwpmlg("wpmlgX"); strncpy(wpmlg.ch,"obs",3); putCmd("chXwpmlg='obs'\n"); //-------------------------------------- // Copy Current Parameters to Processed //------------------------------------- putCmd("groupcopy('current','processed','acquisition')"); // Dutycycle Protection DUTY d = init_dutycycle(); d.dutyon = getval("pw1Xprep1") + getval("pw2Xprep1") + 2.0*wpmlg.q*wpmlg.cycles*wpmlg.pw; d.dutyoff = d1 + 4.0e-6 + 5.0e-6 + wpmlg.r1 + wpmlg.r2 + at - 2.0*wpmlg.q*wpmlg.cycles*wpmlg.pw; d = update_dutycycle(d); abort_dutycycle(d,10.0); // Set Phase Tables settable(ph1Xprep1,4,table1); settable(ph2Xprep1,4,table2); settable(phXwpmlg,4,table3); settable(phRec,4,table4); setreceiver(phRec); // Set the Small-Angle Step double obsstep = 360.0/(PSD*8192); obsstepsize(obsstep); int phfXprep1 = initphase(phXprep1, obsstep); int phXzero = initphase(0.0, obsstep); // Begin Sequence xmtrphase(phfXprep1); txphase(ph1Xprep1); obspwrf(aXprep1); obsunblank(); decunblank(); _unblank34(); delay(d1); sp1on(); delay(2.0e-6); sp1off(); delay(2.0e-6); // Tilted Preparation Pulse for FSLG or PMLG "prep1X" startacq(5.0e-6); rcvroff(); delay(wpmlg.r1); rgpulse(pw1Xprep1, ph1Xprep1, 0.0, 0.0); rgpulse(pw2Xprep1, ph2Xprep1, 0.0, 0.0); xmtrphase(phXzero); delay(wpmlg.r2); // Apply WPMLG Cycles decblank(); _blank34(); _wpmlg(wpmlg, phXwpmlg); endacq(); obsunblank(); decunblank(); _unblank34(); }
pulsesequence() { // Define Variables and Objects and Get Parameter Values PBOXPULSE shp1 = getpboxpulse("sft1A",0,1); PBOXPULSE shp2 = getpboxpulse("sft2A",0,1); PBOXPULSE shp3 = getpboxpulse("sft3A",0,1); DSEQ dec = getdseq("H"); strncpy(dec.t.ch,"dec",3); putCmd("chHtppm='dec'\n"); strncpy(dec.s.ch,"dec",3); putCmd("chHspinal='dec'\n"); //-------------------------------------- // Copy Current Parameters to Processed //------------------------------------- putCmd("groupcopy('current','processed','acquisition')"); // Dutycycle Protection DUTY d = init_dutycycle(); d.dutyon = getval("pwX90") + shp1.pw + shp2.pw + shp3.pw; d.dutyoff = d1 + 4.0e-6; d.c1 = d.c1 + (!strcmp(dec.seq,"tppm")); d.c1 = d.c1 + ((!strcmp(dec.seq,"tppm")) && (dec.t.a > 0.0)); d.t1 = getval("rd") + getval("ad") + at; d.c2 = d.c2 + (!strcmp(dec.seq,"spinal")); d.c2 = d.c2 + ((!strcmp(dec.seq,"spinal")) && (dec.s.a > 0.0)); d.t2 = getval("rd") + getval("ad") + at; d = update_dutycycle(d); abort_dutycycle(d,10.0); // Set Phase Tables settable(phX90,4,table1); settable(phAsft1,4,table2); settable(phAsft2,4,table3); settable(phAsft3,4,table4); settable(phRec,4,table5); setreceiver(phRec); // Begin Sequence txphase(phX90); decphase(zero); obspwrf(getval("aX90")); obsunblank(); decunblank(); _unblank34(); delay(d1); sp1on(); delay(2.0e-6); sp1off(); delay(2.0e-6); // X Direct Polarization rgpulse(getval("pwX90"),phX90,0.0,0.0); delay(20.0e-6); // X Shaped Pulse _pboxpulse(shp1, phAsft1); delay(20.0e-6); // X Simultaneous Shaped Pulse _pboxsimpulse(shp1,shp2,phAsft1,phAsft2); delay(20.0e-6); // X 3-channel Simultaneous Shaped Pulse delay(20.0e-6); _pboxsim3pulse(shp1,shp2,shp3,phAsft1,phAsft2,phAsft3); // Begin Acquisition _dseqon(dec); obsblank(); _blank34(); delay(getval("rd")); startacq(getval("ad")); acquire(np, 1/sw); endacq(); _dseqoff(dec); obsunblank(); decunblank(); _unblank34(); }
pulsesequence() { // Define Variables and Objects and Get Parameter Values double pw1Xstmas = getval("pw1Xstmas"); double pw2Xstmas = getval("pw2Xstmas"); double tXzfselinit = getval("tXzfsel"); double tXzfsel = tXzfselinit - 3.0e-6; if (tXzfsel < 0.0) tXzfsel = 0.0; double d2init = getval("d2"); double d2 = d2init - pw1Xstmas/2.0 - pw2Xstmas/2.0; if (d2 < 0.0) d2 = 0.0; DSEQ dec = getdseq("H"); strncpy(dec.t.ch,"dec",3); putCmd("chHtppm='dec'\n"); strncpy(dec.s.ch,"dec",3); putCmd("chHspinal='dec'\n"); // Set Constant-time Period for d2. if (d2_index == 0) d2_init = getval("d2"); double d2_ = (ni - 1)/sw1 + d2_init; putCmd("d2acqret = %f\n",roundoff(d2_,12.5e-9)); putCmd("d2dwret = %f\n",roundoff(1.0/sw1,12.5e-9)); //-------------------------------------- // Copy Current Parameters to Processed //------------------------------------- putCmd("groupcopy('current','processed','acquisition')"); // Dutycycle Protection DUTY d = init_dutycycle(); d.dutyon = getval("pw1Xstmas") + getval("pw2Xstmas") + getval("pwXzfsel"); d.dutyoff = d1 + 4.0e-6; d.c1 = d.c1 + (!strcmp(dec.seq,"tppm")); d.c1 = d.c1 + ((!strcmp(dec.seq,"tppm")) && (dec.t.a > 0.0)); d.t1 = d2_ + tXzfsel + getval("rd") + getval("ad") + at; d.c2 = d.c2 + (!strcmp(dec.seq,"spinal")); d.c2 = d.c2 + ((!strcmp(dec.seq,"spinal")) && (dec.s.a > 0.0)); d.t2 = d2_ + tXzfsel + getval("rd") + getval("ad") + at; d = update_dutycycle(d); abort_dutycycle(d,10.0); // Set Phase Tables settable(ph1Xstmas,4,table1); settable(ph2Xstmas,4,table2); settable(phXzfsel,8,table3); settable(phRec,8,table4); if (phase1 == 2) { tsadd(ph1Xstmas,1,4); } setreceiver(phRec); // Begin Sequence txphase(ph1Xstmas); decphase(zero); obspower(getval("tpwr")); obspwrf(getval("aXstmas")); obsunblank(); decunblank(); _unblank34(); delay(d1); sp1on(); delay(2.0e-6); sp1off(); delay(2.0e-6); // H Decoupler on Before STMAS _dseqon(dec); // Two-Pulse STMAS rgpulse(getval("pw1Xstmas"),ph1Xstmas,0.0,0.0); txphase(ph2Xstmas); delay(d2); rgpulse(getval("pw2Xstmas"),ph2Xstmas,0.0,0.0); // Z-filter Pulse txphase(phXzfsel); obsblank(); obspower(getval("dbXzfsel")); obspwrf(getval("aXzfsel")); delay(3.0e-6); obsunblank(); delay(tXzfsel); rgpulse(getval("pwXzfsel"),phXzfsel,0.0,0.0); // Begin Acquisition obsblank(); _blank34(); delay(getval("rd")); startacq(getval("ad")); acquire(np, 1/sw); endacq(); _dseqoff(dec); obsunblank(); decunblank(); _unblank34(); }
pulsesequence() { // Define Variables and Objects and Get Parameter Values double aXfam2 = getval("aXfam2"); double pw1Xfam2 = getval("pw1Xfam2"); double pw2Xfam2 = getval("pw2Xfam2"); double pw3Xfam2 = getval("pw3Xfam2"); double pw4Xfam2 = getval("pw4Xfam2"); double nXfam2 = getval("nXfam2"); initval(nXfam2,v4); putCmd("pw2Xmqmas=pwXfam1"); // Sequence uses pwXfam1 and sets pw2Xmqmas double d2init = getval("d2"); // Define the Split d2 in the Pulse Sequence double ival = getval("ival"); double d20 = 1.0; double d21 = 0.0; double d22 = 0.0; if (ival == 1.5) { d20 = 9.0*d2init/16.0; d21 = 7.0*d2init/16.0; d22 = 0.0; } else if (ival == 2.5) { d20 = 12.0*d2init/31.0; d21 = 0.0*d2init/31.0; d22 = 19.0*d2init/31.0; } else { d20 = 1.0*d2init; d21 = 0.0*d2init; d22 = 0.0*d2init; } double tXechselinit = getval("tXechsel"); // Adjust the selective echo delay for the double tXechsel = tXechselinit - 3.0e-6; // attenuator switch time. if (tXechsel < 0.0) tXechsel = 0.0; DSEQ dec = getdseq("H"); strncpy(dec.t.ch,"dec",3); putCmd("chHtppm='dec'\n"); strncpy(dec.s.ch,"dec",3); putCmd("chHspinal='dec'\n"); // Set Constant-time Period for d2. if (d2_index == 0) d2_init = getval("d2"); double d2_ = (ni - 1)/sw1 + d2_init; putCmd("d2acqret = %f\n",roundoff(d2_,12.5e-9)); putCmd("d2dwret = %f\n",roundoff(1.0/sw1,12.5e-9)); //-------------------------------------- // Copy Current Parameters to Processed //------------------------------------- putCmd("groupcopy('current','processed','acquisition')"); // Dutycycle Protection DUTY d = init_dutycycle(); d.dutyon = getval("pw1Xmqmas") + nXfam2*(pw1Xfam2 + pw2Xfam2 + pw3Xfam2 +pw4Xfam2) + getval("pwXechsel"); d.dutyoff = d1 + 4.0e-6; d.c1 = d.c1 + (!strcmp(dec.seq,"tppm")); d.c1 = d.c1 + ((!strcmp(dec.seq,"tppm")) && (dec.t.a > 0.0)); d.t1 = d2_ + tXechselinit + getval("rd") + getval("ad") + at; d.c2 = d.c2 + (!strcmp(dec.seq,"spinal")); d.c2 = d.c2 + ((!strcmp(dec.seq,"spinal")) && (dec.s.a > 0.0)); d.t2 = d2_ + tXechselinit + getval("rd") + getval("ad") + at; d = update_dutycycle(d); abort_dutycycle(d,10.0); // Set Phase Tables if (phase1 == 0) { settable(phf1Xmqmas,12,table1); settable(ph1Xfam2,6,table2); settable(ph2Xfam2,6,table3); settable(phfXechsel,96,table4); settable(phRec,48,table5); } else { settable(phf1Xmqmas,6,table6); settable(ph1Xfam2,6,table7); settable(ph2Xfam2,6,table8); settable(phfXechsel,48,table9); settable(phRec,24,table10); if (phase1 == 2) { tsadd(phf1Xmqmas,30,360); } } setreceiver(phRec); obsstepsize(1.0); // Begin Sequence xmtrphase(phf1Xmqmas); decphase(zero); obspower(getval("tpwr")); obspwrf(getval("aXmqmas")); obsunblank(); decunblank(); _unblank34(); delay(d1); sp1on(); delay(2.0e-6); sp1off(); delay(2.0e-6); // H Decoupler on Before MQMAS _dseqon(dec); // Two-Pulse MQMAS with DFS Conversion rgpulse(getval("pw1Xmqmas"),zero,0.0,0.0); xmtrphase(zero); txphase(ph1Xfam2); obspwrf(aXfam2); delay(d20); // X FAM2 Pulse loop(v4,v5); xmtron(); delay(pw1Xfam2); xmtroff(); txphase(ph2Xfam2); delay(pw2Xfam2); xmtron(); delay(pw3Xfam2); xmtroff(); txphase(ph2Xfam2); delay(pw4Xfam2); endloop(v5); // Tau Delay and Second Selective Echo Pulse xmtrphase(phfXechsel); obsblank(); obspower(getval("dbXechsel")); obspwrf(getval("aXechsel")); delay(3.0e-6); obsunblank(); delay(d21 + tXechsel); rgpulse(getval("pwXechsel"),zero,0.0,0.0); delay(d22); // Begin Acquisition obsblank(); _blank34(); delay(getval("rd")); startacq(getval("ad")); acquire(np, 1/sw); endacq(); _dseqoff(dec); obsunblank(); decunblank(); _unblank34(); }
void pulsesequence() { // Define Variables and Objects and Get Parameter Values double aXhxpto2 = getval("aXhxpto2"); double pw1Xhxpto2 = getval("pw1Xhxpto2"); double pw2Xhxpto2 = getval("pw2Xhxpto2"); double t1HXpto2init = getval("t1HXpto2"); double tau1 = t1HXpto2init - pw1Xhxpto2/2.0; double t2HXpto2init = getval("t2HXpto2"); double tau2 = t2HXpto2init - pw1Xhxpto2/2.0 - pw2Xhxpto2/2.0; double t3HXpto2init = getval("t3HXpto2"); double tau3 = t3HXpto2init - pw2Xhxpto2/2.0; MPSEQ r18 = getr1825("r18H",0,0.0,0.0,0,1); MPSEQ r18ref = getr1825("r18H",r18.iSuper,r18.phAccum,r18.phInt,1,1); strncpy(r18.ch,"dec",3); strncpy(r18ref.ch,"dec",3); putCmd("chHr18='dec'\n"); DSEQ dec = getdseq("H"); strncpy(dec.t.ch,"dec",3); putCmd("chHtppm='dec'\n"); strncpy(dec.s.ch,"dec",3); putCmd("chHspinal='dec'\n"); //-------------------------------------- // Copy Current Parameters to Processed //------------------------------------- putCmd("groupcopy('current','processed','acquisition')"); // Dutycycle Protection DUTY d = init_dutycycle(); d.dutyon = tau1 + tau2 + pw1Xhxpto2 + tau3 + pw2Xhxpto2; d.dutyoff = d1 + 4.0e-6; d.c1 = d.c1 + (!strcmp(dec.seq,"tppm")); d.c1 = d.c1 + ((!strcmp(dec.seq,"tppm")) && (dec.t.a > 0.0)); d.t1 = getval("rd") + getval("ad") + at; d.c2 = d.c2 + (!strcmp(dec.seq,"spinal")); d.c2 = d.c2 + ((!strcmp(dec.seq,"spinal")) && (dec.s.a > 0.0)); d.t2 = getval("rd") + getval("ad") + at; d = update_dutycycle(d); abort_dutycycle(d,10.0); // Set Phase Tables settable(ph1Hhxpto2,4,table1); settable(ph2Hhxpto2,4,table2); settable(ph1Xhxpto2,4,table3); settable(ph2Xhxpto2,4,table4); settable(phHdec,4,table5); settable(phRec,4,table6); setreceiver(phRec); // Begin Sequence txphase(ph1Xhxpto2); decphase(ph1Hhxpto2); obspwrf(aXhxpto2); decpwrf(r18.a); obsunblank(); decunblank(); _unblank34(); delay(d1); sp1on(); delay(2.0e-6); sp1off(); delay(2.0e-6); // H to X Cross Polarization with PRESTO1 _mpseqon(r18,ph1Hhxpto2); delay(tau1); rgpulse(pw1Xhxpto2/2.0,ph1Xhxpto2,0.0,0.0); _mpseqoff(r18); _mpseqon(r18ref,ph2Hhxpto2); rgpulse(pw1Xhxpto2/2.0,ph1Xhxpto2,0.0,0.0); delay(tau2); _mpseqoff(r18ref); decphase(zero); _dseqon(dec); rgpulse(pw2Xhxpto2,ph2Xhxpto2,0.0,0.0); delay(tau3); decphase(zero); // Begin Acquisition _dseqon(dec); obsblank(); _blank34(); delay(getval("rd")); startacq(getval("ad")); acquire(np, 1/sw); endacq(); _dseqoff(dec); obsunblank(); decunblank(); _unblank34(); }
pulsesequence() { // Define Variables and Objects and Get Parameter Values CP hy = getcp("HY",0.0,0.0,0,1); strncpy(hy.fr,"dec",3); strncpy(hy.to,"dec2",4); putCmd("frHY='dec'\n"); putCmd("toHY='dec2'\n"); GP inept = getinept("ineptYX"); strncpy(inept.ch1,"dec2",4); strncpy(inept.ch2,"obs",3); putCmd("ch1YXinept='dec2'\n"); putCmd("ch2YXinept='obs'\n"); DSEQ dec = getdseq("H"); strncpy(dec.t.ch,"dec",3); putCmd("chHtppm='dec'\n"); strncpy(dec.s.ch,"dec",3); putCmd("chHspinal='dec'\n"); DSEQ mix = getdseq("Hmix"); strncpy(mix.t.ch,"dec",3); putCmd("chHmixtppm='dec'\n"); strncpy(mix.s.ch,"dec",3); putCmd("chHmixspinal='dec'\n"); // Dutycycle Protection double simpw1 = inept.pw1; if (inept.pw2 > inept.pw1) simpw1 = inept.pw2; double simpw2 = inept.pw3; if (inept.pw4 > inept.pw3) simpw2 = inept.pw4; DUTY d = init_dutycycle(); d.dutyon = getval("pwH90") + getval("tHY") + 2.0*simpw1 + 2.0*simpw2; d.dutyoff = d1 + 4.0e-6; d.c1 = d.c1 + (!strcmp(dec.seq,"tppm")); d.c1 = d.c1 + ((!strcmp(dec.seq,"tppm")) && (dec.t.a > 0.0)); d.t1 = inept.t1 + inept.t2 + inept.t3 + inept.t4 + getval("rd") + getval("ad") + at; d.c2 = d.c2 + (!strcmp(dec.seq,"spinal")); d.c2 = d.c2 + ((!strcmp(dec.seq,"spinal")) && (dec.s.a > 0.0)); d.t2 = inept.t1 + inept.t2 + inept.t3 + inept.t4 + getval("rd") + getval("ad") + at; d = update_dutycycle(d); abort_dutycycle(d,10.0); // Set Phase Tables settable(phH90,16,table1); settable(phHhy,4,table2); settable(phYhy,4,table3); settable(ph1Yyxinept,4,table4); settable(ph1Xyxinept,4,table5); settable(ph2Yyxinept,4,table6); settable(ph2Xyxinept,16,table7); settable(ph3Yyxinept,8,table8); settable(ph3Xyxinept,4,table9); settable(phRec,8,table10); setreceiver(phRec); // Begin Sequence txphase(ph1Xyxinept); decphase(phH90); dec2phase(phYhy); obspwrf(getval("aXyxinept")); decpwrf(getval("aH90")); dec2pwrf(getval("aYhy")); obsunblank(); decunblank(); _unblank34(); delay(d1); sp1on(); delay(2.0e-6); sp1off(); delay(2.0e-6); // H to Y Cross Polarization decrgpulse(getval("pwH90"),phH90,0.0,0.0); decphase(phHhy); _cp_(hy,phHhy,phYhy); decphase(zero); // INEPT Transfer from Y to X _dseqon(mix); _ineptref(inept,ph1Yyxinept,ph1Xyxinept,ph2Yyxinept,ph2Xyxinept,ph3Yyxinept,ph3Xyxinept); _dseqoff(mix); // Begin Acquisition _dseqon(dec); obsblank(); _blank34(); delay(getval("rd")); startacq(getval("ad")); acquire(np, 1/sw); endacq(); _dseqoff(dec); obsunblank(); decunblank(); _unblank34(); }
void pulsesequence() { // Set the Maximum Dynamic Table Number settablenumber(10); setvvarnumber(30); // Define Variables and Objects and Get Parameter Values WMPA xx = getxx("xxX"); strncpy(xx.ch,"obs",3); putCmd("chXxx='obs'\n"); //-------------------------------------- // Copy Current Parameters to Processed //------------------------------------- putCmd("groupcopy('current','processed','acquisition')"); // Dutycycle Protection DUTY d = init_dutycycle(); d.dutyon = getval("pwXprep") + 2.0*xx.cycles*xx.pw; d.dutyoff = d1 + 4.0e-6 + 5.0e-6 + xx.r1 + xx.r2 + at - 2.0*xx.cycles*xx.pw; d = update_dutycycle(d); abort_dutycycle(d,10.0); // Set Phase Tables settable(phXprep,4,table1); settable(phXxx,4,table2); settable(phRec,4,table3); setreceiver(phRec); // Set the Small-Angle Prep Phase double obsstep = 360.0/(PSD*8192); obsstepsize(obsstep); int phfXprep = initphase(getval("phXprep"), obsstep); int phXzero = initphase(0.0, obsstep); // Begin Sequence xmtrphase(phfXprep); txphase(phXprep); obspwrf(getval("aXprep")); obsunblank(); decunblank(); _unblank34(); delay(d1); sp1on(); delay(2.0e-6); sp1off(); delay(2.0e-6); // Preparation Pulse with Initial Point startacq(5.0e-6); rcvroff(); delay(xx.r1); rgpulse(getval("pwXprep"), phXprep, 0.0, 0.0); xmtrphase(phXzero); // Apply Semi-windowless WHH4 Cycles decblank(); _blank34(); _xx(xx, phXxx); endacq(); obsunblank(); decunblank(); _unblank34(); }