void pulsesequence() { char shname1[MAXSTR], f1180[MAXSTR], f2180[MAXSTR], n15_flg[MAXSTR]; int icosel, t1_counter, t2_counter, ni2 = getval("ni2"), phase; double d2_init=0.0, d3_init=0.0, pwS1,pwS2,pwS3,pwS4,pwS5,pwS6, kappa, lambda = getval("lambda"), gzlvl1 = getval("gzlvl1"), gzlvl2 = getval("gzlvl2"), gzlvl3 = getval("gzlvl3"), gzlvl4 = getval("gzlvl4"), gzlvl5 = getval("gzlvl5"), gzlvl6 = getval("gzlvl6"), gt1 = getval("gt1"), gt3 = getval("gt3"), gt4 = getval("gt4"), gt5 = getval("gt5"), gt6 = getval("gt6"), gstab = getval("gstab"), scale = getval("scale"), sw1 = getval("sw1"), tpwrsf = getval("tpwrsf"), shlvl1, shpw1 = getval("shpw1"), pwClvl = getval("pwClvl"), pwNlvl = getval("pwNlvl"), pwN = getval("pwN"), dpwr2 = getval("dpwr2"), d2 = getval("d2"), t2a,t2b,halfT2, shbw = getval("shbw"), shofs = getval("shofs")-4.77, timeTN = getval("timeTN"), tau1 = getval("tau1"), tau2 = getval("tau2"), taunh = getval("taunh"); getstr("shname1", shname1); getstr("n15_flg",n15_flg); phase = (int) (getval("phase") + 0.5); settable(t1,4,phi1); settable(t2,4,phi2); settable(t3,1,phi3); settable(t5,1,phi5); settable(t14,4,phi14); settable(t15,4,phi15); settable(t24,4,phi24); settable(t25,4,phi25); /* INITIALIZE VARIABLES */ kappa = 5.4e-3; //shpw1 = pw*8.0; shlvl1 = tpwr; f1180[0] ='n'; f2180[0] ='n'; pwS1 = c13pulsepw("co", "ca", "sinc", 90.0); pwS2 = c13pulsepw("co", "ca", "sinc", 180.0); pwS3 = c13pulsepw("ca", "co", "square", 180.0); pwS4 = h_shapedpw("eburp2",shbw,shofs,zero, 0.0, 0.0); pwS6 = h_shapedpw("reburp",shbw,shofs,zero, 0.0, 0.0); pwS5 = h_shapedpw("pc9f",shbw,shofs,zero, 2.0e-6, 0.0); if(ix==1) printf("pwS2 %g pwS3 %g GRADIENT_DELAY %g POWER_DELAY %g PWRF_DELAY %g\n", pwS2,pwS3,2*GRADIENT_DELAY,4*POWER_DELAY,4*PWRF_DELAY); if (phase == 1) ; if (phase == 2) tsadd(t1,1,4); if ( phase2 == 2 ) { tsadd ( t3,2,4 ); tsadd ( t5,2,4 ); icosel = +1; } else icosel = -1; /* Set up f1180 */ tau1 = d2; if((f1180[A] == 'y') && (ni > 1.0)) { tau1 += ( 1.0 / (2.0*sw1) ); if(tau1 < 0.2e-6) tau1 = 0.0; } tau1 = tau1; /* Set up f2180 */ tau2 = d3; if((f2180[A] == 'y') && (ni2 > 1.0)) { tau2 += ( 1.0 / (2.0*sw2) ); if(tau2 < 0.2e-6) tau2 = 0.0; } tau2 = tau2; /************************************************************/ /* modification for phase-cycling in consecutive experiments*/ /* for kinetic measurements */ /************************************************************/ if( ix == 1) d2_init = d2; t1_counter = (int) ( (d2-d2_init)*sw1 + 0.5 ); if(t1_counter % 2) { tsadd(t1,2,4); tsadd(t14,2,4); tsadd(t15,2,4);tsadd(t24,2,4); tsadd(t25,2,4); } if( ix == 1) d3_init = d3; t2_counter = (int) ( (d3-d3_init)*sw2 + 0.5 ); if(t2_counter % 2) { tsadd(t2,2,4); tsadd(t14,2,4); tsadd(t15,2,4);tsadd(t24,2,4); tsadd(t25,2,4); } /* Set up CONSTANT/SEMI-CONSTANT time evolution in N15 */ if (ni2 > 1) { halfT2 = 0.5*(ni2-1)/sw2; t2b = (double) t2_counter*((halfT2 - timeTN)/((double)(ni2-1))); if( ix==1 && halfT2 - timeTN > 0 ) printf("SCT mode on, max ni2=%g\n",timeTN*sw2*2+1); if(t2b < 0.0) t2b = 0.0; t2a = timeTN - tau2*0.5 + t2b; if(t2a < 0.2e-6) t2a = 0.0; } else { t2b = 0.0; t2a = timeTN - tau2*0.5; } status(A); rcvroff(); decpower(pwClvl); decoffset(dof); dec2power(pwNlvl); dec2offset(dof2); obspwrf(tpwrsf); decpwrf(4095.0); obsoffset(tof); set_c13offset("co"); dec2rgpulse(pwN*2.0,zero,0.0,0.0); zgradpulse(1.5*gzlvl4, gt4); delay(1.0e-4); lk_sample(); delay(d1-gt4); lk_hold(); h_shapedpulse("pc9f",shbw,shofs,zero, 2.0e-6, 0.0); delay(lambda-pwS5*0.5-pwS6*0.5); h_sim3shapedpulse("reburp",shbw,shofs,0.0,2.0*pwN, one, zero, zero, 0.0, 0.0); delay(lambda-pwS5*0.5-pwS6*0.5); if(n15_flg[0]=='y') h_shapedpulse("pc9f_",shbw,shofs,three, 0.0, 0.0); else h_shapedpulse("pc9f_",shbw,shofs,one, 0.0, 0.0); obspower(shlvl1); /**************************************************************************/ dec2rgpulse(pwN,zero,0.0,0.0); zgradpulse(gzlvl4, gt4); delay(timeTN-pwS2*0.5-gt4); sim3_c13pulse("", "co", "ca", "sinc", "", 0.0, 180.0, 2.0*pwN, zero, zero, zero, 2.0e-6, 2.0e-6); zgradpulse(gzlvl4, gt4); delay(timeTN-pwS2*0.5-gt4); dec2rgpulse(pwN,one,0.0,0.0); /**************************************************************************/ /* xxxxxxxxxxxxxxxxxxxxxx 13CO EVOLUTION xxxxxxxxxxxxxxxxxx */ obspower(tpwr); c13pulse("co", "ca", "sinc", 90.0, t1, 2.0e-6, 0.0); delay(tau1*0.5); sim3_c13pulse("", "ca", "co", "square", "", 0.0, 180.0, 2.0*pwN, zero, zero, zero, 2.0e-6, 0.0); delay(tau1*0.5); c13pulse("co", "ca", "sinc", 180.0, zero, 2.0e-6, 0.0); sim3_c13pulse("", "ca", "co", "square", "", 0.0, 180.0, 0.0, one, zero, zero, 2.0e-6, 0.0); if (pwN*2.0 > pwS3) delay(pwN*2.0-pwS3); c13pulse("co", "ca", "sinc", 90.0, zero, 2.0e-6, 0.0); /**************************************************************************/ dec2rgpulse(pwN,t2,0.0,0.0); delay(tau2*0.5); c13pulse("ca", "co", "square", 180.0, zero, 0.0, 0.0); // delay(timeTN-pwS3-pwS2-gt1-1.0e-4); delay(timeTN-pwS3-pwS2-gt1-1.0e-4-2.0*GRADIENT_DELAY-4*POWER_DELAY-4*PWRF_DELAY-(4/PI)*pwN); zgradpulse(-gzlvl1, gt1); delay(1.0e-4); c13pulse("co", "ca", "sinc", 180.0, zero, 0.0, 0.0); delay (t2b); dec2rgpulse (2.0*pwN, zero, 0.0, 0.0); delay (t2a); /**************************************************************************/ delay(gt1/10.0+1.0e-4); h_shapedpulse("eburp2_",shbw,shofs,t3, 2.0e-6, 0.0); zgradpulse(gzlvl5, gt5); delay(lambda-pwS6*0.5-pwS4*scale- gt5); h_sim3shapedpulse("reburp",shbw,shofs,0.0,2.0*pwN, zero, zero, zero, 0.0, 0.0); zgradpulse(gzlvl5, gt5); delay(lambda-pwS6*0.5-pwS4*scale- gt5); h_shapedpulse("eburp2",shbw,shofs,zero, 0.0, 0.0); delay(gt1/10.0+1.0e-4); dec2rgpulse(pwN,one,0.0,0.0); zgradpulse(gzlvl6, gt6); txphase(zero); delay(lambda-pwS6*0.5-gt6); h_sim3shapedpulse("reburp",shbw,shofs,0.0,2.0*pwN, zero, zero, zero, 0.0, 0.0); zgradpulse(gzlvl6, gt6); delay(lambda-pwS6*0.5-gt6); dec2rgpulse(pwN,t5,0.0,0.0); /**************************************************************************/ zgradpulse(-icosel*gzlvl2, gt1/10.0); dec2power(dpwr2); /* POWER_DELAY */ lk_sample(); if (n15_flg[0] =='y') { if (phase2==1) setreceiver(t14); else setreceiver(t15); } else { if (phase2==1) setreceiver(t24); else setreceiver(t25); } rcvron(); statusdelay(C,1.0e-4 ); }
void pulsesequence() { char shname1[MAXSTR], f1180[MAXSTR], f2180[MAXSTR], CT_flg[MAXSTR], n15_flg[MAXSTR]; int icosel, t1_counter, t2_counter, ni2 = getval("ni2"), phase; double d2_init=0.0, d3_init=0.0, pwS1,pwS2,pwS3,pwS4,pwS5,pwS6,pwS7,max, kappa, lambda = getval("lambda"), gzlvl1 = getval("gzlvl1"), gzlvl2 = getval("gzlvl2"), gzlvl3 = getval("gzlvl3"), gzlvl4 = getval("gzlvl4"), gzlvl5 = getval("gzlvl5"), gzlvl6 = getval("gzlvl6"), gt1 = getval("gt1"), gt3 = getval("gt3"), gt4 = getval("gt4"), gt5 = getval("gt5"), gt6 = getval("gt6"), gstab = getval("gstab"), tpwrsf = getval("tpwrsf"), shlvl1, shpw1 = getval("shpw1"), pwClvl = getval("pwClvl"), pwNlvl = getval("pwNlvl"), pwN = getval("pwN"), dpwr2 = getval("dpwr2"), d2 = getval("d2"), shbw = getval("shbw"), shofs = getval("shofs")-4.77, scale = getval("scale"), sw1 = getval("sw1"), timeTN = getval("timeTN"), timeTN1, Delta, t2a,t2b,halfT2,ctdelay, tauNCO = getval("tauNCO"), CTdelay = getval("CTdelay"), tauC = getval("tauC"), tau1, tau2, taunh = getval("taunh"); getstr("shname1", shname1); getstr("CT_flg",CT_flg); getstr("n15_flg",n15_flg); getstr("f1180",f1180); getstr("f2180",f2180); phase = (int) (getval("phase") + 0.5); settable(t1,2,phi1); settable(t3,1,phi3); settable(t4,4,phi4); settable(t5,1,phi5); settable(t14,4,phi14); settable(t24,4,phi24); /* INITIALIZE VARIABLES */ timeTN1= timeTN-tauC; Delta = timeTN-tauC-tauNCO; //shpw1 = pw*8.0; shlvl1=tpwr; pwS1 = c13pulsepw("ca", "co", "square", 90.0); pwS2 = c13pulsepw("ca", "co", "square", 180.0); pwS3 = c13pulsepw("co", "ca", "sinc", 180.0); pwS7 = c13pulsepw("co", "ca", "sinc", 90.0); pwS4 = h_shapedpw("eburp2",shbw,shofs,zero, 0.0, 0.0); pwS6 = h_shapedpw("reburp",shbw,shofs,zero, 0.0, 0.0); pwS5 = h_shapedpw("pc9f",shbw,shofs,zero, 2.0e-6, 0.0); if (CT_flg[0] == 'y') { if ( ni*1/(sw1)/2.0 > (CTdelay*0.5-gt3-1.0e-4)) { printf(" ni is too big. Make ni equal to %d or less.\n", ((int)((CTdelay*0.5-gt3-1.0e-4)*2.0*sw1))); psg_abort(1);} } if (phase == 1) ; if (phase == 2) {tsadd(t1,1,4);} if ( phase2 == 2 ) { tsadd ( t3,2,4 ); tsadd ( t5,2,4 ); icosel = +1; } else icosel = -1; /* Set up f1180 */ tau1 = d2; if((f1180[A] == 'y') && (ni > 1.0)) { tau1 += ( 1.0 / (2.0*sw1) ); if(tau1 < 0.2e-6) tau1 = 0.0; } /* Set up f2180 */ tau2 = d3; if((f2180[A] == 'y') && (ni2 > 1.0)) { tau2 += ( 1.0 / (2.0*sw2) ); if(tau2 < 0.2e-6) tau2 = 0.0; } /************************************************************/ if( ix == 1) d2_init = d2; t1_counter = (int) ( (d2-d2_init)*sw1 + 0.5 ); if(t1_counter % 2) { tsadd(t1,2,4); tsadd(t14,2,4); tsadd(t24,2,4); } if( ix == 1) d3_init = d3; t2_counter = (int) ( (d3-d3_init)*sw2 + 0.5 ); if(t2_counter % 2) { tsadd(t4,2,4); tsadd(t14,2,4); tsadd(t24,2,4); } /************************************************************/ /* Set up CONSTANT/SEMI-CONSTANT time evolution in N15 */ /************************************************************/ ctdelay = timeTN1-gt1-1.0e-4; // ctdelay = timeTN1-gt1-1.0e-4-2.0*GRADIENT_DELAY-4*POWER_DELAY-4*PWRF_DELAY-(4/PI)*pwN; if (ni2 > 1) { halfT2 = 0.5*(ni2-1)/sw2; t2b = (double) t2_counter*((halfT2 - ctdelay)/((double)(ni2-1))); if( ix==1 && halfT2 - timeTN > 0 ) printf("SCT mode on, max ni2=%g\n",timeTN*sw2*2+1); if(t2b < 0.0) t2b = 0.0; t2a = ctdelay - tau2*0.5 + t2b; if(t2a < 0.2e-6) t2a = 0.0; } else { t2b = 0.0; t2a = ctdelay - tau2*0.5; } /************************************************************/ status(A); rcvroff(); decpower(pwClvl); decoffset(dof); dec2power(pwNlvl); dec2offset(dof2); obspwrf(tpwrsf); decpwrf(4095.0); obsoffset(tof); set_c13offset("co"); dec2rgpulse(pwN*2.0,zero,0.0,0.0); zgradpulse(gzlvl4, gt4); delay(1.0e-4); delay(d1-gt4); lk_hold(); h_shapedpulse("pc9f",shbw,shofs,zero, 2.0e-6, 0.0); delay(lambda-pwS5*0.5-pwS6*0.4); h_sim3shapedpulse("reburp",shbw,shofs,0.0,2.0*pwN, one, zero, zero, 0.0, 0.0); delay(lambda-pwS5*0.5-pwS6*0.4); if(n15_flg[0]=='y') h_shapedpulse("pc9f_",shbw,shofs,three, 0.0, 0.0); else h_shapedpulse("pc9f_",shbw,shofs,one, 0.0, 0.0); zgradpulse(gzlvl4, gt4*4.0); delay(1.0e-4); obspower(shlvl1); /**************************************************************************/ /* xxxxxxxxxxxxxxxxxxxxxx N-> CA transfer xxxxxxxxxxxxxxxxxx */ /**************************************************************************/ dec2rgpulse(pwN,zero,0.0,0.0); delay(timeTN1); sim3_c13pulse("", "ca", "co", "square", "", 0.0, 180.0, 2.0*pwN, zero, zero, zero, 2.0e-6, 2.0e-6); delay(Delta); c13pulse("co", "ca", "sinc", 180.0, zero, 0.0, 0.0); delay(timeTN1-Delta-pwS3+pwN*4.0/3.0); c13pulse("co", "ca", "sinc", 90.0, zero, 0.0, 0.0); delay(tauC); c13pulse("ca", "co", "square", 180.0, zero, 2.0e-6, 2.0e-6); sim3_c13pulse("", "co", "ca", "sinc", "", 0.0, 180.0, 2.0*pwN, zero, zero, zero, 2.0e-6, 2.0e-6); delay(tauC); c13pulse("ca", "co", "square", 180.0, zero, 2.0e-6, 2.0e-6); c13pulse("co", "ca", "sinc", 90.0, one, 0.0, 0.0); dec2rgpulse(pwN,one,0.0,0.0); /**************************************************************************/ /* xxxxxxxxxxxxxxxxxxxxxx 13CA EVOLUTION xxxxxxxxxxxxxxxxxx */ /**************************************************************************/ set_c13offset("ca"); c13pulse("ca", "co", "square", 90.0, t1, 2.0e-6, 0.0); if(CT_flg[0]=='y') { delay(tau1*0.5); sim3_c13pulse(shname1, "co", "ca", "sinc", "", shpw1, 180.0, 2.0*pwN, zero, zero, zero, 2.0e-6, 2.0e-6); zgradpulse(gzlvl3, gt3); delay(1.0e-4); delay(CTdelay*0.5-gt3-1.0e-4); c13pulse("cab", "co", "square", 180.0, zero, 2.0e-6, 2.0e-6); delay(CTdelay*0.5-gt3-1.0e-4-tau1*0.5); sim3_c13pulse(shname1, "co", "ca", "sinc", "", shpw1, 180.0, 2.0*pwN, zero, zero, zero, 2.0e-6, 2.0e-6); zgradpulse(gzlvl3, gt3); delay(1.0e-4); } else { delay(tau1*0.5); sim3_c13pulse(shname1, "co", "ca", "sinc", "", shpw1, 180.0, 2.0*pwN, zero, zero, zero, 2.0e-6, 2.0e-6); zgradpulse(gzlvl3, gt3); delay(1.0e-4); delay(tau1*0.5); c13pulse("ca", "co", "square", 180.0, zero, 2.0e-6, 2.0e-6); sim3_c13pulse(shname1, "co", "ca", "sinc", "", shpw1, 180.0, 2.0*pwN, zero, zero, zero, 2.0e-6, 2.0e-6); zgradpulse(gzlvl3, gt3); delay(1.0e-4); } c13pulse("ca", "co", "square", 90.0, zero, 0.0, 0.0); set_c13offset("co"); /**************************************************************************/ /* xxxxxxxxxxxxxxxxxxxxxx N-> CA back transfer xxxxxxxxxxxxxxx */ /**************************************************************************/ obspower(shlvl1); dec2rgpulse(pwN,t4,0.0,0.0); c13pulse("co", "ca", "sinc", 90.0, one, 0.0, 0.0); c13pulse("ca", "co", "square", 180.0, zero, 2.0e-6, 2.0e-6); delay(tauC); sim3_c13pulse("", "co", "ca", "sinc", "", 0.0, 180.0, 2.0*pwN, zero, zero, zero, 2.0e-6, 2.0e-6); c13pulse("ca", "co", "square", 180.0, zero, 2.0e-6, 2.0e-6); delay(tauC); c13pulse("co", "ca", "sinc", 90.0, zero, 0.0, 0.0); // delay(timeTN1-Delta+tau2*0.5-pwS2-pwS3); delay(timeTN1-Delta+tau2*0.5-pwS2-pwS3-2.0*GRADIENT_DELAY+4*POWER_DELAY+4*PWRF_DELAY); c13pulse("co", "ca", "sinc", 180.0, zero, 0.0, 0.0); delay(Delta); c13pulse("ca", "co", "square", 180.0, zero, 0.0, 0.0); delay (t2b); dec2rgpulse (2.0*pwN, zero, 0.0, 0.0); zgradpulse(gzlvl1, gt1); delay(1.0e-4); delay (t2a); /**************************************************************************/ /** gradient-selected TROSY sequence *********/ /**************************************************************************/ delay(gt1/10.0+1.0e-4); h_shapedpulse("eburp2_",shbw,shofs,t3, 2.0e-6, 0.0); zgradpulse(gzlvl5, gt5); delay(lambda-pwS6*0.5-pwS4*scale- gt5); h_sim3shapedpulse("reburp",shbw,shofs,0.0,2.0*pwN, zero, zero, zero, 0.0, 0.0); zgradpulse(gzlvl5, gt5); delay(lambda-pwS6*0.5-pwS4*scale- gt5); h_shapedpulse("eburp2",shbw,shofs,zero, 0.0, 0.0); delay(gt1/10.0+1.0e-4); dec2rgpulse(pwN,one,0.0,0.0); zgradpulse(gzlvl6, gt6); txphase(zero); delay(lambda-pwS6*0.5-gt6); h_sim3shapedpulse("reburp",shbw,shofs,0.0,2.0*pwN, zero, zero, zero, 0.0, 0.0); zgradpulse(gzlvl6, gt6); delay(lambda-pwS6*0.5-gt6); dec2rgpulse(pwN,t5,0.0,0.0); /**************************************************************************/ zgradpulse(-icosel*gzlvl2, gt1/10.0); dec2power(dpwr2); lk_sample(); if (n15_flg[0] =='y') { setreceiver(t14); } else { setreceiver(t24); } rcvron(); statusdelay(C,1.0e-4 ); }
pulsesequence() { char autocal[MAXSTR], shname1[MAXSTR], shname2[MAXSTR], ipap_flg[MAXSTR], ab_flg[MAXSTR], f1180[MAXSTR], SE[MAXSTR], /*Use Sensitivity Enhancement */ c13refoc[MAXSTR], refpat[MAXSTR], /* pulse shape pattern refocus. pulse*/ hetsofast_flg[MAXSTR], grad3_flg[MAXSTR]; /*gradient flag */ int t1_counter, phase; double d2_init=0.0, pwS,pwS1,pwS2, tpwrsf = getval("tpwrsf"), adjust = getval("adjust"), gzlvl1 = getval("gzlvl1"), gzlvl2 = getval("gzlvl2"), gzlvl3 = getval("gzlvl3"), gstab = getval("gstab"), gt1 = getval("gt1"), gt2 = getval("gt2"), gt3 = getval("gt3"), shlvl1 = getval("shlvl1"), shlvl2 = getval("shlvl2"), shdmf2 = getval("shdmf2"), shbw = getval("shbw"), shpw1 = getval("shpw1"), shpw2 = getval("shpw2"), shpw3 = 0.0, shofs = getval("shofs"), flipangle = getval("flipangle"), pwNlvl = getval("pwNlvl"), pwN = getval("pwN"), dpwr2 = getval("dpwr2"), d2 = getval("d2"), tau1, taunh = 1.0/(2.0*getval("JNH")); void compo_pulse(); void compo1_pulse(); void makeshape_pc9(); void makeshape_refoc(); void makeshape_ndec(); getstr("autocal",autocal); getstr("f1180",f1180); getstr("c13refoc",c13refoc); getstr("hetsofast_flg",hetsofast_flg); getstr("refpat", refpat); /* pulse pattern refocussing pulse */ getstr("ipap_flg",ipap_flg); getstr("grad3_flg",grad3_flg); getstr("ab_flg",ab_flg); getstr("SE",SE); getstr("shname1",shname1); getstr("shname2",shname2); pwS = c_shapedpw("sech",200.0,0.0,zero, 0.0, 0.0); pwS1 = hn_simshapedpw(refpat,shbw,shofs-4.8,"isnob3",50.0,0.0, zero, zero, 0.0, 0.0); pwS2 = h_shapedpw(refpat,shbw,3.5,zero, 0.0, 0.0); if (hetsofast_flg[0] == 'a') shpw3 = h_shapedpw("isnob5",4.0,-3.0,two, 2.0e-6, 2.0e-6); if (hetsofast_flg[0] == 'b') shpw3 = h_shapedpw("gaus180",0.015,0.0,two, 2.0e-6, 2.0e-6); phase = (int) (getval("phase") + 0.5); settable(t1,2,phi1); settable(t2,2,phi2); if (autocal[0] == 'y') { (void) makeshape_pc9(flipangle, shbw, shofs); /*create pc9 pulse*/ sh90 = getRsh("hn_pc9"); shpw1 = sh90.pw; shlvl1 = sh90.pwr; sprintf(shname1,"hn_pc9"); (void) makeshape_refoc(refpat, shbw, shofs); /* create refocussing pulse */ shref = getDsh("hn_refoc"); shpw2 = shref.pw; shlvl2 = shref.pwr; shdmf2 = shref.dmf; sprintf(shname2,"hn_refoc"); if (dmm2[2] == 'p') /* waveform capability present on channel 3 */ { (void) makeshape_ndec(); /* create n15 wurst decoupling */ shdec = getDsh("hncompdec"); dpwr2 = shdec.pwr; dmf2 = shdec.dmf; dres2 = shdec.dres; sprintf(dseq2,"hncompdec"); } } if (tpwrsf <4095.0) shlvl2 = shlvl2+6.0; if (phase == 1) ; if (phase == 2) tsadd(t1,1,4); tau1 = d2; if((f1180[A] == 'y') && (ni > 1.0)) { tau1 += ( 1.0 / (2.0*sw1) ); if(tau1 < 0.2e-6) tau1 = 0.0; } tau1 = tau1; if (f1180[0] == 'y') tau1 = tau1-pwN*4.0/3.0; if( ix == 1) d2_init = d2; t1_counter = (int) ( (d2-d2_init)*sw1 + 0.5 ); if(t1_counter % 2) { tsadd(t1,2,4); tsadd(t2,2,4); } status(A); decoffset(dof); dec2power(pwNlvl); dec2offset(dof2); obsoffset(tof); obspower(tpwr); /**********************************************/ if (hetsofast_flg[0] != 'n') { if (hetsofast_flg[0] == 'a') h_shapedpulse("isnob5",4.0,-3.0,two, 2.0e-6, 2.0e-6); if (hetsofast_flg[0] == 'b') h_shapedpulse("gaus180",0.015,0.0,two, 2.0e-6, 2.0e-6); zgradpulse(gzlvl2, gt2); delay(gstab); delay(d1-gt2-shpw3); lk_hold(); } else { zgradpulse(gzlvl2, gt2); delay(gstab); delay(d1-gt2); lk_hold(); } obspower(shlvl1); shaped_pulse(shname1,shpw1,zero,2.0e-4,2.0e-6); if (SE[0] == 'y') { if (ipap_flg[0] == 'y') { if ((tau1+pwN*2.0) < pwS2) delay((pwS2*0.5-tau1*0.5-pwN)*0.5); if (grad3_flg[0]== 'y') delay(taunh*0.5-shpw1*0.533-pwS1*0.5+(gt3*2.0+2.0*gstab+pwN*3.0)); else delay(taunh*0.5-shpw1*0.533-pwS1*0.5+pwN); hn_simshapedpulse(refpat,shbw,shofs-4.8,"bip720_50_20",40.0,0.0, zero, zero, 0.0, 0.0); obspower(shlvl2); obspwrf(4095.0); compo1_pulse(shname2,shpw2,pwN,shdmf2,t1,tau1,c13refoc,pwS,taunh,pwS1,pwS2,gt1,gt3,gzlvl3,grad3_flg,gstab); obspower(shlvl2); obspwrf(4095.0); zgradpulse(gzlvl1, gt1); delay(gstab); h_sim3shapedpulse(refpat,shbw,shofs-4.8,0.0,2.0*pwN, one, zero, zero, 0.0, 0.0); zgradpulse(gzlvl1, gt1); delay(gstab); delay(taunh*0.5-gt1-gstab-POWER_DELAY-pwS1*0.5); if ((tau1+pwN*2.0) < pwS2) delay((pwS2*0.5-tau1*0.5-pwN)*0.5); if (ab_flg[0] == 'a') dec2rgpulse(pwN,one,0.0,0.0); else dec2rgpulse(pwN,three,0.0,0.0); if (grad3_flg[0]== 'y') { delay(gt3+gstab); dec2rgpulse(pwN*2.0,zero,0.0,0.0); zgradpulse(gzlvl3,gt3); delay(gstab); } } else { zgradpulse(gzlvl1, gt1); delay(gstab); if ((tau1+pwN*2.0) < pwS2) delay(taunh-gt1-gstab-shpw1*0.533-adjust-(pwS2*0.5-tau1*0.5-pwN)*0.5); else delay(taunh-gt1-gstab-shpw1*0.533-adjust); obspower(shlvl2); obspwrf(tpwrsf); compo_pulse(shname2,shpw2,pwN,shdmf2,t1,tau1,c13refoc,pwS); obspower(shlvl1); obspwrf(4095.0); zgradpulse(gzlvl1, gt1); delay(gstab); if ((tau1+pwN*2.0) < pwS2) delay(taunh-gt1-gstab-POWER_DELAY-(pwS2*0.5-tau1*0.5-pwN)*0.5); else delay(taunh-gt1-gstab-POWER_DELAY); } } else { if ((ni == 0) || (ni == 1)) { zgradpulse(gzlvl1, gt1); delay(gstab); delay(taunh-gt1-gstab-WFG_START_DELAY+pwN*4.0-shpw1*0.533-adjust); obspwrf(tpwrsf); obspower(shlvl2); xmtrphase(zero); xmtron(); obsunblank(); obsprgon(shname2,1/shdmf2,9.0); delay(shpw2); obsprgoff(); obsblank(); xmtroff(); obspower(shlvl2); obspwrf(4095.0); dec2rgpulse(pwN,t1,0.0,0.0); dec2rgpulse(pwN*2.0,zero,0.0,0.0); dec2rgpulse(pwN,zero,0.0,0.0); } else { zgradpulse(gzlvl1, gt1); delay(gstab); delay(taunh-gt1-gstab-shpw1*0.533-adjust); obspower(shlvl2); obspwrf(tpwrsf); compo_pulse(shname2,shpw2,pwN,shdmf2,t1,tau1,c13refoc,pwS); obspower(shlvl1); obspwrf(4095.0); } if (ipap_flg[0] == 'y') { if (ab_flg[0] == 'b') { zgradpulse(gzlvl1, gt1); delay(gstab); delay(taunh-gt1-gstab-pwN-POWER_DELAY); dec2rgpulse(pwN,one,0.0,0.0); } else { zgradpulse(gzlvl1, gt1); delay(gstab); delay(taunh*0.5-gt1-pwN-gstab); dec2rgpulse(pwN*2.0,zero,0.0,0.0); delay(taunh*0.5-pwN-POWER_DELAY); } } else { zgradpulse(gzlvl1, gt1); delay(gstab); delay(taunh-gt1-gstab-POWER_DELAY); } } dec2power(dpwr2); lk_sample(); setreceiver(t2); status(C); }
pulsesequence() { char shname1[MAXSTR], f1180[MAXSTR], f2180[MAXSTR], SE_flg[MAXSTR], dec_flg[MAXSTR], CT_flg[MAXSTR]; int icosel=1, t1_counter, t2_counter, ni2 = getval("ni2"), phase; double d2_init=0.0, d3_init=0.0, pwS1,pwS2,pwS3,pwS4,pwS5,pwS6, lambda = getval("lambda"), CTdelay = getval("CTdelay"), gzlvl1 = getval("gzlvl1"), gzlvl2 = getval("gzlvl2"), gzlvl3 = getval("gzlvl3"), gzlvl4 = getval("gzlvl4"), gzlvl5 = getval("gzlvl5"), gzlvl6 = getval("gzlvl6"), gt1 = getval("gt1"), gt2 = getval("gt2"), gt3 = getval("gt3"), gt4 = getval("gt4"), gt5 = getval("gt5"), gt6 = getval("gt6"), gstab = getval("gstab"), tpwrsf = getval("tpwrsf"), shlvl1, shpw1, pwClvl = getval("pwClvl"), pwC = getval("pwC"), pwNlvl = getval("pwNlvl"), pwN = getval("pwN"), dpwr2 = getval("dpwr2"), d2 = getval("d2"), shbw = getval("shbw"), shofs = getval("shofs")-4.77, timeTN = getval("timeTN"), tauC = getval("tauC"), tau1 = getval("tau1"), tau2 = getval("tau2"), taunh = getval("taunh"); getstr("shname1", shname1); getstr("SE_flg",SE_flg); getstr("dec_flg",dec_flg); getstr("CT_flg",CT_flg); getstr("f1180",f1180); getstr("f2180",f2180); phase = (int) (getval("phase") + 0.5); settable(t1,2,phi1); settable(t3,4,phi3); settable(t10,1,phi10); settable(t12,4,phi12); settable(t13,4,phi13); /* INITIALIZE VARIABLES */ shpw1 = pw*8.0; shlvl1 = tpwr; pwS1 = c13pulsepw("co", "ca", "sinc", 90.0); pwS2 = c13pulsepw("co", "ca", "sinc", 180.0); pwS3 = c13pulsepw("ca", "co", "square", 180.0); pwS4 = h_shapedpw("eburp2",shbw,shofs,zero, 0.0, 0.0); pwS6 = h_shapedpw("reburp",shbw,shofs,zero, 0.0, 0.0); pwS5 = h_shapedpw("pc9f",shbw,shofs,zero, 2.0e-6, 0.0); if (SE_flg[0] == 'y') { if ( ni2*1/(sw2)/2.0 > (timeTN-pwS2*0.5-pwS4)) { printf(" ni2 is too big. Make ni2 equal to %d or less.\n", ((int)((timeTN-pwS2*0.5-pwS4)*2.0*sw2))); psg_abort(1);} } else { if ( ni2*1/(sw2)/2.0 > (timeTN-pwS2*0.5)) { printf(" ni2 is too big. Make ni2 equal to %d or less.\n", ((int)((timeTN-pwS2*0.5)*2.0*sw2))); psg_abort(1);} } if (CT_flg[0] == 'y') { if ( ni*1/(sw1) > (CTdelay)) { printf(" ni is too big. Make ni equal to %d or less.\n", ((int)(CTdelay*sw1))); psg_abort(1);} } if (phase == 1) ; if (phase == 2) tsadd(t1,1,4); if (SE_flg[0] =='y') { if (phase2 == 2) {tsadd(t10,2,4); icosel = +1;} else icosel = -1; } else { if (phase2 == 2) tsadd(t3,1,4); } tau1 = d2; if((f1180[A] == 'y') ) { tau1 += ( 1.0 / (2.0*sw1) ); if(tau1 < 0.2e-6) tau1 = 0.0; } tau1 = tau1; tau2 = d3; if((f2180[A] == 'y') ) { tau2 += ( 1.0 / (2.0*sw2) ); if(tau2 < 0.2e-6) tau2 = 0.0; } tau2 = tau2; if( ix == 1) d2_init = d2; t1_counter = (int) ( (d2-d2_init)*sw1 + 0.5 ); if(t1_counter % 2) { tsadd(t1,2,4); tsadd(t12,2,4); tsadd(t13,2,4); } if( ix == 1) d3_init = d3; t2_counter = (int) ( (d3-d3_init)*sw2 + 0.5 ); if(t2_counter % 2) { tsadd(t3,2,4); tsadd(t12,2,4); tsadd(t13,2,4); } status(A); rcvroff(); decpower(pwClvl); decoffset(dof); dec2power(pwNlvl); dec2offset(dof2); obspwrf(tpwrsf); decpwrf(4095.0); obsoffset(tof); set_c13offset("co"); zgradpulse(gzlvl2, gt2); delay(1.0e-4); delay(d1-gt2); lk_hold(); h_shapedpulse("pc9f",shbw,shofs,zero, 2.0e-6, 0.0); delay(lambda-pwS5*0.5-pwS6*0.4); h_sim3shapedpulse("reburp",shbw,shofs,0.0,2.0*pwN, one, zero, zero, 0.0, 0.0); delay(lambda-pwS5*0.5-pwS6*0.4); h_shapedpulse("pc9f_",shbw,shofs,one, 0.0, 0.0); obspower(shlvl1); /**************************************************************************/ dec2rgpulse(pwN,zero,0.0,0.0); zgradpulse(gzlvl6,gt6); delay(timeTN-pwS2*0.5-gt6); sim3_c13pulse("", "co", "ca", "sinc", "", 0.0, 180.0, 2.0*pwN, zero, zero, zero, 2.0e-6, 2.0e-6); delay(timeTN-pwS2*0.5-taunh*0.5-shpw1); shaped_pulse(shname1,shpw1,two,0.0,0.0); zgradpulse(gzlvl6, gt6); delay(taunh*0.5-gt6); dec2rgpulse(pwN,zero,0.0,0.0); shaped_pulse(shname1,shpw1,zero,0.0,0.0); /**************************************************************************/ /*** CO -> CA transfer *********************************/ /**************************************************************************/ c13pulse("co", "ca", "sinc", 90.0, zero, 2.0e-6, 0.0); zgradpulse(-gzlvl4, gt4); decphase(zero); delay(tauC - gt4 - 0.5*10.933*pwC); decrgpulse(pwC*158.0/90.0, zero, 0.0, 0.0); decrgpulse(pwC*171.2/90.0, two, 0.0, 0.0); decrgpulse(pwC*342.8/90.0, zero, 0.0, 0.0); /* Shaka 6 composite */ decrgpulse(pwC*145.5/90.0, two, 0.0, 0.0); decrgpulse(pwC*81.2/90.0, zero, 0.0, 0.0); decrgpulse(pwC*85.3/90.0, two, 0.0, 0.0); zgradpulse(-gzlvl4, gt4); decphase(one); delay(tauC - gt4 - 0.5*10.933*pwC - WFG_START_DELAY - 2.0e-6); c13pulse("co", "ca", "sinc", 90.0, one, 2.0e-6, 0.0); /**************************************************************************/ /* xxxxxxxxxxxxxxxxxxxx 13Ca EVOLUTION xxxxxxxxxxxxxxxxxx */ /**************************************************************************/ set_c13offset("ca"); if (CT_flg[0] == 'y') { c13pulse("ca", "co", "square", 90.0, t1, 2.0e-6, 0.0); delay(tau1*0.5); sim3_c13pulse("", "co", "ca", "sinc", "", 0.0, 180.0, 2.0*pwN, zero, zero, zero, 0.0, 0.0); delay(CTdelay*0.5); c13pulse("cab", "co", "square", 180.0, zero, 0.0, 0.0); delay((CTdelay-tau1)*0.5); c13pulse("co", "ca", "sinc", 180.0, zero, 0.0, 0.0); c13pulse("ca", "co", "square", 90.0, zero, 0.0, 0.0); } else { if (dec_flg[0] == 'y') { c13pulse("ca", "co", "square", 90.0, t1, 2.0e-6, 2.0e-6); delay(tau1*0.5); c_shapedpulse2("isnob5",30.0,-31.0,"isnob5",30.0,120.0 , zero, 0.0, 0.0); dec2rgpulse(pwN*2.0,zero,0.0,0.0); delay(tau1*0.5); c13pulse("ca", "co", "square", 180.0, zero, 2.0e-6, 2.0e-6); dec2rgpulse(pwN*2.0,two,0.0,0.0); c_shapedpulse2("isnob5",30.0,-31.0,"isnob5",30.0,120.0 , two, 0.0, 0.0); c13pulse("ca", "co", "square", 90.0, zero, 2.0e-6, 2.0e-6); } else { c13pulse("ca", "co", "square", 90.0, t1, 2.0e-6, 2.0e-6); delay(tau1*0.5); sim3_c13pulse("", "co", "ca", "sinc", "", 0.0, 180.0, 2.0*pwN, zero, zero, zero, 2.0e-6, 2.0e-6); delay(tau1*0.5); c13pulse("ca", "co", "square", 180.0, zero, 2.0e-6, 2.0e-6); c13pulse("co", "ca", "sinc", 180.0, zero, 2.0e-6, 2.0e-6); if (pwN*2.0 > pwS2) delay(pwN*2.0 - pwS2); c13pulse("ca", "co", "square", 90.0, zero, 2.0e-6, 2.0e-6); } } set_c13offset("co"); zgradpulse(gzlvl3, gt3); delay(1.0e-4); /**************************************************************************/ /*** CO -> CA transfer *********************************/ /**************************************************************************/ c13pulse("co", "ca", "sinc", 90.0, one, 2.0e-6, 0.0); zgradpulse(gzlvl4, gt4*0.7); delay(tauC - gt4*0.7 - 0.5*10.933*pwC); decrgpulse(pwC*158.0/90.0, zero, 0.0, 0.0); decrgpulse(pwC*171.2/90.0, two, 0.0, 0.0); decrgpulse(pwC*342.8/90.0, zero, 0.0, 0.0); /* Shaka 6 composite */ decrgpulse(pwC*145.5/90.0, two, 0.0, 0.0); decrgpulse(pwC*81.2/90.0, zero, 0.0, 0.0); decrgpulse(pwC*85.3/90.0, two, 0.0, 0.0); zgradpulse(gzlvl4, gt4*0.7); delay(tauC - gt4*0.7 - 0.5*10.933*pwC - WFG_START_DELAY - 2.0e-6); /* WFG_START_DELAY */ c13pulse("co", "ca", "sinc", 90.0, zero, 2.0e-6, 0.0); /**************************************************************************/ obspower(shlvl1); shaped_pulse(shname1,shpw1,zero,0.0,0.0); dec2rgpulse(pwN,t3,0.0,0.0); if (SE_flg[0] == 'y') { delay(tau2*0.5); c13pulse("ca", "co", "square", 180.0, zero, 0.0, 0.0); delay(taunh*0.5-pwS3); shaped_pulse(shname1,shpw1,two,0.0,0.0); delay(timeTN-pwS2*0.5-shpw1-taunh*0.5-gt1-1.0e-4); zgradpulse(-gzlvl1, gt1); delay(1.0e-4); sim3_c13pulse("", "co", "ca", "sinc", "", 0.0, 180.0, 2.0*pwN, zero, zero, zero, 2.0e-6, 2.0e-6); delay(timeTN-pwS2*0.5-tau2*0.5-pwS4); h_shapedpulse("eburp2",shbw,shofs,zero, 2.0e-6, 0.0); dec2rgpulse(pwN, t10, 0.0, 0.0); } else { delay(tau2*0.5); c13pulse("ca", "co", "square", 180.0, zero, 0.0, 0.0); delay(taunh*0.5-pwS3); shaped_pulse(shname1,shpw1,two,0.0,0.0); delay(timeTN-pwS2*0.5-taunh*0.5-shpw1); sim3_c13pulse("", "co", "ca", "sinc", "", 0.0, 180.0, 2.0*pwN, zero, zero, zero, 2.0e-6, 2.0e-6); delay(timeTN-pwS2*0.5-tau2*0.5); dec2rgpulse(pwN, zero, 0.0, 0.0); } /**************************************************************************/ if (SE_flg[0] == 'y') { zgradpulse(gzlvl5, gt5); delay(lambda-pwS6*0.4 - gt5); h_sim3shapedpulse("reburp",shbw,shofs,0.0,2.0*pwN, zero, zero, zero, 0.0, 0.0); zgradpulse(gzlvl5, gt5); delay(lambda-pwS6*0.4 - gt5); dec2rgpulse(pwN, one, 0.0, 0.0); h_shapedpulse("eburp2_",shbw,shofs,one, 0.0, 0.0); txphase(zero); dec2phase(zero); delay(lambda-pwS4*0.5-pwS6*0.4); h_sim3shapedpulse("reburp",shbw,shofs,0.0,2.0*pwN, zero, zero, zero, 0.0, 0.0); dec2phase(t10); delay(lambda-pwS4*0.5-pwS6*0.4); h_shapedpulse("eburp2",shbw,shofs,zero, 0.0, 0.0); delay((gt1/10.0) + 1.0e-4 +gstab + 2.0*GRADIENT_DELAY + POWER_DELAY); h_shapedpulse("reburp",shbw,shofs,zero, 0.0, rof2); zgradpulse(icosel*gzlvl2, gt1/10.0); /* 2.0*GRADIENT_DELAY */ delay(gstab); } else { h_shapedpulse("eburp2",shbw,shofs,zero, 2.0e-6, 0.0); zgradpulse(gzlvl5, gt5); delay(lambda-pwS6*0.4 - gt5); h_sim3shapedpulse("reburp",shbw,shofs,0.0,2.0*pwN, zero, zero, zero, 0.0, 0.0); zgradpulse(gzlvl5, gt5); delay(lambda-pwS6*0.4 - gt5-POWER_DELAY-1.0e-4); } dec2power(dpwr2); /* POWER_DELAY */ lk_sample(); if (SE_flg[0] == 'y') setreceiver(t13); else setreceiver(t12); rcvron(); statusdelay(C,1.0e-4 ); }
pulsesequence() { char shname1[MAXSTR], f1180[MAXSTR], f2180[MAXSTR], SE_flg[MAXSTR]; int icosel = 0, t1_counter, t2_counter, ni2 = getval("ni2"), phase; double d2_init=0.0, d3_init=0.0, pwS1,pwS2,pwS3,pwS4,pwS5,pwS6,pwS7, lambda = getval("lambda"), gzlvl1 = getval("gzlvl1"), gzlvl2 = getval("gzlvl2"), gzlvl6 = getval("gzlvl6"), gzlvl5 = getval("gzlvl5"), gt1 = getval("gt1"), gt6 = getval("gt6"), gt5 = getval("gt5"), gstab = getval("gstab"), shlvl1 = getval("shlvl1"), shpw1 = getval("shpw1"), pwClvl = getval("pwClvl"), pwNlvl = getval("pwNlvl"), pwN = getval("pwN"), d2 = getval("d2"), timeTN = getval("timeTN"), timeTN1, Delta, tauNCO = getval("tauNCO"), tauC = getval("tauC"), tau1 = getval("tau1"), tau2 = getval("tau2"), taunh = getval("taunh"); getstr("shname1", shname1); getstr("SE_flg",SE_flg); getstr("f1180",f1180); getstr("f2180",f2180); phase = (int) (getval("phase") + 0.5); settable(t1,2,phi1); settable(t3,4,phi3); settable(t10,1,phi10); settable(t12,4,phi12); settable(t13,4,phi13); /* INITIALIZE VARIABLES */ timeTN1= timeTN-tauC; Delta = timeTN-tauC-tauNCO; pwS1 = c13pulsepw("ca", "co", "square", 90.0); pwS2 = c13pulsepw("ca", "co", "square", 180.0); pwS3 = c13pulsepw("co", "ca", "sinc", 180.0); pwS7 = c13pulsepw("co", "ca", "sinc", 90.0); pwS4 = h_shapedpw("eburp2",4.0,3.5,zero, 0.0, 0.0); pwS5 = h_shapedpw("reburp",4.0,3.5,zero, 0.0, 0.0); pwS6 = h_shapedpw("pc9f",4.0,3.5,zero, 2.0e-6, 0.0); if (SE_flg[0] == 'y') { if ( ni2*1/(sw2)/2.0 > (timeTN1-Delta-pwS3-pwS4)) { printf(" ni2 is too big. Make ni2 equal to %d or less.\n", ((int)((timeTN1-Delta-pwS3-pwS4)*2.0*sw2))); psg_abort(1);} } else { if ( ni2*1/(sw2)/2.0 > (timeTN1-Delta-pwS3)) { printf(" ni2 is too big. Make ni2 equal to %d or less.\n", ((int)((timeTN1-Delta-pwS3)*2.0*sw2))); psg_abort(1);} } if (phase == 1) ; if (phase == 2) tsadd(t1,1,4); if (SE_flg[0] =='y') { if (phase2 == 2) {tsadd(t10,2,4); icosel = +1;} else icosel = -1; } else { if (phase2 == 2) {tsadd(t3,1,4); icosel = 1;} } tau1 = d2; if((f1180[A] == 'y') ) { tau1 += ( 1.0 / (2.0*sw1) ); if(tau1 < 0.2e-6) tau1 = 0.0; } tau1 = tau1; tau2 = d3; if((f2180[A] == 'y') ) { tau2 += ( 1.0 / (2.0*sw2) ); if(tau2 < 0.2e-6) tau2 = 0.0; } tau2 = tau2; if( ix == 1) d2_init = d2; t1_counter = (int) ( (d2-d2_init)*sw1 + 0.5 ); if(t1_counter % 2) { tsadd(t1,2,4); tsadd(t12,2,4); tsadd(t13,2,4); } if( ix == 1) d3_init = d3; t2_counter = (int) ( (d3-d3_init)*sw2 + 0.5 ); if(t2_counter % 2) { tsadd(t3,2,4); tsadd(t12,2,4); tsadd(t13,2,4); } status(A); decpower(pwClvl); dec2power(pwNlvl); set_c13offset("co"); zgradpulse(gzlvl6, gt6); delay(d1-gt6 +1.0e-4); lk_hold(); rcvroff(); h_shapedpulse("pc9f",4.0,3.5,zero, 2.0e-6, 0.0); delay(lambda-pwS5*0.5-pwS6*0.4); h_sim3shapedpulse("reburp",4.0,3.5,0.0,2.0*pwN, one, zero, zero, 0.0, 0.0); delay(lambda-pwS5*0.5-pwS6*0.4); h_shapedpulse("pc9f_",4.0,3.5,one, 2.0e-6, 0.0); obspower(shlvl1); /**************************************************************************/ /* xxxxxxxxxxxxxxxxxxxxxx N-> CA transfer xxxxxxxxxxxxxxxxxx */ /**************************************************************************/ dec2rgpulse(pwN,zero,0.0,0.0); delay(timeTN1); sim3_c13pulse("", "ca", "co", "square", "", 0.0, 180.0, 2.0*pwN, zero, zero, zero, 2.0e-6, 2.0e-6); delay(Delta); c13pulse("co", "ca", "sinc", 180.0, zero, 0.0, 0.0); delay(timeTN1-Delta-pwS3+pwN*4.0/3.0); c13pulse("co", "ca", "sinc", 90.0, zero, 0.0, 0.0); delay(tauC); c13pulse("ca", "co", "square", 180.0, zero, 2.0e-6, 2.0e-6); sim3_c13pulse("", "co", "ca", "sinc", "", 0.0, 180.0, 2.0*pwN, zero, zero, zero, 2.0e-6, 2.0e-6); delay(tauC-taunh*0.5-shpw1+pwS2+pwS7); shaped_pulse(shname1,shpw1,zero,0.0,0.0); delay(taunh*0.5-pwS2-pwS7); c13pulse("ca", "co", "square", 180.0, zero, 2.0e-6, 2.0e-6); c13pulse("co", "ca", "sinc", 90.0, one, 0.0, 0.0); dec2rgpulse(pwN,zero,0.0,0.0); /**************************************************************************/ /* xxxxxxxxxxxxxxxxxxxxxx 13CA EVOLUTION xxxxxxxxxxxxxxxxxx */ /**************************************************************************/ set_c13offset("ca"); c13pulse("ca", "co", "square", 90.0, t1, 2.0e-6, 0.0); delay(tau1*0.5); sim3_c13pulse(shname1, "co", "ca", "sinc", "", shpw1, 180.0, 2.0*pwN, zero, zero, zero, 0.0, 0.0); delay(tau1*0.5); c13pulse("ca", "co", "square", 180.0, zero, 0.0, 0.0); sim3_c13pulse("", "co", "ca", "sinc", "", 0.0, 180.0, 0.0, zero, zero, zero, 0.0, 0.0); if (pwN*2.0 > pwS3) delay(pwN*2.0-pwS3); c13pulse("ca", "co", "square", 90.0, zero, 0.0, 0.0); set_c13offset("co"); /**************************************************************************/ /**************************************************************************/ /**************************************************************************/ obspower(shlvl1); dec2rgpulse(pwN,t3,0.0,0.0); c13pulse("co", "ca", "sinc", 90.0, one, 0.0, 0.0); c13pulse("ca", "co", "square", 180.0, zero, 2.0e-6, 2.0e-6); delay(tauC); sim3_c13pulse("", "co", "ca", "sinc", "", 0.0, 180.0, 2.0*pwN, zero, zero, zero, 2.0e-6, 2.0e-6); c13pulse("ca", "co", "square", 180.0, zero, 2.0e-6, 2.0e-6); delay(tauC-taunh*0.5-shpw1); shaped_pulse(shname1,shpw1,zero,0.0,0.0); delay(taunh*0.5); c13pulse("co", "ca", "sinc", 90.0, zero, 0.0, 0.0); /**************************************************************************/ if (SE_flg[0] == 'y') { delay(tau2*0.5); shaped_pulse(shname1,shpw1,two,0.0,0.0); delay(timeTN1+pwN*4.0/3.0-shpw1-gt1-1.0e-4); zgradpulse(-gzlvl1, gt1); delay(1.0e-4); sim3_c13pulse("", "ca", "co", "square", "", 0.0, 180.0, 2.0*pwN, zero, zero, zero, 2.0e-6, 2.0e-6); delay(Delta); c13pulse("co", "ca", "sinc", 180.0, zero, 0.0, 0.0); delay(timeTN1-tau2*0.5-pwS4-Delta-pwS3); h_shapedpulse("eburp2",4.0,3.5,zero, 2.0e-6, 0.0); dec2rgpulse(pwN, t10, 0.0, 0.0); } else { delay(tau2*0.5); shaped_pulse(shname1,shpw1,two,0.0,0.0); delay(timeTN1+pwN*4.0/3.0-shpw1); sim3_c13pulse("", "ca", "co", "square", "", 0.0, 180.0, 2.0*pwN, zero, zero, zero, 2.0e-6, 2.0e-6); delay(Delta); c13pulse("co", "ca", "sinc", 180.0, zero, 0.0, 0.0); delay(timeTN1-tau2*0.5-Delta-pwS3); dec2rgpulse(pwN, zero, 0.0, 0.0); } /**************************************************************************/ if (SE_flg[0] == 'y') { zgradpulse(gzlvl5, gt5); delay(lambda-pwS6*0.4 - gt5); h_sim3shapedpulse("reburp",4.0,3.5,0.0,2.0*pwN, zero, zero, zero, 0.0, 0.0); zgradpulse(gzlvl5, gt5); delay(lambda-pwS6*0.4 - gt5); dec2rgpulse(pwN, one, 0.0, 0.0); h_shapedpulse("eburp2_",4.0,3.5,one, 0.0, 0.0); txphase(zero); dec2phase(zero); delay(lambda-pwS4*0.5-pwS6*0.4); h_sim3shapedpulse("reburp",4.0,3.5,0.0,2.0*pwN, zero, zero, zero, 0.0, 0.0); dec2phase(t10); delay(lambda-pwS4*0.5-pwS6*0.4); h_shapedpulse("eburp2",4.0,3.5,zero, 0.0, 0.0); delay((gt1/10.0) + 1.0e-4 +gstab + 2.0*GRADIENT_DELAY + POWER_DELAY); h_shapedpulse("reburp",4.0,3.5,zero, 0.0, 0.0); zgradpulse(icosel*gzlvl2, gt1/10.0); /* 2.0*GRADIENT_DELAY */ delay(gstab); } else { h_shapedpulse("eburp2",4.0,3.5,zero, 2.0e-6, 0.0); zgradpulse(gzlvl5, gt5); delay(lambda-pwS6*0.4 - gt5); h_sim3shapedpulse("reburp",4.0,3.5,0.0,2.0*pwN, zero, zero, zero, 0.0, 0.0); zgradpulse(gzlvl5, gt5); delay(lambda-pwS6*0.4 - gt5-POWER_DELAY-1.0e-4); } dec2power(dpwr2); /* POWER_DELAY */ lk_sample(); if (SE_flg[0] == 'y') setreceiver(t13); else setreceiver(t12); rcvron(); statusdelay(C,1.0e-4 ); }
pulsesequence() { char shname1[MAXSTR], f1180[MAXSTR], SE_flg[MAXSTR]; int icosel = 0, t1_counter, phase; double d2_init=0.0, pwS4,pwS5,pwS6,pwS7, lambda = getval("lambda"), gzlvl1 = getval("gzlvl1"), gzlvl2 = getval("gzlvl2"), gzlvl3 = getval("gzlvl3"), gzlvl5 = getval("gzlvl5"), gt1 = getval("gt1"), gt3 = getval("gt3"), gt5 = getval("gt5"), gstab = getval("gstab"), shpw1,shlvl1=getval("shlvl1"), pwClvl = getval("pwClvl"), pwNlvl = getval("pwNlvl"), pwN = getval("pwN"), ni = getval("ni"), d2 = getval("d2"), tau1 = getval("tau1"); getstr("shname1", shname1); getstr("SE_flg",SE_flg); getstr("f1180",f1180); phase = (int) (getval("phase") + 0.5); settable(t3,2,phi3); settable(t10,1,phi10); settable(t12,2,phi12); settable(t13,2,phi13); /* INITIALIZE VARIABLES */ shpw1 = getval("shpw1"); pwS4 = h_shapedpw("eburp2",4.0,3.5,zero, 0.0, 0.0); pwS5 = h_shapedpw("pc9f",4.0,3.5,zero, 2.0e-6, 0.0); pwS6 = h_shapedpw("reburp",4.0,3.5,zero, 0.0, 0.0); pwS7 = c_shapedpw2("isnob5",40.0,-125.0,"isnob5",40.0,0.0 , two, 0.0, 0.0); if (SE_flg[0] =='y') { if (phase == 2) {tsadd(t10,2,4); icosel = +1;} else icosel = -1; } else { if (phase == 2) {tsadd(t3,1,4); icosel=1;} } tau1 = d2; if((f1180[A] == 'y') ) { tau1 += ( 1.0 / (2.0*sw1) ); if(tau1 < 0.2e-6) tau1 = 0.0; } tau1 = tau1; if( ix == 1) d2_init = d2; t1_counter = (int) ( (d2-d2_init)*sw1 + 0.5 ); if(t1_counter % 2) { tsadd(t3,2,4);tsadd(t12,2,4); tsadd(t13,2,4); } status(A); decpower(pwClvl); dec2power(pwNlvl); set_c13offset("co"); zgradpulse(gzlvl3, gt3); delay(d1-gt3); lk_hold(); rcvroff(); h_shapedpulse("pc9f",4.0,3.5,zero, 2.0e-6, 0.0); delay(lambda-pwS5*0.5-pwS6*0.4); h_sim3shapedpulse("reburp",4.0,3.5,0.0,2.0*pwN, one, zero, zero, 0.0, 0.0); delay(lambda-pwS5*0.5-pwS6*0.4); h_shapedpulse("pc9f_",4.0,3.5,one, 0.0, 0.0); obspower(shlvl1); /**************************************************************************/ /** Sensitivity enhanced version **********************/ /**************************************************************************/ if (SE_flg[0] == 'y') { shaped_pulse(shname1,shpw1,zero,0.0,0.0); dec2rgpulse(pwN,t3,0.0,0.0); delay(tau1*0.5); shaped_pulse(shname1,shpw1,two,0.0,0.0); c_shapedpulse2("isnob5",40.0,-125.0,"isnob5",40.0,0.0 , two, 0.0, 0.0); delay(tau1*0.5); zgradpulse(-gzlvl1, gt1); delay(pwS4-shpw1-pwS7-gt1); dec2rgpulse(pwN*2.0,zero,0.0,0.0); h_shapedpulse("eburp2",4.0,3.5,zero, 2.0e-6, 0.0); dec2rgpulse(pwN, t10, 0.0, 0.0); } /**************************************************************************/ /** standard INEPT-based version **********************/ /**************************************************************************/ else { if (ni < 1.0) { dec2rgpulse(pwN,t3,0.0,0.0); dec2rgpulse(pwN*2.0, zero, 0.0, 0.0); dec2rgpulse(pwN, zero, 0.0, 0.0); } else { if (tau1 < shpw1) { shaped_pulse(shname1,shpw1,two,0.0,0.0); shaped_pulse(shname1,shpw1,zero,0.0,0.0); dec2rgpulse(pwN,t3,0.0,0.0); delay(tau1); dec2rgpulse(pwN*3.0, zero, 0.0, 0.0); } else { if (tau1*0.5 < (pwS7+shpw1*0.5)) { shaped_pulse(shname1,shpw1,two,0.0,0.0); dec2rgpulse(pwN,t3,0.0,0.0); delay(tau1*0.5-shpw1*0.5); shaped_pulse(shname1,shpw1,zero,0.0,0.0); delay(tau1*0.5-shpw1*0.5); dec2rgpulse(pwN*3.0, zero, 0.0, 0.0); } else { shaped_pulse(shname1,shpw1,two,0.0,0.0); dec2rgpulse(pwN,t3,0.0,0.0); delay(tau1*0.5-shpw1*0.5); shaped_pulse(shname1,shpw1,zero,0.0,0.0); c_shapedpulse2("isnob5",40.0,-125.0,"isnob5",40.0,0.0 , two, 0.0, 0.0); delay(tau1*0.5-shpw1*0.5-pwS7); dec2rgpulse(pwN*3.0, zero, 0.0, 0.0); } } } } /**************************************************************************/ if (SE_flg[0] == 'y') { zgradpulse(gzlvl5, gt5); delay(lambda-pwS6*0.4 - gt5); h_sim3shapedpulse("reburp",4.0,3.5,0.0,2.0*pwN, zero, zero, zero, 0.0, 0.0); zgradpulse(gzlvl5, gt5); delay(lambda-pwS6*0.4 - gt5); dec2rgpulse(pwN, one, 0.0, 0.0); h_shapedpulse("eburp2_",4.0,3.5,one, 0.0, 0.0); txphase(zero); dec2phase(zero); delay(lambda-pwS4*0.5-pwS6*0.4); h_sim3shapedpulse("reburp",4.0,3.5,0.0,2.0*pwN, zero, zero, zero, 0.0, 0.0); dec2phase(t10); delay(lambda-pwS4*0.5-pwS6*0.4); h_shapedpulse("eburp2",4.0,3.5,zero, 0.0, 0.0); delay((gt1/10.0) + 1.0e-4 +gstab + 2.0*GRADIENT_DELAY + POWER_DELAY); h_shapedpulse("reburp",4.0,3.5,zero, 0.0, 0.0); zgradpulse(icosel*gzlvl2, gt1/10.0); /* 2.0*GRADIENT_DELAY */ delay(gstab); } else { h_shapedpulse("eburp2",4.0,3.5,zero, 2.0e-6, 0.0); zgradpulse(gzlvl5, gt5); delay(lambda-pwS6*0.4 - gt5); h_sim3shapedpulse("reburp",4.0,3.5,0.0,2.0*pwN, zero, zero, zero, 0.0, 0.0); zgradpulse(gzlvl5, gt5); delay(lambda-pwS6*0.4 - gt5-POWER_DELAY-1.0e-4); } dec2power(dpwr2); /* POWER_DELAY */ lk_sample(); if (SE_flg[0] == 'y') setreceiver(t13); else setreceiver(t12); statusdelay(C,1.0e-4 ); }
pulsesequence() { char shname1[MAXSTR], f1180[MAXSTR], f2180[MAXSTR], n15_flg[MAXSTR], CT_flg[MAXSTR]; int icosel, t1_counter, t2_counter, ni2 = getval("ni2"), phase; double d2_init=0.0, d3_init=0.0, pwS1,pwS2,pwS3,pwS4,pwS5,pwS6, kappa, lambda = getval("lambda"), CTdelay = getval("CTdelay"), gzlvl1 = getval("gzlvl1"), gzlvl2 = getval("gzlvl2"), gzlvl4 = getval("gzlvl4"), gzlvl5 = getval("gzlvl5"), gzlvl6 = getval("gzlvl6"), gt1 = getval("gt1"), gt4 = getval("gt4"), gt5 = getval("gt5"), gt6 = getval("gt6"), gstab = getval("gstab"), scale = getval("scale"), sw1 = getval("sw1"), tpwrsf = getval("tpwrsf"), shlvl1, shpw1 = getval("shpw1"), pwC = getval("pwC"), pwClvl = getval("pwClvl"), pwNlvl = getval("pwNlvl"), pwN = getval("pwN"), dpwr2 = getval("dpwr2"), d2 = getval("d2"), t2a,t2b,halfT2, t1a,t1b,halfT1, shbw = getval("shbw"), shofs = getval("shofs")-4.77, timeTN = getval("timeTN"), timeTN1 = getval("timeTN1"), timeCN = getval("timeCN"), tauC = getval("tauC"), tauCC = getval("tauCC"), tau1 = getval("tau1"), tau2 = getval("tau2"), taunh = getval("taunh"); getstr("shname1", shname1); getstr("f1180",f1180); getstr("f2180",f2180); getstr("n15_flg",n15_flg); getstr("CT_flg",CT_flg); phase = (int) (getval("phase") + 0.5); settable(t1,2,phi1); settable(t2,4,phi2); settable(t3,1,phi3); settable(t4,8,phi4); settable(t5,1,phi5); settable(t14,8,phi14); settable(t24,8,phi24); /* INITIALIZE VARIABLES */ kappa = 5.4e-3; //shpw1 = pw*8.0; shlvl1 = tpwr; f1180[0] ='n'; f2180[0] ='n'; pwS1 = c13pulsepw("co", "ca", "sinc", 90.0); pwS2 = c13pulsepw("co", "ca", "sinc", 180.0); pwS3 = c13pulsepw("ca", "co", "square", 180.0); pwS4 = h_shapedpw("eburp2",shbw,shofs,zero, 0.0, 0.0); pwS6 = h_shapedpw("reburp",shbw,shofs,zero, 0.0, 0.0); pwS5 = h_shapedpw("pc9f",shbw,shofs,zero, 2.0e-6, 0.0); if (phase == 1) ; if (phase == 2) {tsadd(t1,1,4);} if ( phase2 == 2 ) { tsadd ( t3,2,4 ); tsadd ( t5,2,4 ); icosel = +1; } else icosel = -1; /* Set up f1180 */ tau1 = d2; if((f1180[A] == 'y') && (ni > 1.0)) { tau1 += ( 1.0 / (2.0*sw1) ); if(tau1 < 0.2e-6) tau1 = 0.0; } tau1 = tau1; /* Set up f2180 */ tau2 = d3; if((f2180[A] == 'y') && (ni2 > 1.0)) { tau2 += ( 1.0 / (2.0*sw2) ); if(tau2 < 0.2e-6) tau2 = 0.0; } tau2 = tau2; /************************************************************/ if( ix == 1) d2_init = d2; t1_counter = (int) ( (d2-d2_init)*sw1 + 0.5 ); if(t1_counter % 2) { tsadd(t1,2,4);tsadd(t14,2,4); tsadd(t24,2,4); } if( ix == 1) d3_init = d3; t2_counter = (int) ( (d3-d3_init)*sw2 + 0.5 ); if(t2_counter % 2) { tsadd(t4,2,4); tsadd(t14,2,4); tsadd(t24,2,4); } /************************************************************/ /* Set up CONSTANT/SEMI-CONSTANT time evolution in N15 */ /************************************************************/ if (ni2 > 1) { halfT2 = 0.5*(ni2-1)/sw2; t2b = (double) t2_counter*((halfT2 - timeTN)/((double)(ni2-1))); if( ix==1 && halfT2 - timeTN > 0 ) printf("SCT mode on, max ni2=%g\n",timeTN*sw2*2+1); if(t2b < 0.0) t2b = 0.0; t2a = timeTN - tau2*0.5 + t2b; if(t2a < 0.2e-6) t2a = 0.0; } else { t2b = 0.0; t2a = timeTN - tau2*0.5; } /************************************************************/ if (ni > 1) { halfT1 = 0.5*(ni-1)/sw1; t1b = (double) t1_counter*((halfT1 - timeTN1)/((double)(ni-1))); if(t1b < 0.0) t1b = 0.0; t1a = timeTN1 - tau1*0.5 + t1b; if(t1a < 0.2e-6) t1a = 0.0; } else { t1b = 0.0; t1a = timeTN1 - tau1*0.5; } /************************************************************/ status(A); rcvroff(); decpower(pwClvl); decoffset(dof); dec2power(pwNlvl); dec2offset(dof2); obspwrf(tpwrsf); decpwrf(4095.0); obsoffset(tof); set_c13offset("co"); dec2rgpulse(pwN*2.0,zero,0.0,0.0); zgradpulse(1.7*gzlvl4, gt4); delay(1.0e-4); lk_sample(); delay(d1-gt4); lk_hold(); h_shapedpulse("pc9f",shbw,shofs,zero, 2.0e-6, 0.0); delay(lambda-pwS5*0.5-pwS6*0.5); h_sim3shapedpulse("reburp",shbw,shofs,0.0,2.0*pwN, one, zero, zero, 0.0, 0.0); delay(lambda-pwS5*0.5-pwS6*0.5); if(n15_flg[0]=='y') h_shapedpulse("pc9f_",shbw,shofs,three, 0.0, 0.0); else h_shapedpulse("pc9f_",shbw,shofs,one, 0.0, 0.0); shaped_pulse(shname1,shpw1,zero,0.0,0.0); zgradpulse(2.3*gzlvl4, gt4); delay(1.0e-4); /**************************************************************************/ /*** N -> CO transfer *********************************/ /**************************************************************************/ dec2rgpulse(pwN,t1,0.0,0.0); delay(tau1*0.5); c13pulse("ca", "co", "square", 180.0, zero, 0.0, 0.0); delay(taunh-pwS3); shaped_pulse(shname1,shpw1,two,0.0,0.0); delay(timeTN1-pwS2-taunh-shpw1); c13pulse("co", "ca", "sinc", 180.0, zero, 0.0, 0.0); delay (t1b); dec2rgpulse (2.0*pwN, zero, 0.0, 0.0); delay (t1a); dec2rgpulse(pwN,zero,0.0,0.0); /**************************************************************************/ /*** CO -> CA transfer *********************************/ /**************************************************************************/ c13pulse("co", "ca", "sinc", 90.0, t2, 2.0e-6, 0.0); zgradpulse(-gzlvl4, gt4); decphase(zero); delay(tauC - gt4 - 0.5*10.933*pwC); decrgpulse(pwC*158.0/90.0, zero, 0.0, 0.0); decrgpulse(pwC*171.2/90.0, two, 0.0, 0.0); decrgpulse(pwC*342.8/90.0, zero, 0.0, 0.0); /* Shaka 6 composite */ decrgpulse(pwC*145.5/90.0, two, 0.0, 0.0); decrgpulse(pwC*81.2/90.0, zero, 0.0, 0.0); decrgpulse(pwC*85.3/90.0, two, 0.0, 0.0); zgradpulse(-gzlvl4, gt4); decphase(one); delay(tauC - gt4 - 0.5*10.933*pwC - WFG_START_DELAY - 2.0e-6); c13pulse("co", "ca", "sinc", 90.0, one, 0.0, 0.0); /**************************************************************************/ /*** CA -> N transfer *********************************/ /**************************************************************************/ set_c13offset("ca"); c13pulse("ca", "co", "square", 90.0, zero, 2.0e-6, 0.0); delay(tauC); c13pulse("co", "ca", "sinc", 180.0, zero, 0.0, 0.0); delay(timeCN-tauC); sim3_c13pulse("", "cab", "co", "square", "", 0.0, 180.0, 2.0*pwN, zero, zero, zero, 2.0e-6, 2.0e-6); delay(timeCN); c13pulse("co", "ca", "sinc", 180.0, zero, 0.0, 0.0); c13pulse("ca", "co", "square", 90.0, one, 2.0e-6, 0.0); /**************************************************************************/ /*** N -> CA back transfer *********************************/ /**************************************************************************/ dec2rgpulse(pwN,t4,0.0,0.0); delay(tau2*0.5); c13pulse("co", "ca", "sinc", 180.0, zero, 0.0, 0.0); //delay(timeTN-pwS3-pwS2-gt1-1.0e-4); delay(timeTN-pwS3-pwS2-gt1-1.0e-4-2.0*GRADIENT_DELAY-4*POWER_DELAY-4*PWRF_DELAY-(4/PI)*pwN); zgradpulse(-gzlvl1, gt1); delay(1.0e-4); c13pulse("ca", "co", "square", 180.0, zero, 0.0, 0.0); delay (t2b); dec2rgpulse (2.0*pwN, zero, 0.0, 0.0); delay (t2a); /**************************************************************************/ delay(gt1/10.0+1.0e-4); h_shapedpulse("eburp2_",shbw,shofs,t3, 2.0e-6, 0.0); zgradpulse(gzlvl5, gt5); delay(lambda-pwS6*0.5-pwS4*scale- gt5); h_sim3shapedpulse("reburp",shbw,shofs,0.0,2.0*pwN, zero, zero, zero, 0.0, 0.0); zgradpulse(gzlvl5, gt5); delay(lambda-pwS6*0.5-pwS4*scale- gt5); h_shapedpulse("eburp2",shbw,shofs,zero, 0.0, 0.0); delay(gt1/10.0+1.0e-4); dec2rgpulse(pwN,one,0.0,0.0); zgradpulse(gzlvl6, gt6); txphase(zero); delay(lambda-pwS6*0.5-gt6); h_sim3shapedpulse("reburp",shbw,shofs,0.0,2.0*pwN, zero, zero, zero, 0.0, 0.0); zgradpulse(gzlvl6, gt6); delay(lambda-pwS6*0.5-gt6); dec2rgpulse(pwN,t5,0.0,0.0); /**************************************************************************/ zgradpulse(-icosel*gzlvl2, gt1/10.0); dec2power(dpwr2); /* POWER_DELAY */ lk_sample(); if (n15_flg[0] =='y') { setreceiver(t14); } else { setreceiver(t24); } rcvron(); statusdelay(C,1.0e-4 ); }